The hot deformation characteristics of induction quenched Zr-Sn-Nb-Fe-Cr alloy forged rod in the temperature range of 600–900°C and strain rate range of 0.001–1 s^(-1)were studied by Gleeble3800 uniaxial hot co...The hot deformation characteristics of induction quenched Zr-Sn-Nb-Fe-Cr alloy forged rod in the temperature range of 600–900°C and strain rate range of 0.001–1 s^(-1)were studied by Gleeble3800 uniaxial hot compression experiment.The results show that the flow stress decreases with the decrease in strain rate and the increase in deformation temperature in the true stress-true strain curve of Zr-Sn-Nb-Fe-Cr alloy forged rod.Moreover,the hot deformation characteristics of the material can be described by the hyperbolic sine constitutive equation.Under the experimental conditions,the average thermal activation energy(Q)of the alloy was 412.9105 kJ/mol.The microstructure analysis of the processing map and the sample after hot compression shows that the optimum hot working parameters of the alloy are 795–900°C,0.001–0.0068 s^(-1),at the deformation temperature of 600–900°C,and the strain rate of 0.001–1 s^(-1).展开更多
This study systematically investigates the hot deformation behavior and microstructural evolution of CoNiV medium-entropy alloy(MEA)in the temperature range of 950-1100℃ and strain rates of 0.001-1 s^(-1).The Arrheni...This study systematically investigates the hot deformation behavior and microstructural evolution of CoNiV medium-entropy alloy(MEA)in the temperature range of 950-1100℃ and strain rates of 0.001-1 s^(-1).The Arrhenius model and machine learning model were developed to forecast flow stresses at various conditions.The predictive capability of both models was assessed using the coefficients of determination(R^(2)),average absolute relative error(AARE),and root mean square error(RMSE).The findings show that the osprey optimization algorithm convolutional neural network(OOA-CNN)model outperforms the Arrhenius model,achieving a high R^(2) value of 0.99959 and lower AARE and RMSE values.The flow stress that the OOA-CNN model predicted was used to generate power dissipation maps and instability maps under different strains.Finally,combining the processing map and microstructure characterization,the ideal processing domain was identified as 1100℃ at strain rates of 0.01-0.1 s^(-1).This study provided key insights into optimizing the hot working process of CoNiV MEA.展开更多
The hot deformation behavior of GH3230 superalloy under selected deformation conditions ranging from 950 to 1150℃with strain rates ranging from 0.01 to 10 s^(–1)was studied through isothermal hot compression experim...The hot deformation behavior of GH3230 superalloy under selected deformation conditions ranging from 950 to 1150℃with strain rates ranging from 0.01 to 10 s^(–1)was studied through isothermal hot compression experiments.Based on the obtained flow stresses,a strain-compensated Arrhenius-type model was developed for the description of hot deformation behavior,and the consistency of the predicted flow stresses with the experimental values confirms the accuracy of the developed model.Furthermore,the processing maps were constructed and classified into the instability domain,low-dissipation stability domain and high-dissipation stability domain in accordance with the dynamic material model and the instability criterion.Microstructure observations indicated that the instability domain exhibits the adiabatic shear bands formation,and the low-power dissipation domain exhibits partial dynamic recrystallization(DRX),with the temperature increase/strain rate decrease being favorable for the DRX.The high-dissipation stability domain was occupied by uniformly fine equiaxed grains,and was identified as the optimal processing window,which corresponds to the deformation conditions at 1070–1150℃ with strain rates ranging from 0.01 to 0.15 s^(–1).Moreover,various DRX mechanisms are observed to occur during the hot deformation,which include the discontinuous dynamic recrystallization,characterized by nucleation at bulged boundaries,the continuous dynamic recrystallization with subgrain progressive rotation and the particle stimulated nucleation mechanism with stimulated nucleation of carbide particles.展开更多
