摘要
以炔醛法合成１，４一丁二醇反应的炔化反应过程和加氢反应过程为研究对象，应用工业反应过程开发方法的基本原则，进行炔化反应和加氢反应开发方法的论述，包括确定优选工艺条件、反应器型大的选择和反应器的主要工程问题。从小试、中试、冷漠试验到工业规模试验，为大型装置设计提供依据。
The syntheSis of 1,4-butanediol by acetylenation and hydrogenation is presented in thispaper.The basic principles used for the process development methods of these industrial reac-tions are discussed,including optimization of reaction condition,selection of reactor typeand also the main engineering problems of the reactor considered.The study was done withlaboratory bench-scale,pilot-scale and finally industrial scale reactor,and a complete setof design information for large scale equipment was established.
出处
《石油化工》
CAS
CSCD
北大核心
1994年第5期313-319,共7页
Petrochemical Technology
关键词
丁二醇
炔醛法
合成
butyne-1,4-dio1,1,4-butanediol,trickle-bed,slurry-bed,process development and scale-up
