摘要
用新型测定卤素的方法:石墨炉原子化元素特种检测器检测法,研究了氯元素在该仪器上的响应行为;测定出该方法对氯元素的检出限为5ng,线性范围为10ng~1.5μg,平均相对标准偏差为2.65%,用该法对实际水样品的测定结果与离子色谱法测定结果相吻合。研究结果亦表明,这种新型分析方法具有简单、快速、对卤素选择性好、可测无机氯和有机氯的特点。
The element specific detector(ESD)is connected to a graphite furnace HGA-500。By means of this new analytical technique,the determination of chloride compound in differentsamples has been tried.Samples are prepared using Li-form exchange resin, then analyseddirectly. The detection limit is 5 ng and the relative standard deviation(RSD)is 2.65%. Thedetermination of real samples shows that the new analysis method is simple,reliabe and suitablefor the determination of chloride in natural water.
出处
《大连理工大学学报》
EI
CAS
CSCD
北大核心
1995年第3期334-338,共5页
Journal of Dalian University of Technology
关键词
水质分析
氯
检测器
石墨化炉
water quality analysis
chlorine
detector units
graphitizing furnace