High temperature compressive deformation behaviors of as-cast Ti-43Al-4Nb-1.4W-0.6B alloy was investigated at temperatures ranging from 1323 K to 1473 K, and strain rates from 0.001 s-1 to 1 s-1. The results indicated...High temperature compressive deformation behaviors of as-cast Ti-43Al-4Nb-1.4W-0.6B alloy was investigated at temperatures ranging from 1323 K to 1473 K, and strain rates from 0.001 s-1 to 1 s-1. The results indicated that the true stress-true strain curves show a dynamic flow softening behavior. The flow curves after the friction and the temperature compensations were employed to develop constitutive equations. The effects of temperature and the strain rate on the deformation behavior were represented by Zener-Holloman exponential equation. The influence of strain was incorporated in the constitutive analysis by considering the effect of the strain on material constants by a five-order polynomial. A revised model was proposed to describe the relationships among the flow stress, strain rate and temperature and the predicted flow stress curves were in good agreement with experimental results. Appropriate deformation processing parameters were suggested based on the processing map which was constructed from friction and temperature corrected flow curves, determined as 1343 K, 0.02 s-1 and were successfully applied in the canned forging of billets to simulate industrial work condition.展开更多
The high-temperature deformation behavior of Cu-Ni-Si-P alloy was investigated by using the hot compression test in the temperature range of 600-800 ℃ and strain rate of 0.01-5 s-1. The hot deformation activation ene...The high-temperature deformation behavior of Cu-Ni-Si-P alloy was investigated by using the hot compression test in the temperature range of 600-800 ℃ and strain rate of 0.01-5 s-1. The hot deformation activation energy, Q, was calculated and the hot compression constitutive equation was established. The processing maps of the alloy were constructed based on the experiment data and the forging process parameters were then optimized based on the generated maps for forging process determination. The flow behavior and the microstructural mechanism of the alloy were studied. The flow stress of the Cu-Ni-Si-P alloy increases with increasing strain rate and decreasing deformation temperature, and the dynamic recrystallization temperature of alloy is around 700 ℃. The hot deformation activation energy for dynamic recrystallization is determined as 485.6 kJ/mol. The processing maps for the alloy obtained at strains of 0.3 and 0.5 were used to predict the instability regimes occurring at the strain rate more than 1 s-1 and low temperature （〈650 ℃）. The optimum range for the alloy hot deformation processing in the safe domain obtained from the processing map is 750-800 ℃ at the strain rate of 0.01-0.1 s i The characteristic microstructures predicted from the processing map agree well with the results of microstructural observations.展开更多
Hot compression test of a novel nickel-free white alloy Cu?12Mn?15Zn?1.5Al?0.3Ti?0.14B?0.1Ce (mass fraction, %) was conducted on a Gleeble?1500 machine in the temperature range of 600?800 °C and the strain rate r...Hot compression test of a novel nickel-free white alloy Cu?12Mn?15Zn?1.5Al?0.3Ti?0.14B?0.1Ce (mass fraction, %) was conducted on a Gleeble?1500 machine in the temperature range of 600?800 °C and the strain rate range of 0.01?10 s?1. The constitutive equation and hot processing map of the alloy were built up according to its hot deformation behavior and hot working characteristics. The deformation activation energy of the alloy is 203.005 kJ/mol. An instability region appears in the hot deformation temperature of 600?700 °C and the strain rate range of 0.32?10 s?1 when the true strain of the alloy is up to 0.7. Under the optimal hot deformation condition of 800 °C and 10 s?1 the prepared specimen has good surface quality and interior structure. The designed nickel-free alloy has very similar white chromaticity with the traditional white copper alloy (Cu?15Ni?24Zn?1.5Pb), and the color difference between them is less than 1.5, which can hardly be distinguished by human eyes.展开更多
Hot deformation behavior of extrusion preform of the spray-formed Al-9.0Mg-0.5Mn-0.1Ti alloy was studied using hot compression tests over deformation temperature range of 300-450 ℃ and strain rate range of 0.01...Hot deformation behavior of extrusion preform of the spray-formed Al-9.0Mg-0.5Mn-0.1Ti alloy was studied using hot compression tests over deformation temperature range of 300-450 ℃ and strain rate range of 0.01-10 s-1. On the basis of experiments and dynamic material model, 2D processing maps and 3D power dissipation maps were developed for identification of exact instability regions and optimization of hot processing parameters. The experimental results indicated that the efficiency factor of energy dissipate （η） lowered to the minimum value when the deformation conditions located at the strain of 0.4, temperature of 300 ° C and strain rate of 1 s-1. The softening mechanism was dynamic recovery, the grain shape was mainly flat, and the portion of high angle grain boundary （〉15°） was 34%. While increasing the deformation temperature to 400 ° C and decreasing the strain rate to 0.1 s-1, a maximum value of η was obtained. It can be found that the main softening mechanism was dynamic recrystallization, the structures were completely recrystallized, and the portion of high angle grain boundary accounted for 86.5%. According to 2D processing maps and 3D power dissipation maps, the optimum processing conditions for the extrusion preform of the spray-formed Al？9.0Mg？0.5Mn？0.1Ti alloy were in the deformation temperature range of 340-450 ° C and the strain rate range of 0.01-0.1 s-1 with the power dissipation efficiency range of 38%？43%.展开更多
