The in-flight heating process of cerium dioxide(CeO_(2))powders was investigated through experiments and numerical simulations.In the experiment,CeO_(2)powder(average size of 30μm)was injected into radio-frequency(RF...The in-flight heating process of cerium dioxide(CeO_(2))powders was investigated through experiments and numerical simulations.In the experiment,CeO_(2)powder(average size of 30μm)was injected into radio-frequency(RF)argon plasma,and the temperatures were measured using a DPV-2000 monitor.A model combining the electromagnetism,thermal flow,and heat transfer characteristics of powder during in-flight heating in argon plasma was proposed.The melting processes of CeO_(2)powders of different diameters,with and without thermal resistance effect,were investigated.Results show that the heating process of CeO_(2)powder particles consists of three main stages,one of which is relevant to a dimensionless parameter known as the Biot number.When the Biot value≥0.1,thermal resistance increases significantly,especially for the larger powders.The predicted temperature of the particles at the outlet(1800–2880 K)is in good agreement with the experimental result.展开更多
Two-step-processed(TSP)inverted p-i-n perovskite solar cells(PSCs)have demonstrated significant promise in tandem applications.However,the power conversion efficiency(PCE)of TSP p-i-n PSCs rarely exceeds 24%.Here,we d...Two-step-processed(TSP)inverted p-i-n perovskite solar cells(PSCs)have demonstrated significant promise in tandem applications.However,the power conversion efficiency(PCE)of TSP p-i-n PSCs rarely exceeds 24%.Here,we demonstrate that TSP perovskite films exhibit a vertically gradient distribution of residual PbI_(2)clusters,which form Schottky heterojunctions with the perovskite,leading to substantial interfacial energy-level mismatches within NiO_(x)-based TSP p-i-n PSCs.These limitations were effectively addressed via a vertical interfacial engineering enabled by dual-interface modification incorporating tin trifluoromethanesulfonate(Sn(OTF)_(2))and 4-Fluorophenylethylamine chloride(F-PEA)at the NiO_(x)/perovskite and perovskite/C60 interfaces,respectively.The functional Sn(OTF)_(2)not only enhances the conductivity of NiO_(x)films but also suppresses ion migration,while inducing the formation of a Pb-Sn mixed perovskite interlayer that precisely regulates the energy level at the NiO_(x)/perovskite interface.Complementally,F-PEA post-treatment effectively converts surface residual PbI_(2)clusters into a 2D perovskite capping layer,which simultaneously passivates surface defects and enhances energy-level alignment at the perovskite/C60 interface.Consequently,the optimized NiO_(x)-based TSP p-i-n PSCs achieve a notable PCE of 25.6%with superior operational stability.This study elucidates the underlying mechanisms limiting the efficiency of TSP p-i-n PSCs,while establishing design principles for these devices targeting 26%efficiency.展开更多
During the production of Ti-bearing Al-killed ultra-low-carbon(ULC) steel, two different heating processes were used when the converter tapping temperature or the molten steel temperature in the Ruhrstahl–Heraeus(RH)...During the production of Ti-bearing Al-killed ultra-low-carbon(ULC) steel, two different heating processes were used when the converter tapping temperature or the molten steel temperature in the Ruhrstahl–Heraeus(RH) process was low: heating by Al addition during the RH decarburization process and final deoxidation at the end of the RH decarburization process(process-Ⅰ), and increasing the oxygen content at the end of RH decarburization, heating and final deoxidation by one-time Al addition(process-Ⅱ). Temperature increases of 10°C by different processes were studied; the results showed that the two heating processes could achieve the same heating effect. The T.[O] content in the slab and the refining process was better controlled by process-Ⅰ than by process-Ⅱ. Statistical analysis of inclusions showed that the numbers of inclusions in the slab obtained by process-Ⅰ were substantially less than those in the slab obtained by process-Ⅱ. For process-Ⅰ, the Al_2O_3 inclusions produced by Al added to induce heating were substantially removed at the end of decarburization. The amounts of inclusions were substantially greater for process-Ⅱ than for process-Ⅰ at different refining stages because of the higher dissolved oxygen concentration in process-Ⅱ. Industrial test results showed that process-Ⅰ was more beneficial for improving the cleanliness of molten steel.展开更多
A mathematical model of the particle heating process in the reaction shaft of flash smelting furnace was established and the calculation was performed.The results indicate that radiation plays a significant role in th...A mathematical model of the particle heating process in the reaction shaft of flash smelting furnace was established and the calculation was performed.The results indicate that radiation plays a significant role in the heat transfer process within the first 0.6 m in the upper part of the reaction shaft,whilst the convection is dominant in the area below 0.6 m for the particle heating.In order to accelerate the particle ignition,it is necessary to enhance the convection,thus to speed up the particle heating.A high-speed preheated oxygen jet technology was then suggested to replace the nature gas combustion in the flash furnace,aiming to create a lateral disturbance in the gaseous phase around the particles,so as to achieve a slip velocity between the two phases and a high convective heat transfer coefficient.Numerical simulation was carried out for the cases with the high-speed oxygen jet and the normal nature gas burners.The results show that with the high-speed jet technology,particles are heated up more rapidly and ignited much earlier,especially within the area of the radial range of R=0.3−0.6 m.As a result,a more efficient smelting process can be achieved under the same operational condition.展开更多
