A carbon wire amperometric flow through detector is described which is easily constructed at low cost for application to flow injection analysis,continuous stream analysis and liquid chromatography.The theoretical lim...A carbon wire amperometric flow through detector is described which is easily constructed at low cost for application to flow injection analysis,continuous stream analysis and liquid chromatography.The theoretical limiting current of the detector is 2.14×10~6nCD^(2/3)u_f^(1/3) with 36% actual current efficiency.By use of flow injection analysis,the detecting limits for Ag(I)and Cr(VI)had achieved 1 ppb and 0.4 ppb respectively with 1.2%(n=20)relative standard deviation after preliminary experiments.展开更多
The giant magneto-impedance（GMI）effect of amorphous wire was analyzed theoretically.The amorphous wire had strong GMI effect in the stimulation of sharp pulse of 680kHz and18 mV.A pulse generator was designed to pro...The giant magneto-impedance（GMI）effect of amorphous wire was analyzed theoretically.The amorphous wire had strong GMI effect in the stimulation of sharp pulse of 680kHz and18 mV.A pulse generator was designed to provide high frequency pulse to a magnetic impedance（MI）element.The induced voltage on the pickup coil wound on the amorphous wire was sampled and held with a detect circuit using analog switch.A stable magnetic sensor was constructed.A three-dimension micro magnetic field detector was designed with a central controller MSP430F449.High stability and sensitivity were obtained in the MI sensor with the detect circuit.Experiment results showed that the resolution of the detector was 1nT in the full scale of±2 Oe and the detector worked stably from the room temperature to about 80℃.A small ferromagnetic target was detected by the three-dimension detector in laboratory environment without magnetic shielding.The target moving direction was ascertained with the wave shape of axis parallel in that direction.展开更多
为有效实现数字射线扫描成像检测系统性能的定量分析评价,据此进行检测工艺参数的优化,对数字射线扫描成像检测系统调制传递函数(Modulation transfer function,MTF)进行了测试分析。采用刀口工具、双线型像质计、分辨率测试卡,对系统...为有效实现数字射线扫描成像检测系统性能的定量分析评价,据此进行检测工艺参数的优化,对数字射线扫描成像检测系统调制传递函数(Modulation transfer function,MTF)进行了测试分析。采用刀口工具、双线型像质计、分辨率测试卡,对系统在不同焦点大小、放大倍数、运动方向的检测情况,分别进行了MTF的测试并进行了比较。结果表明,双线型像质计与分辨率测试卡的测试结果基本一致,但双线型像质计更便于对比度的定量计算;双线型像质计的对比度传递函数近似符合二次曲线,经转换得到的调制传递函数值高于刀口法的测试值,刀口法计算数值偏低的原因在于运动不平稳所带来的不利影响。分析表明,数字射线扫描成像系统性能受到多个因素的共同影响,MTF测试结果可较全面地对影响因素进行定量评价,可用于确定最佳的检测参数或找出等价的参数组合。展开更多
基金This Project is supported by the National Science Foundation of China
文摘A carbon wire amperometric flow through detector is described which is easily constructed at low cost for application to flow injection analysis,continuous stream analysis and liquid chromatography.The theoretical limiting current of the detector is 2.14×10~6nCD^(2/3)u_f^(1/3) with 36% actual current efficiency.By use of flow injection analysis,the detecting limits for Ag(I)and Cr(VI)had achieved 1 ppb and 0.4 ppb respectively with 1.2%(n=20)relative standard deviation after preliminary experiments.
基金Supported by the National Natural Science Foundation of China(60874100)
文摘The giant magneto-impedance（GMI）effect of amorphous wire was analyzed theoretically.The amorphous wire had strong GMI effect in the stimulation of sharp pulse of 680kHz and18 mV.A pulse generator was designed to provide high frequency pulse to a magnetic impedance（MI）element.The induced voltage on the pickup coil wound on the amorphous wire was sampled and held with a detect circuit using analog switch.A stable magnetic sensor was constructed.A three-dimension micro magnetic field detector was designed with a central controller MSP430F449.High stability and sensitivity were obtained in the MI sensor with the detect circuit.Experiment results showed that the resolution of the detector was 1nT in the full scale of±2 Oe and the detector worked stably from the room temperature to about 80℃.A small ferromagnetic target was detected by the three-dimension detector in laboratory environment without magnetic shielding.The target moving direction was ascertained with the wave shape of axis parallel in that direction.
文摘为有效实现数字射线扫描成像检测系统性能的定量分析评价,据此进行检测工艺参数的优化,对数字射线扫描成像检测系统调制传递函数(Modulation transfer function,MTF)进行了测试分析。采用刀口工具、双线型像质计、分辨率测试卡,对系统在不同焦点大小、放大倍数、运动方向的检测情况,分别进行了MTF的测试并进行了比较。结果表明,双线型像质计与分辨率测试卡的测试结果基本一致,但双线型像质计更便于对比度的定量计算;双线型像质计的对比度传递函数近似符合二次曲线,经转换得到的调制传递函数值高于刀口法的测试值,刀口法计算数值偏低的原因在于运动不平稳所带来的不利影响。分析表明,数字射线扫描成像系统性能受到多个因素的共同影响,MTF测试结果可较全面地对影响因素进行定量评价,可用于确定最佳的检测参数或找出等价的参数组合。
