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^(35)S-稻丰散的制备 被引量:2

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摘要 稻丰散(Ersan)即O,O-二甲基-S(苯基乙酸酯)。其^(35)S标记物制备,可由^(35)S-五硫化二磷与甲醇制成O,O-二甲基二硫代磷(CH_3O)_2P^(35)S,进而制备O,O-二甲基二硫代磷酸酯钠盐,后者再与α-氯代苯乙酸乙酯作用,合成^(35)S-稻丰散。放化收率26%。
作者 綦立元
出处 《核农学通报》 1995年第5期245-246,共2页
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  • 1王萍,周志强,叶贵标,王鹏,任红,王秋霞,江树人.高效液相色谱纤维素类手性固定相对外消旋稻丰散的拆分[J].农药,2004,43(12):542-543. 被引量:6
  • 2雷进海.有机磷农药相转移催化合成技术进展[J].河南化工,1994,13(9):2-4. 被引量:1
  • 3费永成.稻丰散的生产及其市场前景[J].化工时刊,2007,21(8):54-57. 被引量:3
  • 4Kimihiko Yoshii, Yukari Tsumum, Susumu Ishimitsu., et al. Degradation of Malathion and Phenthoate by Glutathione Reductase in Wheat Germ[J]. J. Agric. Food Chem. 2000, 48: 2502 - 2505
  • 5Mahmoud Mahajna, Gary B Quistad, John E Casida. S-Methylation of O, 0 - Dialkyl Phosphorodithioic Acids : O, O, S-Trimethyl Phosphorodithioate and phosphorothiolate Metabolites of Dimethoate in Mice [ J] . Chem. Res. Toxicol. 1996, 9:1202- 1206
  • 6Dennis Y Takade, Thurman Allsup, Abdallah Khasawinah., et al. Metabolism of O, O - dimethyl S - [ α - carboethoxy) benzyl] phosphorodithioate (phenthoate) in the white mouse and house flies [ J ]. Pesticide Biochemistry and Physiology, 1976,6 (4) :367 - 376
  • 7http ://www. fao. org/ag/agp/agpp/Pesticid/JMPR/Dowrdoad/ 81/Penthoat. PDF.
  • 8M A Al - Omar, R H Al - Suhaily, Y Kamel. Distribution and Dissipation of Phenthoate Insecticide Following Aerial Application[J]. Bulletin of Environmental Conta mination and Toxicology, 2004, 73(5) :825 - 831
  • 9Zhao - Yang Li, Zhi - Chao Zhang, Qi - Lin Zhou., et al. Fast and precise determination of phenthoate and its enantiomeric ratio in soil by the matrix solid - phase dispersion method and liquid chromatography[ J]. Journal of Chromatography A, 2002, 977( 1 ) : 17 - 25
  • 10Carmen Garcia - Ruiz, Gloria Alvarez - Llamas, Angel Puerta., et al. Enantiomeric separation of organophosphorus pesticides by capillary electrophoresis - Application to the determination of malathion in water samples after preconcentration by off- line solid- phase extraction[J]. Analytica Chimica Acta, 2005,543(1 - 2) :77 - 83

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