摘要
以硫酸二甲酯为烷基化剂,与间甲酚在碱性条件下进行反应,合成间甲苯甲醚,系统地研究了反应物用量比,反应温度,反应时间等因素对间甲苯甲醚产率的影响.在最佳工艺条件下,其产率可达99%.
<Abstrcat>Under the alkali conditions, m-methylanisole was synthesized from m-cresol and dimethyl sulfate . The influence of reaction time, reaction temperature and the amount of materials on the yield of the product was studied systematically and the optimized technique conditions were then determined, under which m-methylanisole was obtained 99% yield.
出处
《福建师范大学学报(自然科学版)》
CAS
CSCD
北大核心
2005年第2期55-57,共3页
Journal of Fujian Normal University:Natural Science Edition
基金
福建省教育厅基金资助项目(JA00165).