This paper focuses on work related to post irradiation examination of 300-series austenitic stainless steel taken from reactor vessel internals of PWR. High neutron irradiation dose in NNP＇s leads to a degradation of...This paper focuses on work related to post irradiation examination of 300-series austenitic stainless steel taken from reactor vessel internals of PWR. High neutron irradiation dose in NNP＇s leads to a degradation of microstructure of the material in a nano-metric scale. Hence, it is important to characterize the irradiated materials to understand the physical basis of the degradation mechanisms. Microstructural characterization of neutron-irradiated materials by TEM requires enhanced sample preparation methodologies, which commonly needs general improvements regarding particular experiment to be performed. In this study, the authors have developed methodology specialized in 1 mm TEM thin foil preparation from a deformed shank of a broken miniaturized tensile specimen. TEM foil size in current studies is smaller than standard because of the small shank diameter and high radioactivity of the studied material. The reduction of the TEM foil radioactivity to minimum is crucial to perform EDX chemical analysis and to increase the EDX detector lifetime. This paper describes whole process from bulk sample handling, including remote-controlled material cutting in shielded hot-cells and disc polishing in glow-boxes, up to the final procedure of electrolytic-polishing of electron transparent 1 mm TEM foils. Eventually, results of TEM microanalysis of radiation-induced defects were present.展开更多
Ultrasonic testing is a very important non-destructive method for testing components for safety of nuclear power plants and other security and delicate parts in other industries. Nowadays, thanks to the development of...Ultrasonic testing is a very important non-destructive method for testing components for safety of nuclear power plants and other security and delicate parts in other industries. Nowadays, thanks to the development of computer technology, it is possible to simulate processes which occur during ultrasonic testing. That is why numerical simulations are becoming an integral part of non-destructive testing. Simulations are used to determine parameters of ultrasonic examination, especially parameters of probes and scan plan and also in the analysis of results. They are used in such cases, when it is necessary to verify applicability of probes and methods. This verification could be provided on the weld and test block which are not manufactured. It could be also provided on defects, which are not manufactured in test block, but their presence is possible in given weld joint. Simulations are very useful for verifying the propagation of ultrasonic signal in given area (e.g. weld area). If movement of probe is limited, possibility of whole volume scan should be verified.展开更多
文摘This paper focuses on work related to post irradiation examination of 300-series austenitic stainless steel taken from reactor vessel internals of PWR. High neutron irradiation dose in NNP＇s leads to a degradation of microstructure of the material in a nano-metric scale. Hence, it is important to characterize the irradiated materials to understand the physical basis of the degradation mechanisms. Microstructural characterization of neutron-irradiated materials by TEM requires enhanced sample preparation methodologies, which commonly needs general improvements regarding particular experiment to be performed. In this study, the authors have developed methodology specialized in 1 mm TEM thin foil preparation from a deformed shank of a broken miniaturized tensile specimen. TEM foil size in current studies is smaller than standard because of the small shank diameter and high radioactivity of the studied material. The reduction of the TEM foil radioactivity to minimum is crucial to perform EDX chemical analysis and to increase the EDX detector lifetime. This paper describes whole process from bulk sample handling, including remote-controlled material cutting in shielded hot-cells and disc polishing in glow-boxes, up to the final procedure of electrolytic-polishing of electron transparent 1 mm TEM foils. Eventually, results of TEM microanalysis of radiation-induced defects were present.
文摘Ultrasonic testing is a very important non-destructive method for testing components for safety of nuclear power plants and other security and delicate parts in other industries. Nowadays, thanks to the development of computer technology, it is possible to simulate processes which occur during ultrasonic testing. That is why numerical simulations are becoming an integral part of non-destructive testing. Simulations are used to determine parameters of ultrasonic examination, especially parameters of probes and scan plan and also in the analysis of results. They are used in such cases, when it is necessary to verify applicability of probes and methods. This verification could be provided on the weld and test block which are not manufactured. It could be also provided on defects, which are not manufactured in test block, but their presence is possible in given weld joint. Simulations are very useful for verifying the propagation of ultrasonic signal in given area (e.g. weld area). If movement of probe is limited, possibility of whole volume scan should be verified.
