摘要
采用离心脱水、取样器取样、混合酸分解、亚铁还原-钒酸铵容量法测定树脂中的铀。方法简便、快速,精密度≤±5%,回收率达98%-100%.1.5h可测定10个树脂样。
simple and rapid volumetrical method for determination of the uranium in the ion-exchange resin was proposed. The uranium was determined by volumetry.using ammonium vanadate after centrifugal dewatering of the resin, sampling with a specially-disigned sampler, decomposition with H2SO4,HNO, and HClO4, and reduction with Fe2+. The precision of the method was ≤±5%, and the recovery reached 98%-100%. 10 resin samples could be analysed within 1. 5h.
出处
《铀矿冶》
CAS
1994年第1期53-56,共4页
Uranium Mining and Metallurgy
关键词
铀
树脂
容量法
测量
Uranium
Resin
Volumetry
Dewatering