摘要
报道了以呋喃和顺丁烯二酸酐为原料,主要通过Diels-Alder反应合成蒽环酮2-乙酰基-5,12-二乙酰氧基-1,2,3,4-四氢-6,11-并四苯醌的路线,总产率达15％左右。用红外光谱,~1H核磁共振谱和质谱表征合成产物。
This paper reported the synthesis of anthracyclinone 2-acetyl-5 12-diacetoxy-l,2,3,4-tetrahydro-6,11-naphthacenequinone mainly by the Diels-Alder reaction with an overall yield of 15%, starting from furan and maleic anhydride. The structure of the products were characterised by IR,'HNMR and MS.
出处
《厦门大学学报（自然科学版）》
CAS
CSCD
北大核心
1989年第4期401-405,共5页
Journal of Xiamen University：Natural Science
基金
国家教育委员会基金
关键词
DIELS-ALDER
蒽环酮
合成
Diel-Alder Reaction, Anthracyclinone, 2-Acetyl- 5-12-diacetoxy-1,2,3,4-tetrahydro 6-ll,naphthaceaequinone.