The hot deformation behavior of as-cast Mg-8Zn-1Al-0.5Cu-0.5Mn alloy was studied by hot compression tests at temperatures of 200-350 °C and strain rates of 0.001-1 s-1.The results show that the flow stress increa...The hot deformation behavior of as-cast Mg-8Zn-1Al-0.5Cu-0.5Mn alloy was studied by hot compression tests at temperatures of 200-350 °C and strain rates of 0.001-1 s-1.The results show that the flow stress increases significantly with increasing strain rate,and decreases as the temperature increases.The flow stress model based on the regression analysis was developed to predict the flow behavior of Mg-8Zn-1Al-0.5Cu-0.5Mn alloy during the hot compression,and the model shows a good agreement with experimental results.Meanwhile,the processing maps were established according to the dynamic materials model.The processing maps show that the increase of strain enlarges the instability domains,and the alloy shows good hot workability at high temperatures and low strain rates.展开更多
Hot compression tests of the extruded 7075Al/15%SiC (volume fraction) particle reinforced composite prepared by spray deposition were performed on Gleeble?1500 system in the temperature range of 300?450 °C and st...Hot compression tests of the extruded 7075Al/15%SiC (volume fraction) particle reinforced composite prepared by spray deposition were performed on Gleeble?1500 system in the temperature range of 300?450 °C and strain rate range of 0.001?1 s?1. The results indicate that the true stress?true strain curve almost exhibits rapid flow softening phenomenon without an obvious work hardening, and the stress decreases with increasing temperature and decreasing strain rate. Moreover, the stress levels are higher at temperature below 400 °C but lower at 450 °C compared with the spray deposited 7075Al alloy. Superplastic deformation characteristics are found at temperature of 450 °C and strain rate range of 0.001?0.1 s?1 with corresponding strain rate sensitivity of 0.72. The optimum parameters of hot working are determined to be temperature of 430?450 °C and strain rate of 0.001?0.05 s?1 based on processing map and optical microstructural observation.展开更多
The hot deformation behavior of GH3535 superalloy was investigated by hot compression tests in the temperature range of 1000-1200 °C and strain rate range of 0.01-50 s-1. The activation energy is about 356.3 k J/...The hot deformation behavior of GH3535 superalloy was investigated by hot compression tests in the temperature range of 1000-1200 °C and strain rate range of 0.01-50 s-1. The activation energy is about 356.3 k J/mol, and the flow curves and processing map were developed on the basis of experimental data. The processing map exhibits a stable domain which occurs in the strain rate range of 0.01-1 s-1 at all the temperatures and a instable domain which occurs in the strain rate range of 1-50 s-1. Microstructural observations reveal that the full dynamic recrystallization（DRX） occurs in the conditions of（1150 °C, 0.01 s-1）,（1200 °C, 0.01 s-1） and（1200 °C, 0.1 s-1） with different grain sizes and undissolved carbides. The flow localization and cracks occur in the regime of flow instability.展开更多
The true stress-strain curves of as-cast 7075 aluminum alloy have been obtained by isothermal compression tests at temperatures of 300 500 ~C and strain rates of 0.01 10 s i. The plastic flow instability map is establ...The true stress-strain curves of as-cast 7075 aluminum alloy have been obtained by isothermal compression tests at temperatures of 300 500 ~C and strain rates of 0.01 10 s i. The plastic flow instability map is established based on Gegel B and Murthy instability criteria because the deformed compression samples suggest that the combination of the above two instability criteria has more comprehensive crack prediction ability. And the processing map based on Dynamic Mate- rial Model （DMM） of as-cast 7075 aluminum alloy has been developed through a superposition of the established instability map and power dissipation map. In terms of microstructure of the deformed samples and whether plastic flow is stable or not, the processing map can be divided into five areas： stable area with as-cast grain, stable area with homogeneous grain resulting from dynamic recovery, instability area with as-cast grain, instability area with the second phase and instability area with mixed grains. In consideration of microstructure characteristics in the above five areas of the processing map, the stable area with homogeneous grain resulting from dynamic recovery, namely the temperatures at 425465 ℃ and the strain rates at 0.01^-1 s^-1, is suggested to be suitable processing window for the as-cast 7075 aluminum alloy.展开更多