Ultrafast heating(UFH)at the rates of 10-300℃/s was employed as a new strategy to anneal a coldrolled 7 wt%Mn steel,followed by the immediate cooling.Severely deformed strain-induced martensite and lightly-deformed t...Ultrafast heating(UFH)at the rates of 10-300℃/s was employed as a new strategy to anneal a coldrolled 7 wt%Mn steel,followed by the immediate cooling.Severely deformed strain-induced martensite and lightly-deformed thermal martensite,both had been already enriched with C and Mn before,transformed to fine and coarse austenite grains during the UFH,leading to the bimodal size distribution.Compared with the long intercritical annealing(IA)process,the UFH processes produced larger fraction of RA grains(up to 37%)with a high density of dislocation,leading to the significant increase in yield strength by 270 MPa and the product of strength and elongation up to 55 GPa%due to the enormous work hardening capacity.Such a significant strengthening is first attributed to high density dislocations preserved after UFH and then to the microstructural refinement and the precipitation strengthening;whilst the sustainable work hardening is attributed to the successive TRIP effect during deformation,resulting from the large fraction of RA instantly formed with the bimodal size distribution during UFH.Moreover,the results on the microstructural characterization,thermodynamics calculation on the reverse transformation temperature and the kinetic simulations on the reverse transformation all suggest that the austenitization during UFH is displacive and involves the diffusion and partition of C.Therefore,we propose that it is a bainite-like transformation.展开更多
The exothermic efficiency of microwave heating an electrolyte/water solution is remarkably high due to the dielectric heating by orientation polarization of water and resistance heating by the Joule process occurred s...The exothermic efficiency of microwave heating an electrolyte/water solution is remarkably high due to the dielectric heating by orientation polarization of water and resistance heating by the Joule process occurred simultaneously compared with pure water.A three-dimensional finite element numerical model of multi-feed microwave heating industrial liquids continuously flowing in a meter-scale circular tube is presented.The temperature field inside the applicator tube in the cavity is solved by COMSOL Multiphysics and professional programming to describe the momentum,energy and Maxwell's equations.The evaluations of the electromagnetic field,the temperature distribution and the velocity field are simulated for the fluids dynamically heated by singleand multi-feed microwave system,respectively.Both the pilot experimental investigations and numerical results of microwave with single-feed heating for fluids with different effective permittivity and flow rates show that the presented numerical modeling makes it possible to analyze dynamic process of multi-feed microwave heating the industrial liquid.The study aids in enhancing the understanding and optimizing of dynamic process in the use of multi-feed microwave heating industrial continuous flow for a variety of material properties and technical parameters.展开更多
This paper focuses on the process for pillow shape plate by line heating technique, which is widely applied in the production of ship hull. Based on the analysis of primary parameters and experimental data in line hea...This paper focuses on the process for pillow shape plate by line heating technique, which is widely applied in the production of ship hull. Based on the analysis of primary parameters and experimental data in line heating process, the amount of local contraction generated by line heating has been illustrated. Then, combining with the computational result of local deformation determined by shell plate development, an optimization method for line heating parameters has been studied. This prediction system may provide rational arrangements of heating lines and technical parameters of process. By integrating the prediction system into the line heating robot for pillow shape plate, the automatic process of line heating for pillow shape plate can be achieved.展开更多
The microstructural changes of Fe83Si4B13 amorphous mother alloy during the heating process were investigated by Laser Scanning Confocal Microscopy （LSCM） ,and the phase transformation was determined by the Thermo-C...The microstructural changes of Fe83Si4B13 amorphous mother alloy during the heating process were investigated by Laser Scanning Confocal Microscopy （LSCM） ,and the phase transformation was determined by the Thermo-Calc calculations. The differences in the melting points measured by Differential Scanning Calorimetry （DSC） and LSCM, and those obtained by Thermo-Calc calculations were also discussed. It is found that the melting points measured by DSC and LSCM are relatively similar, whereas the onset and end of the melting temperatures calculated by Thermo-Calc software are higher than those measured by DSC and observed by LSCM.展开更多
