摘要
以甲苯为溶剂 ,用NaHSO4催化假性紫罗兰酮合成紫罗兰酮 ,收率 60 %。考察了反应温度、反应时间、催化剂用量及其它相关因素对收率的影响 ,确立了优化的反应条件。
Ionone with the yield of 60% was synthesized from pseudoionone catalysed by NaHSO 4 with toluene as a solvent. The effects of reaction temperature, reaction time, the amount of catalyst used and other related factors on the yield of ionone were investigated to obtain the optimal reaction conditions.
出处
《合成化学》
CAS
CSCD
2004年第6期589-590,共2页
Chinese Journal of Synthetic Chemistry
