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三(三溴苯氧基)三聚氰酸酯的合成 被引量:7

SYNTHESIS OF TRI(TRI-BROMOPHENOXY)CYANURATE
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摘要 以三聚氯氰(CNCl)3和三溴苯酚(TBP)为主要原料,于水溶液中在催化剂、还原剂存在下合成了1种新型含溴氮三嗪的添加型阻燃剂,当n(CNCl)3/n(TBP)=1∶3~3 1时,产品产率可达98%,纯度大于97%。 A novel bromo-and nitrogen-containing triazine,additive flame retardant,was synthesized using tricyanogen chloride (CNCl)_3 and tribromophend as main raws in water-containing solution and in the present of catalyst and reducer and it showed that the rate of production was more than 98 percent and its purity was more than 97 percent while mole ratio of n(CNCl)_3/n(TBP)=1∶3~3.1 in this paper.
出处 《热固性树脂》 CAS CSCD 2005年第1期25-27,共3页 Thermosetting Resin
关键词 三(三溴苯氧基)三聚氰酸酯 阻燃剂 合成 tri-(tri-bromophenoxy)cyanurate flame retardant synthesis.
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参考文献4

  • 1Zimmermann Jeanp. Halo- , alkoxy- , and amino-1, 3, 5-triazine [P]. FR 1566 675, 1969.
  • 2Setsuo Nishibori shiga, Hideto Kondo. Highly concentrated aqueous tribromophenolate solution and a method for preparing the same[P]. US 5 696 302, 1997.
  • 3Klinkenberg, Herbert, Petersen. Preparation of tri- (hatophenoxy) - sym- triazines [P]. US 4 039 538, 1977.
  • 4Nishibori Setsuo, Nabeshima Toshiichi. Fire- resistant thermoplastic resin compositions with excellent heat and weather resistance[P]. JP 94 128 410.1994.

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