To overcome the shortage of complex equipment,large volume,and high energy consumption in space capsule manufacturing,a novel sliding pressure Joule heat fuse additive manufacturing technique with reduced volume and l...To overcome the shortage of complex equipment,large volume,and high energy consumption in space capsule manufacturing,a novel sliding pressure Joule heat fuse additive manufacturing technique with reduced volume and low energy consumption was proposed.But the unreasonable process parameters may lead to the inferior consistency of the forming quality of single-channel multilayer in Joule heat additive manufacturing process,and it is difficult to reach the condition for forming thinwalled parts.Orthogonal experiments were designed to fabricate single-channel multilayer samples with varying numbers of layers,and their forming quality was evaluated.The influence of printing current,forming speed,and contact pressure on the forming quality of the single-channel multilayer was analyzed.The optimal process parameters were obtained and the quality characterization of the experiment results was conducted.Results show that the printing current has the most significant influence on the forming quality of the single-channel multilayer.Under the optimal process parameters,the forming section is well fused and the surface is continuously smooth.The surface roughness of a single-channel 3-layer sample is 0.16μm,and the average Vickers hardness of cross section fusion zone is 317 HV,which lays a foundation for the subsequent use of Joule heat additive manufacturing technique to form thinwall parts.展开更多
In the anticorrosive coating line of a welded tube plant, the current status and existing problems of the medium-frequency induction heating equipment were discussed.Partial renovations of the power control cabinet ha...In the anticorrosive coating line of a welded tube plant, the current status and existing problems of the medium-frequency induction heating equipment were discussed.Partial renovations of the power control cabinet have been conducted.Parameters such as the DC current, DC voltage, intermediate frequency power, heating temperature, and the positioning signal at the pipe end were collected.A data acquisition and processing system, which can process data according to user needs and provide convenient data processing functions, has been developed using LabVIEW software.This system has been successfully applied in the coating line for the automatic control of high-power induction heating equipment, production management, and digital steel tube and/or digital delivery.展开更多
Induction heating has important applications in science and industry. The method of induction heating can be successfully used for melting and heat treatment of titanium and zirconium alloys. Different applications us...Induction heating has important applications in science and industry. The method of induction heating can be successfully used for melting and heat treatment of titanium and zirconium alloys. Different applications using induction precise heating before plastic deformation are discussed in this paper. For alloys of many metals such as titanium, zirconium, niobium, tantalum, etc., it is important to provide precision heating with a high degree of homogeneity of the temperature field and strict adherence to the condition of heating. This is explained by polymorphism of the alloys based on these metals, their chemical activity at high temperatures and the specific thermal and electrical properties. It is very important for induction heating to define the extreme achievable unevenness of the temperature field. For special alloys it is necessary to use resistance furnaces for homogenization of billets’ temperature after heating in the inductors. Optimal control can be used for massive billets to reduce significantly the heating time, energy expenses and to improve the quality of the temperature field distribution. Optimization of induction heating process can be achieved by synchronous solution of the problem of optimal control and design with specially developed models.展开更多
Ground-state cooling of mesoscopic mechanical objects is still a major challenge in the unresolved-sideband regime.We present a frequency modulation(FM)scheme to achieve cooling of the mechanical resonator to its grou...Ground-state cooling of mesoscopic mechanical objects is still a major challenge in the unresolved-sideband regime.We present a frequency modulation(FM)scheme to achieve cooling of the mechanical resonator to its ground-state in a double-cavity optomechanical system containing a mechanical resonator.The mean phonon number is determined by numerically solving a set of differential equations derived from the quantum master equations.Due to efficient suppression of Stokes heating processes in the presence of FM,the ground-state cooling,indicated by numerical calculations,is significantly achievable,regardless of whether in the resolved-sideband regime or the unresolved-sideband regime.Furthermore,by choosing parameters reasonably,the improvement of the quantum cooling limit is found to be capable of being positively correlated with the modulation frequency.This method provides new insight into quantum manipulation and creates more possibilities for applications of quantum devices.展开更多
Three-dimensional thermal a nalysis simulation of a horizontal zone refining system is conducted for germanimn semiconductor materials. The considered geometry includes a g＇ral）hite boat filled with germanium placed...Three-dimensional thermal a nalysis simulation of a horizontal zone refining system is conducted for germanimn semiconductor materials. The considered geometry includes a g＇ral）hite boat filled with germanium placed in a cylindrical quartz tube. A flow of Ar and H2 gas mixture is purged througll the tube. A narrow section of the, boat is assmned to be exposed to a constant heat rate produced b v an rf coil located outside the quartz tube. The results of this analysis provide essential information about various parameters such as the shape of tile molten zone, required power and temperature gradient in the system.展开更多
