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气相合成氮化铁纳米粉末及其物性表征 被引量:11

SYNTHESISOF NITRIDED-IRON NANOMETER POWDER BY THERMAL CHEMICAL VAPOR-PHASE REACTION METHOD AND CHARACTERIZATION OF ITS PHYSICAL PROPERTIES
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摘要 Nitrided- iron nanometer powder is prepared by thermal chemical vapor- phase reaction method,using Fe Cl2 · n H2 O and NH3 as starting material.The physical properties of the powder is measured by means of XRD,XPS,TEM,VSM etc,and physical phase shape, size and magneticpropertiesof the powderis also characterized.Experimentresults show ni- trided- iron ultrafine powder of uniform,high pure,chain- of- spherical and high magnetics can be prepared by improving synthesis reaction instrument.The physical property index of the powder prepared in this instrumentis preferable to Tanaka′s same study results. Nitrided- iron nanometer powder is prepared by thermal chemical vapor- phase reaction method,using Fe Cl2 · n H2 O and NH3 as starting material.The physical properties of the powder is measured by means of XRD,XPS,TEM,VSM etc,and physical phase shape, size and magneticpropertiesof the powderis also characterized.Experimentresults show ni- trided- iron ultrafine powder of uniform,high pure,chain- of- spherical and high magnetics can be prepared by improving synthesis reaction instrument.The physical property index of the powder prepared in this instrumentis preferable to Tanaka′s same study results.
出处 《无机化学学报》 SCIE CAS CSCD 北大核心 1996年第1期88-91,共4页 Chinese Journal of Inorganic Chemistry
基金 黑龙江省自然科学基金资助项目
关键词 热化学气相法 氮化铁 纳米粉末 纳米材料 thermal chemical vapor- phase reaction method nitrided- iron nanometer powder
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参考文献4

  • 1曹茂盛,硅酸盐通报,1995年,6期,36页
  • 2曹茂盛,超微颗粒制备科学与技术,1995年
  • 3曹惠民,无机化合物合成手册.1,1983年
  • 4曹茂盛,941090426

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