摘要
甲丙氨酯经酸水解，酰胺键断裂，游离ＮＨ可与Ｎａ－ＴＰＢ定量形成沉淀。本文即以此原理，用交流示波极谱法测定其含量，回收率为９９．４９％，ＲＳＤ为０．０９３％（ｎ＝４）。
Meprobamate was hydrolyzed in acid condition to cleavage its amide bond, and the decomposed group NH yielded. NH reacts with Na-TPB and produces precipitate quantitatively.According to these conditions, Meprobamate was determined by Oscillopolarographic method.Recovery is 99.49%. Relative standard deviation is 0.093%(n=4).
出处
《药物分析杂志》
CAS
CSCD
北大核心
1995年第3期31-32,共2页
Chinese Journal of Pharmaceutical Analysis