In-situ HVEM observation on phase transition of the YBa_2Cu_3O_(7-x) superconducting compound in pro- cess of heating was carried out,and high temperature X-ray diffraction analysis in air and X-ray diffraction phase ...In-situ HVEM observation on phase transition of the YBa_2Cu_3O_(7-x) superconducting compound in pro- cess of heating was carried out,and high temperature X-ray diffraction analysis in air and X-ray diffraction phase analysis for the sample treated in vacuum condition were made.The results showed that the temperature of phase transition is related to oxygen content in the sample and in general,is 100℃ to 120℃ lower in vacu- um condition than in air.At 320℃ to 350℃ twin bands begin to disappear,and some Cu_2O are formed on the surface of the sample and transit from orthorhombic YBa_2Cu_3O_(7-x) to arthorhombic Y_2BaCuO_5 compound. This transition was completed at about 500℃.Above 900℃,this compound consists of the Y_2BaCuO_5, BaCuO_2,Y_2O_3 and some other minor compounds.No phase transition was observed during cooling the sample.展开更多
2195 aluminum-lithium alloy was widely applied in the aviation and aerospace industry, but it is highly susceptible to pitting and intergranular corrosion undergoing sever corrosive circumstance and moisture atmospher...2195 aluminum-lithium alloy was widely applied in the aviation and aerospace industry, but it is highly susceptible to pitting and intergranular corrosion undergoing sever corrosive circumstance and moisture atmosphere. To solve this problem and consequently to prolong its service life, a multi-step-heating-rate(MSRC) process was carried out. Investigations were carried out to find the effect of the MSRC process on the alloys corrosion resistance. It is found that the MSRC process is more favorable for the uniform phase precipitation by comparing the corrosion resistance of samples treated by traditional heat treatments. The potential difference between phases can be reduced and intergranular corrosion is able to be prohibited efficiently. Besides, the rare earth infiltration is beneficial to improving the corrosion resistance. As heating time increases, the corrosion resistance declines gradually, samples treated by artificial aging and solid solution also exhibit a better corrosion resistance.展开更多
Sand mold 3D printing technology has been recognized as a digital,high-quality,and promising sand mold forming method.However,sand mold 3D printing technology has drawbacks,such as single molding material and long cur...Sand mold 3D printing technology has been recognized as a digital,high-quality,and promising sand mold forming method.However,sand mold 3D printing technology has drawbacks,such as single molding material and long curing time,which limit its further industrial application.Therefore,this study proposes a method for forming composite sand molds based on a layer-stacking structure and a strengthening method based on interlayer heating.The influence of the process parameters on the properties of traditional and composite sand molds was systematically studied.Experimental results demonstrated that when the heating temperature was 150℃,the enhancement of the sand mold was obvious,with an increase of approximately 20%compared to untreated sand mold.When the composite sand mold with a laminated thickness of 1.5 mm was heated at this temperature,its tensile strength reached 1.53 MPa,and compressive strength reached 5.80 MPa,which met the casting requirements.The composite sand mold printed by interlayer heating has excellent casting performance and economic advantages,which provide theoretical guidance for the high-performance printing of sand molds.展开更多
In this study, a two-step heating process is introduced for transient liquid phase ( TLP) diffusion bonding fo r sound joints with T91 heat resistant steels. At first, a short-time higher temperature heating ...In this study, a two-step heating process is introduced for transient liquid phase ( TLP) diffusion bonding fo r sound joints with T91 heat resistant steels. At first, a short-time higher temperature heating step is addressed to melt the interlayer, followed by the second step to complete isothermal solidification at a low temperature. The most critical feature of our new method is producing a non-planar interface at the T9/ heat resistant steels joint. We propose a transitional liquid phase bonding of T91 heat resistant steels by this approach. Since joint microstructures have been studied, we tested the tensile strength to assess joint mechanical property. The result indicates that the solidified bond may contain a primary solid-solution, similar composition to the parent metal and free from precipitates. Joint tensile strength of the joint is not lower than parent materials. Joint bend's strengths are enhanced due to the higher metal-to-metal junction producing a non-planar bond lines. Nevertheless, the traditional transient liquid phase diffusion bonding produces planar ones. Bonding parameters of new process are 1 260 °C for 0. 5 min and 1 230 °C fo r 4 min.展开更多
Based on the theory of thermal conductivity, in this paper we derived a formula to estimate the prolongation period （AtL） of cooling-crystallization process of a granitic melt caused by latent heat of crystallizatio...Based on the theory of thermal conductivity, in this paper we derived a formula to estimate the prolongation period （AtL） of cooling-crystallization process of a granitic melt caused by latent heat of crystallization as follows：△tL=QL×△tcol/（TM-TC）×CP where TM is initial temperature of the granite melt, Tc crystallization temperature of the granite melt, Cp specific heat, △tcol cooling period of a granite melt from its initial temperature （TM） to its crystallization temperature （Tc）, QL latent heat of the granite melt. The cooling period of the melt for the Fanshan granodiorite from its initial temperature （900℃） to crystallization temperature （600℃） could be estimated -210,000 years if latent heat was not considered. Calculation for the Fanshan melt using the above formula yields a AtL value of -190,000 years, which implies that the actual cooling period within the temperature range of 900°-600℃ should be 400,000 years. This demonstrates that the latent heat produced from crystallization of the granitic melt is a key factor influencing the cooling-crystallization process of a granitic melt, prolongating the period of crystallization and resulting in the large emplacement-crystallization time difference （ECTD） in granite batholith.展开更多