The effect of the volume fraction of I-phase on the hot compressive behavior and processing maps of the extruded Mg-Zn-Y alloys was examined, and the obtained results were compared with those of the cast alloys in a p...The effect of the volume fraction of I-phase on the hot compressive behavior and processing maps of the extruded Mg-Zn-Y alloys was examined, and the obtained results were compared with those of the cast alloys in a previous work. The average grain sizes, fractions of dynamically recrystallized(DRXed) grains,and sizes of DRXed grains of the extruded alloys after compressive deformation were significantly smaller,higher and smaller, respectively, than those of the cast alloys after compressive deformation under the same experimental conditions. This was because the microstructures of the extruded alloys, having much more grain boundaries and more refined I-phase particles than the cast alloys, provided a larger number of nucleation sites for dynamic recrystallization than those of the cast alloys. The constitutive equations for high-temperature deformation of the extruded and cast alloys could be derived using the same activation energy for plastic flow, which was close to the activation energy for lattice diffusion in magnesium.Compared with the cast alloys, the onset of the power law breakdown(PLB) occurred at larger ZenerHolloman(Z) parameter values in the extruded alloys. This was because the extruded alloys had finer initial grain sizes and higher fractions of finer DRXed grains compared to the cast alloys, such that the onset of PLB caused by creation of excessive concentrations of deformation-induced vacancies was delayed to a higher strain rate and a lower temperature. The flow-stress difference between the extruded alloys and the cast alloys could be attributed to the difference in the fraction of DRXed grains. According to the processing maps, the extruded alloys exhibited higher power dissipation efficiency and flow stability than the cast alloys. This agreed with the microstructural observations.展开更多
The hot deformation behavior of a fine-grained Mg–8 Sn–2 Zn–2 Al(TZA822, in wt%) alloy was investigated in the temperature range of 150–350°C and the strain rate of 0.01–10 s^-1 employing thermomechanical si...The hot deformation behavior of a fine-grained Mg–8 Sn–2 Zn–2 Al(TZA822, in wt%) alloy was investigated in the temperature range of 150–350°C and the strain rate of 0.01–10 s^-1 employing thermomechanical simulator. In most of the cases, the material showed typical dynamic recrystallization(DRX) features i.e., a signal peak value followed by a gradual decrease or to reach a steady state. The work hardening rate was found to increase with decreasing temperature and increasing strain rate, while strain rates had great effects on work hardening behavior. Meanwhile, the constitutive analysis indicated that cross-slip of dislocations was likely to be the dominant deformation mechanism. In addition, the processing map at the strain of 0.1–0.7 showed two stability domains with high power dissipation efficiencies and the optimum hot working parameters for the studied alloy was determined to be 350°C/0.01 s^-1 and 350°C/10 s^-1, at which continuous DRX(CDRX) and discontinuous DRX(DDRX) as main softening mechanism. The instability regions occurred at 200–250°C/10 s^-1 and the main flow instability mechanism was twinning and/or flow localization bands, which were prone to induce cracks and caused in-consistent mechanical properties of the alloy.展开更多
The hot deformation behaviour of 7075 aluminium alloy reinforced with 10%of SiC particles was studied by employing both"processing maps"and microstructural observations.The composite was characterized by emp...The hot deformation behaviour of 7075 aluminium alloy reinforced with 10%of SiC particles was studied by employing both"processing maps"and microstructural observations.The composite was characterized by employing optical microscope to evaluate the microstructural transformations and instability phenomena.The material investigated was deformed by compression in the temperature and strain rate ranges of 300-500℃and 0.001-1.0 s-1,respectively.The deformation efficiency was calculated by strain rate sensitivity(m)values obtained by hot compression tests.The power dissipation efficiency and instability parameters were evaluated and processing maps were constructed for strain of 0.5.The optimum domains and instability zone were obtained for the composites.The optimum processing conditions are obtained in the strain rate range of 0.1-0.9 s-1and temperature range of 390-440 ℃with the efficiency of 30%.展开更多
