摘要
详细论述了溶剂在2,4,6-三氯苯胺合成中的作用和影响。提出了用冰醋酸-甲醇混合物作溶剂,结果表明,2,4,6-三氯苯胺的得率和纯度分别达到80％～85％和98％以上。
The function and influence of solevents in the synthesis of 2,4,6-trichloroaniline were discussed in detail. A new mixed solvent containing methanol and acetic acid was introduced. The yield and purity of 2,4,6-trichioroaniline were 80％～85％ and above 98％ respeodvely.
出处
《精细石油化工》
CAS
CSCD
1993年第2期35-38,共4页
Speciality Petrochemicals
关键词
三氯苯胺
溶剂
冰醋酸
甲醇
2,4,6-trichloroaniline
Mixed Solvent
Acetic Acid
Methanol