AA5083 friction stir welds were produced using systematic experimental design, the process forces and heat input with varying parameters were studied. Helpful empirical models were developed in designing friction stir...AA5083 friction stir welds were produced using systematic experimental design, the process forces and heat input with varying parameters were studied. Helpful empirical models were developed in designing friction stir welding （FSW） tools and FSW welders. These models may be further helpful for making process parameter choice for this sort of alloy, defining welding program and control of process parameters by using computer numerical control friction stir welding welders. The results show that tool rotational speed, welding speed and tool shoulder diameter are most significant parameters affecting axial force and heat input, while longitudinal force is significantly affected by welding speed and probe diameter.展开更多
基金National Natural Science Foundation of China(11875039)Shanxi Scholarship Council of China(2023-033)+2 种基金Fundamental Research Program of Shanxi Province(202303021221071)China Baowu Low Carbon Metallurgical Innovation Foundation(2022)2023 Anhui Major Industrial Innovation Plan Project。
文摘The in-flight heating process of cerium dioxide(CeO_(2))powders was investigated through experiments and numerical simulations.In the experiment,CeO_(2)powder(average size of 30μm)was injected into radio-frequency(RF)argon plasma,and the temperatures were measured using a DPV-2000 monitor.A model combining the electromagnetism,thermal flow,and heat transfer characteristics of powder during in-flight heating in argon plasma was proposed.The melting processes of CeO_(2)powders of different diameters,with and without thermal resistance effect,were investigated.Results show that the heating process of CeO_(2)powder particles consists of three main stages,one of which is relevant to a dimensionless parameter known as the Biot number.When the Biot value≥0.1,thermal resistance increases significantly,especially for the larger powders.The predicted temperature of the particles at the outlet(1800–2880 K)is in good agreement with the experimental result.
基金supported by the National Nature Science Foundation of China(62504130)National Key Research and Development Program of China(2018YFB0704100)+1 种基金the Key university laboratory of highly efficient utilization of solar energy and sustainable development of Guangdong(Y01256331)the Technology Development Project of Henan Province(252102240047).
文摘Two-step-processed(TSP)inverted p-i-n perovskite solar cells(PSCs)have demonstrated significant promise in tandem applications.However,the power conversion efficiency(PCE)of TSP p-i-n PSCs rarely exceeds 24%.Here,we demonstrate that TSP perovskite films exhibit a vertically gradient distribution of residual PbI_(2)clusters,which form Schottky heterojunctions with the perovskite,leading to substantial interfacial energy-level mismatches within NiO_(x)-based TSP p-i-n PSCs.These limitations were effectively addressed via a vertical interfacial engineering enabled by dual-interface modification incorporating tin trifluoromethanesulfonate(Sn(OTF)_(2))and 4-Fluorophenylethylamine chloride(F-PEA)at the NiO_(x)/perovskite and perovskite/C60 interfaces,respectively.The functional Sn(OTF)_(2)not only enhances the conductivity of NiO_(x)films but also suppresses ion migration,while inducing the formation of a Pb-Sn mixed perovskite interlayer that precisely regulates the energy level at the NiO_(x)/perovskite interface.Complementally,F-PEA post-treatment effectively converts surface residual PbI_(2)clusters into a 2D perovskite capping layer,which simultaneously passivates surface defects and enhances energy-level alignment at the perovskite/C60 interface.Consequently,the optimized NiO_(x)-based TSP p-i-n PSCs achieve a notable PCE of 25.6%with superior operational stability.This study elucidates the underlying mechanisms limiting the efficiency of TSP p-i-n PSCs,while establishing design principles for these devices targeting 26%efficiency.
基金financially supported by the National Natural Science Foundation of China (No.51404022)
文摘During the production of Ti-bearing Al-killed ultra-low-carbon(ULC) steel, two different heating processes were used when the converter tapping temperature or the molten steel temperature in the Ruhrstahl–Heraeus(RH) process was low: heating by Al addition during the RH decarburization process and final deoxidation at the end of the RH decarburization process(process-Ⅰ), and increasing the oxygen content at the end of RH decarburization, heating and final deoxidation by one-time Al addition(process-Ⅱ). Temperature increases of 10°C by different processes were studied; the results showed that the two heating processes could achieve the same heating effect. The T.[O] content in the slab and the refining process was better controlled by process-Ⅰ than by process-Ⅱ. Statistical analysis of inclusions showed that the numbers of inclusions in the slab obtained by process-Ⅰ were substantially less than those in the slab obtained by process-Ⅱ. For process-Ⅰ, the Al_2O_3 inclusions produced by Al added to induce heating were substantially removed at the end of decarburization. The amounts of inclusions were substantially greater for process-Ⅱ than for process-Ⅰ at different refining stages because of the higher dissolved oxygen concentration in process-Ⅱ. Industrial test results showed that process-Ⅰ was more beneficial for improving the cleanliness of molten steel.
基金funded by Jinguan Copper of Tongling Non-ferrous Metals Group Co., Ltd.
