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Biodiesel Production by Enzymatic Catalysis Process Using Two Analytical Ways: Gas Chromatography and Total Glycerol Determination
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作者 Ignacio Contreras Andrade Jonathan Parra Santiago +2 位作者 Jose Ricardo Sodre Joseph Sebastian Pathiyamattom Carlos Alberto Guerrero-Fajardo 《Journal of Chemistry and Chemical Engineering》 2014年第7期717-726,共10页
Currently, biodiesel is presented as one of the best alternatives for gradually replacing the use of fossil fuels, but it has some factors that make it economically impractical if it does not have a government support... Currently, biodiesel is presented as one of the best alternatives for gradually replacing the use of fossil fuels, but it has some factors that make it economically impractical if it does not have a government support. For this reason, research efforts focused on this area have been responsible for optimizing the process of biodiesel production by different catalytic routes to achieve greater efficiency at a lower cost. In this case, the biggest problem has been the high cost generated by an investigation, which in many occasions is the main factor to decide if an investigation could be carried out. Trying to reduce these costs, in the current study, we are using a technique of glycerol quantification by volumetric methods and comparing obtained results with the chromatographic method, which is conventionally used and comparatively much more expensive. Biodiesel employee was obtained by an enzymatic catalysis process varying one of three process variables:oil:alcohol molar ratio, temperature and proportion of catalyst. The numerical differences obtained between the two quantification methods generated relative errors lower than 10%, resulting in some occasions lower than 1%. By gas chromatography analysis the best yield was obtained at the same conditions of the volumetric method, a temperature of 45 ℃, an oil:alcohol ratio 1:4 and 8 wt.% of catalyst, but a yield of 95.5% and 97.1%, respectively. Due to the high precision of gas chromatography, this method is used to carry out a surface response analysis obtaining as ideal operating conditions a temperature of 43.5 ℃, 8.9 wt.%. of catalyst and an oil:alcohol ratio 1:4. 展开更多
关键词 Biodiesel production glycerol determination gas chromatography enzymatic catalysis.
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Electromagnetic Torque Estimation of a Three-Phase Induction Motor for Setting the Feedrate of a Milling Machine
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作者 Elida Fernanda Xavier Julio Simplicio Amaud da Silva +1 位作者 Cicero da Rocha Souto Isaac Soares de Freitas 《Journal of Mechanics Engineering and Automation》 2014年第6期511-520,共10页
In this paper, it presents a project of a fuzzy controller and a neural estimator to control a coordinate table powered by three-phase induction motor, aiming to implement an intelligent milling system. The position/s... In this paper, it presents a project of a fuzzy controller and a neural estimator to control a coordinate table powered by three-phase induction motor, aiming to implement an intelligent milling system. The position/speed control is performed using vector techniques of three-phase induction machines. The estimation of the motor electromagnetic torque is used for setting the feedrate of the table. The speed control is developed using TS (Takagi-Sugeno) fuzzy logic model and electromagnetic torque estimation using neural network type LMS (least mean square) algorithm. The induction motor is powered by a frequency inverter driven by a DSP (digital signal processor). Control strategies are implemented in DSP. Simulation results are presented for evaluating the performance of the system. 展开更多
关键词 MACHINING speed control torque estimation fuzzy logic neural network
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