摘要
The nanocrystalline γ-(Fe,Ni) alloy whiskers have been prepared by chemical reduction of Fe2+ and Ni2+ ions with potassium borohydride under the function of a dispersant agent PE followed by heat treatment at 600℃ under the protection of nitrogen.Conditions, such as quantity of NaOH, concentration of salts, and species of surfactants, of preparation of Fe-Ni alloy have been discussed. X-ray diffraction(XRD), transmission electron microscopy(TEM) and vibrating sample magnetometer(VSM) characterized the synthesized Fe-Ni alloy. Character, capability and use of the materials have been summarized.
The nanocrystalline γ - ( Fe, Ni) alloy whiskers have been prepared by chemical reduction of Fe 2+ and Ni 2+ ions with potassium borohydride under the function of a dispersant agent PE followed by heat treatment at 600℃ under the protection of nitrogen . Conditions, such as quantity of NaOH, concentration of salts, and species of surfactants, of preparation of Fe - Ni alloy have been discussed. X-ray diffraction ( XRD) , transmission electron microscopy ( TEM ) and vibrating sample magnetometer (VSM) characterized the synthesized Fe-Ni alloy. Character, capability and use of the materials have been summarized.