文摘A mathematical model of the particle heating process in the reaction shaft of flash smelting furnace was established and the calculation was performed.The results indicate that radiation plays a significant role in the heat transfer process within the first 0.6 m in the upper part of the reaction shaft,whilst the convection is dominant in the area below 0.6 m for the particle heating.In order to accelerate the particle ignition,it is necessary to enhance the convection,thus to speed up the particle heating.A high-speed preheated oxygen jet technology was then suggested to replace the nature gas combustion in the flash furnace,aiming to create a lateral disturbance in the gaseous phase around the particles,so as to achieve a slip velocity between the two phases and a high convective heat transfer coefficient.Numerical simulation was carried out for the cases with the high-speed oxygen jet and the normal nature gas burners.The results show that with the high-speed jet technology,particles are heated up more rapidly and ignited much earlier,especially within the area of the radial range of R=0.3−0.6 m.As a result,a more efficient smelting process can be achieved under the same operational condition.
基金financial support from National Natural Science Foundation of China[Nos.51831002 and 51861135302]the Fundamental Research Funds for the Central Universities(No.FRF-TP-18-002C2)。
文摘Ultrafast heating(UFH)at the rates of 10-300℃/s was employed as a new strategy to anneal a coldrolled 7 wt%Mn steel,followed by the immediate cooling.Severely deformed strain-induced martensite and lightly-deformed thermal martensite,both had been already enriched with C and Mn before,transformed to fine and coarse austenite grains during the UFH,leading to the bimodal size distribution.Compared with the long intercritical annealing(IA)process,the UFH processes produced larger fraction of RA grains(up to 37%)with a high density of dislocation,leading to the significant increase in yield strength by 270 MPa and the product of strength and elongation up to 55 GPa%due to the enormous work hardening capacity.Such a significant strengthening is first attributed to high density dislocations preserved after UFH and then to the microstructural refinement and the precipitation strengthening;whilst the sustainable work hardening is attributed to the successive TRIP effect during deformation,resulting from the large fraction of RA instantly formed with the bimodal size distribution during UFH.Moreover,the results on the microstructural characterization,thermodynamics calculation on the reverse transformation temperature and the kinetic simulations on the reverse transformation all suggest that the austenitization during UFH is displacive and involves the diffusion and partition of C.Therefore,we propose that it is a bainite-like transformation.
基金Project(KKSY201503006)supported by Scientific Research Foundation of Kunming University of Science and Technology,ChinaProject(2014FD009)supported by the Applied Basic Research Foundation(Youth Program)of ChinaProject(51090385)supported by the National Natural Science Foundation of China
文摘The exothermic efficiency of microwave heating an electrolyte/water solution is remarkably high due to the dielectric heating by orientation polarization of water and resistance heating by the Joule process occurred simultaneously compared with pure water.A three-dimensional finite element numerical model of multi-feed microwave heating industrial liquids continuously flowing in a meter-scale circular tube is presented.The temperature field inside the applicator tube in the cavity is solved by COMSOL Multiphysics and professional programming to describe the momentum,energy and Maxwell's equations.The evaluations of the electromagnetic field,the temperature distribution and the velocity field are simulated for the fluids dynamically heated by singleand multi-feed microwave system,respectively.Both the pilot experimental investigations and numerical results of microwave with single-feed heating for fluids with different effective permittivity and flow rates show that the presented numerical modeling makes it possible to analyze dynamic process of multi-feed microwave heating the industrial liquid.The study aids in enhancing the understanding and optimizing of dynamic process in the use of multi-feed microwave heating industrial continuous flow for a variety of material properties and technical parameters.
文摘This paper focuses on the process for pillow shape plate by line heating technique, which is widely applied in the production of ship hull. Based on the analysis of primary parameters and experimental data in line heating process, the amount of local contraction generated by line heating has been illustrated. Then, combining with the computational result of local deformation determined by shell plate development, an optimization method for line heating parameters has been studied. This prediction system may provide rational arrangements of heating lines and technical parameters of process. By integrating the prediction system into the line heating robot for pillow shape plate, the automatic process of line heating for pillow shape plate can be achieved.
文摘The microstructural changes of Fe83Si4B13 amorphous mother alloy during the heating process were investigated by Laser Scanning Confocal Microscopy （LSCM） ,and the phase transformation was determined by the Thermo-Calc calculations. The differences in the melting points measured by Differential Scanning Calorimetry （DSC） and LSCM, and those obtained by Thermo-Calc calculations were also discussed. It is found that the melting points measured by DSC and LSCM are relatively similar, whereas the onset and end of the melting temperatures calculated by Thermo-Calc software are higher than those measured by DSC and observed by LSCM.
