摘要
本文用高效液相色谱法测定金银花中保卫田残留量,使用ODS柱,流动相2%NH_4Ac-甲醇(6:4),流速1mL/min,柱温30℃,紫外检测器检测波长285nm。方法加标回收率80.3%~89.4%,方法最低检出浓度0.02μg/g。
A reversed phase high performance liquidchromatographic method is described for de-termining carbendazim residue in honeysuck-le. With an ODS column, the mobile phase is2% NH_4Ac aqueous solution: methanol (6:4) at a flow rate of 1mL/min, column temper-ature 30℃, UV detection wavelength at285nm. The carbendazim recovery rate is 80.3%~89.4% and the lowest detection concen-tration is 0.02μg/g
出处
《分析试验室》
CAS
CSCD
北大核心
1996年第3期82-83,共2页
Chinese Journal of Analysis Laboratory