The hot deformation behavior of AA2014forging aluminum alloy was investigated by isothermal compression tests attemperatures of350-480°C and strain rates of0.001-1s-1on a Gleeble-3180simulator.The corresponding m...The hot deformation behavior of AA2014forging aluminum alloy was investigated by isothermal compression tests attemperatures of350-480°C and strain rates of0.001-1s-1on a Gleeble-3180simulator.The corresponding microstructures of thealloys under different deformation conditions were studied using optical microscopy(OM),electron back scattered diffraction(EBSD)and transmission electron microscopy(TEM).The processing maps were constructed with strains of0.1,0.3,0.5and0.7.The results showed that the instability domain was more inclined to occur at strain rates higher than0.1s-1and manifested in theform of local non-uniform deformation.At the strain of0.7,the processing map showed two stability domains:domain I(350-430°C,0.005-0.1s-1)and domain II(450-480°C,0.001-0.05s-1).The predominant softening mechanisms in both of the twodomains were dynamic recovery.Uniform microstructures were obtained in domain I,and an extended recovery occurred in domainII,which would lead to the potential sub-grain boundaries progressively transforming into new high-angle grain boundaries.Theoptimum hot working parameters for the AA2014forging aluminum alloy were determined to be370-420°C and0.008-0.08s-1.展开更多
High strength β titanium alloys are widely used in large load bearing components in the aerospace field. At present, large parts are generally formed by die forging. Different initial microstructures and deformation ...High strength β titanium alloys are widely used in large load bearing components in the aerospace field. At present, large parts are generally formed by die forging. Different initial microstructures and deformation process parameters will significantly affect the flow behavior. To precisely control the microstructures, researchers have conducted many studies to analyze the microstructure evolution law and deformation mechanism during hot compression. This review focuses on the microstructure evolution of high strength β titanium alloys during hot deformation, including dynamic recrystallization and dynamic recovery in the single-phase region and the dynamic evolution of the α phase in the two-phase region. Furthermore, the optimal hot processing regions, instability regions,and the relationship between the efficiency of power dissipation and the deformation mechanism in the hot processing map are summarized. Finally, the problems and development direction of using hot processing maps to optimize process parameters are also emphasized.展开更多
The hot deformation characteristics of the Ti-5.7Al-2.1Sn-3.9Zr-2Mo-0.1Si(Ti-6242S)alloy with an acicular starting microstructure were analyzed using processing map.The uniaxial hot compression tests were performed at...The hot deformation characteristics of the Ti-5.7Al-2.1Sn-3.9Zr-2Mo-0.1Si(Ti-6242S)alloy with an acicular starting microstructure were analyzed using processing map.The uniaxial hot compression tests were performed at temperatures ranging from 850 to 1000℃and at strain rates of 0.001-1 s-1.The developed processing map was used to determine the safe and unsafe deformation conditions of the alloy in association with the microstructural evolution by SEM and OM.It was recognized that the flow stress revealed differences in flow softening behavior by deformation at 1000℃compared to the lower deformation temperatures,which was attributed to microstructural changes.The processing map developed for typical strain of 0.7 in two-phase field exhibited high efficiency value of power dissipation of about 55%at 950℃and 0.001 s-1,basically due to extensive globularization.An increase in strain rate and a decrease in temperature resulted in a decrease in globularization ofαlamellae,whileαlamellar kinking increased.Eventually,the instability domain of flow behavior was identified in the temperature range of 850-900℃and at the strain rate higher than 0.01 s-1 reflecting the flow localization and adiabatic shear banding.By considering the power efficiency domains and the microstructural observations,the deformation in the temperature range of 950-1000℃and strain rate range of 0.001-0.01 s-1 was desirable leading to high efficiencies.It was realized that(950℃,0.001 s-1)was the optimum deformation condition for the alloy.展开更多