基金Shaanxi Province Qin Chuangyuan“Scientist+Engineer”Team Construction Project(2022KXJ-071)2022 Qin Chuangyuan Achievement Transformation Incubation Capacity Improvement Project(2022JH-ZHFHTS-0012)+1 种基金Shaanxi Province Key Research and Development Plan-“Two Chains”Integration Key Project-Qin Chuangyuan General Window Industrial Cluster Project(2023QCY-LL-02)Xixian New Area Science and Technology Plan(2022-YXYJ-003,2022-XXCY-010)。
文摘To overcome the shortage of complex equipment,large volume,and high energy consumption in space capsule manufacturing,a novel sliding pressure Joule heat fuse additive manufacturing technique with reduced volume and low energy consumption was proposed.But the unreasonable process parameters may lead to the inferior consistency of the forming quality of single-channel multilayer in Joule heat additive manufacturing process,and it is difficult to reach the condition for forming thinwalled parts.Orthogonal experiments were designed to fabricate single-channel multilayer samples with varying numbers of layers,and their forming quality was evaluated.The influence of printing current,forming speed,and contact pressure on the forming quality of the single-channel multilayer was analyzed.The optimal process parameters were obtained and the quality characterization of the experiment results was conducted.Results show that the printing current has the most significant influence on the forming quality of the single-channel multilayer.Under the optimal process parameters,the forming section is well fused and the surface is continuously smooth.The surface roughness of a single-channel 3-layer sample is 0.16μm,and the average Vickers hardness of cross section fusion zone is 317 HV,which lays a foundation for the subsequent use of Joule heat additive manufacturing technique to form thinwall parts.
文摘In the anticorrosive coating line of a welded tube plant, the current status and existing problems of the medium-frequency induction heating equipment were discussed.Partial renovations of the power control cabinet have been conducted.Parameters such as the DC current, DC voltage, intermediate frequency power, heating temperature, and the positioning signal at the pipe end were collected.A data acquisition and processing system, which can process data according to user needs and provide convenient data processing functions, has been developed using LabVIEW software.This system has been successfully applied in the coating line for the automatic control of high-power induction heating equipment, production management, and digital steel tube and/or digital delivery.
文摘Induction heating has important applications in science and industry. The method of induction heating can be successfully used for melting and heat treatment of titanium and zirconium alloys. Different applications using induction precise heating before plastic deformation are discussed in this paper. For alloys of many metals such as titanium, zirconium, niobium, tantalum, etc., it is important to provide precision heating with a high degree of homogeneity of the temperature field and strict adherence to the condition of heating. This is explained by polymorphism of the alloys based on these metals, their chemical activity at high temperatures and the specific thermal and electrical properties. It is very important for induction heating to define the extreme achievable unevenness of the temperature field. For special alloys it is necessary to use resistance furnaces for homogenization of billets’ temperature after heating in the inductors. Optimal control can be used for massive billets to reduce significantly the heating time, energy expenses and to improve the quality of the temperature field distribution. Optimization of induction heating process can be achieved by synchronous solution of the problem of optimal control and design with specially developed models.
基金supported by the National Natural Science Foundation of China(Grant No.62061028)the Foundation for Distinguished Young Scientists of Jiangxi Province(Grant No.20162BCB23009)+2 种基金the Open Research Fund Program of the State Key Laboratory of Low-Dimensional Quantum Physics(Grant No.KF202010)the Interdisciplinary Innovation Fund of Nanchang University(Grant No.9166-27060003-YB12)the Open Research Fund Program of Key Laboratory of Opto-Electronic Information Acquisition and Manipulation of Ministry of Education(Grant No.OEIAM202004)。
文摘Ground-state cooling of mesoscopic mechanical objects is still a major challenge in the unresolved-sideband regime.We present a frequency modulation(FM)scheme to achieve cooling of the mechanical resonator to its ground-state in a double-cavity optomechanical system containing a mechanical resonator.The mean phonon number is determined by numerically solving a set of differential equations derived from the quantum master equations.Due to efficient suppression of Stokes heating processes in the presence of FM,the ground-state cooling,indicated by numerical calculations,is significantly achievable,regardless of whether in the resolved-sideband regime or the unresolved-sideband regime.Furthermore,by choosing parameters reasonably,the improvement of the quantum cooling limit is found to be capable of being positively correlated with the modulation frequency.This method provides new insight into quantum manipulation and creates more possibilities for applications of quantum devices.
文摘Three-dimensional thermal a nalysis simulation of a horizontal zone refining system is conducted for germanimn semiconductor materials. The considered geometry includes a g＇ral）hite boat filled with germanium placed in a cylindrical quartz tube. A flow of Ar and H2 gas mixture is purged througll the tube. A narrow section of the, boat is assmned to be exposed to a constant heat rate produced b v an rf coil located outside the quartz tube. The results of this analysis provide essential information about various parameters such as the shape of tile molten zone, required power and temperature gradient in the system.
文摘In-situ HVEM observation on phase transition of the YBa_2Cu_3O_(7-x) superconducting compound in pro- cess of heating was carried out,and high temperature X-ray diffraction analysis in air and X-ray diffraction phase analysis for the sample treated in vacuum condition were made.The results showed that the temperature of phase transition is related to oxygen content in the sample and in general,is 100℃ to 120℃ lower in vacu- um condition than in air.At 320℃ to 350℃ twin bands begin to disappear,and some Cu_2O are formed on the surface of the sample and transit from orthorhombic YBa_2Cu_3O_(7-x) to arthorhombic Y_2BaCuO_5 compound. This transition was completed at about 500℃.Above 900℃,this compound consists of the Y_2BaCuO_5, BaCuO_2,Y_2O_3 and some other minor compounds.No phase transition was observed during cooling the sample.
