Wettability is an important phenomenon in the liquid phase sintering of silicon carbide （SiC） ceramics. This work involved a study of the wetting of SiC ceramics by two oxide systems, Al2O3 /Dy2O3 and Al2O3 /Yb2O3, ...Wettability is an important phenomenon in the liquid phase sintering of silicon carbide （SiC） ceramics. This work involved a study of the wetting of SiC ceramics by two oxide systems, Al2O3 /Dy2O3 and Al2O3 /Yb2O3, which have so far not been studied for application in the sintering of SiC ceramics. Five mixtures of each system were prepared, with different compositions close to their respective eutectic ones. Samples of the mixtures were pressed into cylindrical specimens, which were placed on a SiC plate and subjected to temperatures above their melting points using a graphite resistance furnace. The behavior of the melted mixtures on the SiC plate was observed by means of an imaging system using a CCD camera and the sessile drop method was employed to determine the contact angle, the parameter that measures the degree of wettability. The results of variation in the contact angle as a function of temperature were plotted in graphic form which showed that the curves displayed a fast decline and good spreading. All the samples of the two systems presented final contact angles of 40o to 10o indicating their good wetting on SiC in the argon atmosphere. The melted/solidified area and interface between SiC and melted/solidified phase were evaluated by scanning electron microscopy （SEM） and their crystalline phases were identified by X-ray diffraction （DRX）. The DRX analysis showed that Al2O3 and RE2O3 reacted and formed the Dy3Al5O12 （DyAg） and Yb3Al5O12 （YbAg） phases. The results indicated that the two systems had a promising potential as additives for the sintering of SiC ceramics.展开更多
As low cost and highly portable sensors, inertial measurements units (IMU) have become increas-ingly used in gait analysis, embodying an efficient alternative to motion capture systems. Mean-while, being able to compu...As low cost and highly portable sensors, inertial measurements units (IMU) have become increas-ingly used in gait analysis, embodying an efficient alternative to motion capture systems. Mean-while, being able to compute reliably accurate spatial gait parameters using few sensors remains a relatively complex problematic. Providing a clinical oriented solution, our study presents a gy-rometer and accelerometer based algorithm for stride length estimation. Compared to most of the numerous existing works where only an averaged stride length is computed from several IMU, or where the use of the magnetometer is incompatible with everyday use, our challenge here has been to extract each individual stride length in an easy-to-use algorithm requiring only one inertial sensor attached to the subject shank. Our results were validated on healthy subjects and patients suffering from Parkinson’s disease (PD). Estimated stride lengths were compared to GAITRite? walkway system data: the mean error over all the strides was less than 6% for healthy group and 10.3% for PD group. This method provides a reliable portable solution for monitoring the in-stantaneous stride length and opens the way to promising applications.展开更多
基金supported by Brazilian Research Funding Agencies FAPESP(So Paulo Research Foundation)(Project 2010/51925-6,Process 2012/01177-9,and Process 2012/01665-3)CNPq(National Council for Scientific and Technological Development)(Process 304760/2010-2)CAPES(Federal Agency for the Support and Improvement of Higher Education)(Project 33002088001P4)
文摘Wettability is an important phenomenon in the liquid phase sintering of silicon carbide （SiC） ceramics. This work involved a study of the wetting of SiC ceramics by two oxide systems, Al2O3 /Dy2O3 and Al2O3 /Yb2O3, which have so far not been studied for application in the sintering of SiC ceramics. Five mixtures of each system were prepared, with different compositions close to their respective eutectic ones. Samples of the mixtures were pressed into cylindrical specimens, which were placed on a SiC plate and subjected to temperatures above their melting points using a graphite resistance furnace. The behavior of the melted mixtures on the SiC plate was observed by means of an imaging system using a CCD camera and the sessile drop method was employed to determine the contact angle, the parameter that measures the degree of wettability. The results of variation in the contact angle as a function of temperature were plotted in graphic form which showed that the curves displayed a fast decline and good spreading. All the samples of the two systems presented final contact angles of 40o to 10o indicating their good wetting on SiC in the argon atmosphere. The melted/solidified area and interface between SiC and melted/solidified phase were evaluated by scanning electron microscopy （SEM） and their crystalline phases were identified by X-ray diffraction （DRX）. The DRX analysis showed that Al2O3 and RE2O3 reacted and formed the Dy3Al5O12 （DyAg） and Yb3Al5O12 （YbAg） phases. The results indicated that the two systems had a promising potential as additives for the sintering of SiC ceramics.
基金supported by an INRIA internal financial support:ADT SENSBIO and a Montpellier Hospital internal financial support(AOI PARKDEMAR CHU Montpellier).
文摘As low cost and highly portable sensors, inertial measurements units (IMU) have become increas-ingly used in gait analysis, embodying an efficient alternative to motion capture systems. Mean-while, being able to compute reliably accurate spatial gait parameters using few sensors remains a relatively complex problematic. Providing a clinical oriented solution, our study presents a gy-rometer and accelerometer based algorithm for stride length estimation. Compared to most of the numerous existing works where only an averaged stride length is computed from several IMU, or where the use of the magnetometer is incompatible with everyday use, our challenge here has been to extract each individual stride length in an easy-to-use algorithm requiring only one inertial sensor attached to the subject shank. Our results were validated on healthy subjects and patients suffering from Parkinson’s disease (PD). Estimated stride lengths were compared to GAITRite? walkway system data: the mean error over all the strides was less than 6% for healthy group and 10.3% for PD group. This method provides a reliable portable solution for monitoring the in-stantaneous stride length and opens the way to promising applications.