Hot deformation behavior of the Cu-Cr-Zr alloy was investigated using hot compressive tests in the tem- perature range of 650-850℃ and strain rate range of 0.001-10 s-1. The constitutive equation of the alloy based o...Hot deformation behavior of the Cu-Cr-Zr alloy was investigated using hot compressive tests in the tem- perature range of 650-850℃ and strain rate range of 0.001-10 s-1. The constitutive equation of the alloy based on the hyperbolic-sine equation was established to characterize the flow stress as a function of strain rate and deformation temperature. The critical conditions for the occurrence of dynamic recrystallization were determined based on the alloy strain hardening rate curves. Based on the dynamic material model, the processing maps at the strains of 0.3, 0.4 and 0.5 were obtained. When the true strain was 0.5, greater power dissipation efficiency was observed at 800-850 ℃ and under 0.001-0.1 s-1, with the peak efficiency of 47%. The evolution of DRX microstructure strongly depends on the deformation temperature and the strain rate. Based on the processing maps and microstructure evolution, the optimal hot working conditions for the Cu-Cr-Zr alloy are in the temperature range of 800-850 ℃ and the strain rate range of 0.001-0.1 s-1.展开更多
The hot deformation behavior and processing map of Cu-bearing 2205 duplex stainless steel(2205-Cu DSS)were investigated at temperatures of 950-1150℃ and strain rates of 0.01-10 s^-1.The effects of Cu addition and dif...The hot deformation behavior and processing map of Cu-bearing 2205 duplex stainless steel(2205-Cu DSS)were investigated at temperatures of 950-1150℃ and strain rates of 0.01-10 s^-1.The effects of Cu addition and different deformation parameters on deformation behavior were,respectively,characterized by analyzing flow curves,constitutive equations and microstructures.The results indicated that the shapes of flow curves strongly depended on the volume fraction of two phases.When deformed at low strain rate,DRV in ferrite was prompted with increase in the temperature and was further developed to continuous DRX.At high strain rate,flow localization preferentially occurred in ferrite at low deformation temperature due to the strain partitioning and relatively less fraction of ferrite.The activation energy for 2205-Cu DSS was 452 kJ/mol and was found to connect with the variation of strain,strain rate and deformation temperature.The optimum hot deformation parameters for 2205-Cu DSS were obtained in the temperature range of 1100-1150℃ and strain rate range of 0.1-1 s^-1 with a peak power dissipation efficiency of 41%.Flow localization was the main way to lead to flow instability.Meanwhile,the Cu-rich precipitates were generated within a few ferrite grains when deformed at temperature lower than 1000℃.The interaction between dislocations and Cu-rich precipitates at high strain rate,as well as the limited DRV in ferrite and DRX in austenite,contributed to the complex microstructure and flow behavior.展开更多
The hot deformation behavior of Ti22A125 Nb was investigated by hot compression test.The flow stressstrain curves can be divided into two types：conventional dynamic recrystallization（DRX） and discontinuous DRX.The ...The hot deformation behavior of Ti22A125 Nb was investigated by hot compression test.The flow stressstrain curves can be divided into two types：conventional dynamic recrystallization（DRX） and discontinuous DRX.The different softening mechanism and micro structure observation of conventional DRX and discontinuous DRX were analyzed.The processing map（PM） of Ti22A125 Nb was built to predict the safe deformation region.The optimal low strain rate domain（DOM I） with high power dissipation efficiency indicates the complete DRX.Additionally,in the high strain rate and low-temperature domain（DOM Ⅲ）,the power dissipation efficiency is low and some adiabatic shear bands and glide bands are observed,which are unsafe and should be avoided.Finally,the DRX map was established.In DOM I,it reveals low dislocation density and high DRX content,which is in agreement with PM.展开更多
文摘The hot deformation characteristics of induction quenched Zr-Sn-Nb-Fe-Cr alloy forged rod in the temperature range of 600–900°C and strain rate range of 0.001–1 s^(-1)were studied by Gleeble3800 uniaxial hot compression experiment.The results show that the flow stress decreases with the decrease in strain rate and the increase in deformation temperature in the true stress-true strain curve of Zr-Sn-Nb-Fe-Cr alloy forged rod.Moreover,the hot deformation characteristics of the material can be described by the hyperbolic sine constitutive equation.Under the experimental conditions,the average thermal activation energy(Q)of the alloy was 412.9105 kJ/mol.The microstructure analysis of the processing map and the sample after hot compression shows that the optimum hot working parameters of the alloy are 795–900°C,0.001–0.0068 s^(-1),at the deformation temperature of 600–900°C,and the strain rate of 0.001–1 s^(-1).