基金Project(51471050105HK0101) supported by the National Key Laboratory of Precision Thermal Treatment, Harbin Institute of Technology,China
文摘2195 aluminum-lithium alloy was widely applied in the aviation and aerospace industry, but it is highly susceptible to pitting and intergranular corrosion undergoing sever corrosive circumstance and moisture atmosphere. To solve this problem and consequently to prolong its service life, a multi-step-heating-rate(MSRC) process was carried out. Investigations were carried out to find the effect of the MSRC process on the alloys corrosion resistance. It is found that the MSRC process is more favorable for the uniform phase precipitation by comparing the corrosion resistance of samples treated by traditional heat treatments. The potential difference between phases can be reduced and intergranular corrosion is able to be prohibited efficiently. Besides, the rare earth infiltration is beneficial to improving the corrosion resistance. As heating time increases, the corrosion resistance declines gradually, samples treated by artificial aging and solid solution also exhibit a better corrosion resistance.
基金supported by National Key R&D Program of China(Grant No.2021YFB3401200)Jiangsu Basic Research Program(Natural Science Fund)Youth Fund(Grant No.BK20230885)Special Technical Project for Equipment Pre-research(Grant No.30104040302).
文摘Sand mold 3D printing technology has been recognized as a digital,high-quality,and promising sand mold forming method.However,sand mold 3D printing technology has drawbacks,such as single molding material and long curing time,which limit its further industrial application.Therefore,this study proposes a method for forming composite sand molds based on a layer-stacking structure and a strengthening method based on interlayer heating.The influence of the process parameters on the properties of traditional and composite sand molds was systematically studied.Experimental results demonstrated that when the heating temperature was 150℃,the enhancement of the sand mold was obvious,with an increase of approximately 20%compared to untreated sand mold.When the composite sand mold with a laminated thickness of 1.5 mm was heated at this temperature,its tensile strength reached 1.53 MPa,and compressive strength reached 5.80 MPa,which met the casting requirements.The composite sand mold printed by interlayer heating has excellent casting performance and economic advantages,which provide theoretical guidance for the high-performance printing of sand molds.
基金supported by the Natural Science Foundation of Henan Province(Grant No.152107000047)
文摘In this study, a two-step heating process is introduced for transient liquid phase ( TLP) diffusion bonding fo r sound joints with T91 heat resistant steels. At first, a short-time higher temperature heating step is addressed to melt the interlayer, followed by the second step to complete isothermal solidification at a low temperature. The most critical feature of our new method is producing a non-planar interface at the T9/ heat resistant steels joint. We propose a transitional liquid phase bonding of T91 heat resistant steels by this approach. Since joint microstructures have been studied, we tested the tensile strength to assess joint mechanical property. The result indicates that the solidified bond may contain a primary solid-solution, similar composition to the parent metal and free from precipitates. Joint tensile strength of the joint is not lower than parent materials. Joint bend's strengths are enhanced due to the higher metal-to-metal junction producing a non-planar bond lines. Nevertheless, the traditional transient liquid phase diffusion bonding produces planar ones. Bonding parameters of new process are 1 260 °C for 0. 5 min and 1 230 °C fo r 4 min.
文摘Based on the theory of thermal conductivity, in this paper we derived a formula to estimate the prolongation period （AtL） of cooling-crystallization process of a granitic melt caused by latent heat of crystallization as follows：△tL=QL×△tcol/（TM-TC）×CP where TM is initial temperature of the granite melt, Tc crystallization temperature of the granite melt, Cp specific heat, △tcol cooling period of a granite melt from its initial temperature （TM） to its crystallization temperature （Tc）, QL latent heat of the granite melt. The cooling period of the melt for the Fanshan granodiorite from its initial temperature （900℃） to crystallization temperature （600℃） could be estimated -210,000 years if latent heat was not considered. Calculation for the Fanshan melt using the above formula yields a AtL value of -190,000 years, which implies that the actual cooling period within the temperature range of 900°-600℃ should be 400,000 years. This demonstrates that the latent heat produced from crystallization of the granitic melt is a key factor influencing the cooling-crystallization process of a granitic melt, prolongating the period of crystallization and resulting in the large emplacement-crystallization time difference （ECTD） in granite batholith.
文摘AA5083 friction stir welds were produced using systematic experimental design, the process forces and heat input with varying parameters were studied. Helpful empirical models were developed in designing friction stir welding （FSW） tools and FSW welders. These models may be further helpful for making process parameter choice for this sort of alloy, defining welding program and control of process parameters by using computer numerical control friction stir welding welders. The results show that tool rotational speed, welding speed and tool shoulder diameter are most significant parameters affecting axial force and heat input, while longitudinal force is significantly affected by welding speed and probe diameter.
