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液相色谱多残留测定氨基甲酸酯农药的方法 被引量:2

Determination of N-methylcarbamates in water by post-column derivatization HPLC
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摘要 采用反相液相色谱柱后荧光衍生的方法测定了水质中的涕灭威风、西维因、呋喃丹及其代谢产物3-羟基呋喃丹和3-酮基呋喃丹的残留,样品通过大网状XAD-7树脂进行了富集和净化。在NuclessiIC_8柱上分离,然后通过氧化镁短柱水解和邻苯二甲醛荧光衍生,荧光检测E_x338nm,E_M455nm,最低检测浓度为1ng/mL方法回收率达75%-98%,相对标准偏差为0.036。
出处 《浙江农业大学学报》 CSCD 1995年第4期403-406,共4页
基金 浙江省测试基金
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  • 1高学军,李庆章.苯并咪唑氨基甲酸酯类抗蠕虫药物作用机理研究进展[J].东北农业大学学报,2004,35(4):492-495. 被引量:15
  • 2那晓琳,张旸,陈文华.高效液相色谱测定水源水中西维因[J].中国卫生检验杂志,1995,5(2):77-78. 被引量:5
  • 3李崇瑛,卢彦,余利军,余朝琦.在线富集高效液相色谱法检测水样中的克百威残留[J].成都理工大学学报(自然科学版),2005,32(4):383-385. 被引量:7
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