基金supported by the National Natural Science Foundation of China(NSFC)(Grant No.51901078)the Central Guidance for Local Scientific and Technological Development Funding Project(Grant No.236Z1003G)+3 种基金the Science and Technology Plan Project of Tangshan City(Grant No.24130207C)the Natural Science Foundation of Hebei Province(Grant No.E2022209070)the High-level Talent Project of Hebei(Grant No.E2019100007)the Open Project Program of Key Laboratory of Ministry of Education for Modern Metallurgy Technology(Grant No.2024YJKF02).
文摘This study systematically investigates the hot deformation behavior and microstructural evolution of CoNiV medium-entropy alloy(MEA)in the temperature range of 950-1100℃ and strain rates of 0.001-1 s^(-1).The Arrhenius model and machine learning model were developed to forecast flow stresses at various conditions.The predictive capability of both models was assessed using the coefficients of determination(R^(2)),average absolute relative error(AARE),and root mean square error(RMSE).The findings show that the osprey optimization algorithm convolutional neural network(OOA-CNN)model outperforms the Arrhenius model,achieving a high R^(2) value of 0.99959 and lower AARE and RMSE values.The flow stress that the OOA-CNN model predicted was used to generate power dissipation maps and instability maps under different strains.Finally,combining the processing map and microstructure characterization,the ideal processing domain was identified as 1100℃ at strain rates of 0.01-0.1 s^(-1).This study provided key insights into optimizing the hot working process of CoNiV MEA.
基金the National Key Research and Development Program of China(No.2016YFB0700505)the National Natural Science Foundation of China(No.51571020).
文摘The hot deformation behavior of GH3230 superalloy under selected deformation conditions ranging from 950 to 1150℃with strain rates ranging from 0.01 to 10 s^(–1)was studied through isothermal hot compression experiments.Based on the obtained flow stresses,a strain-compensated Arrhenius-type model was developed for the description of hot deformation behavior,and the consistency of the predicted flow stresses with the experimental values confirms the accuracy of the developed model.Furthermore,the processing maps were constructed and classified into the instability domain,low-dissipation stability domain and high-dissipation stability domain in accordance with the dynamic material model and the instability criterion.Microstructure observations indicated that the instability domain exhibits the adiabatic shear bands formation,and the low-power dissipation domain exhibits partial dynamic recrystallization(DRX),with the temperature increase/strain rate decrease being favorable for the DRX.The high-dissipation stability domain was occupied by uniformly fine equiaxed grains,and was identified as the optimal processing window,which corresponds to the deformation conditions at 1070–1150℃ with strain rates ranging from 0.01 to 0.15 s^(–1).Moreover,various DRX mechanisms are observed to occur during the hot deformation,which include the discontinuous dynamic recrystallization,characterized by nucleation at bulged boundaries,the continuous dynamic recrystallization with subgrain progressive rotation and the particle stimulated nucleation mechanism with stimulated nucleation of carbide particles.
基金Project(2011CB605505)supported by the National Key Fundamental Research Development Project of ChinaProjects(51301204,51174233)supported by the National Natural Science Foundation of ChinaProject(2011JQ002)supported by the Fundamental Research Funds for the Central Universities of China
文摘High temperature compressive deformation behaviors of as-cast Ti-43Al-4Nb-1.4W-0.6B alloy was investigated at temperatures ranging from 1323 K to 1473 K, and strain rates from 0.001 s-1 to 1 s-1. The results indicated that the true stress-true strain curves show a dynamic flow softening behavior. The flow curves after the friction and the temperature compensations were employed to develop constitutive equations. The effects of temperature and the strain rate on the deformation behavior were represented by Zener-Holloman exponential equation. The influence of strain was incorporated in the constitutive analysis by considering the effect of the strain on material constants by a five-order polynomial. A revised model was proposed to describe the relationships among the flow stress, strain rate and temperature and the predicted flow stress curves were in good agreement with experimental results. Appropriate deformation processing parameters were suggested based on the processing map which was constructed from friction and temperature corrected flow curves, determined as 1343 K, 0.02 s-1 and were successfully applied in the canned forging of billets to simulate industrial work condition.
基金Project(51101052) supported by the National Natural Science Foundation of China
文摘The high-temperature deformation behavior of Cu-Ni-Si-P alloy was investigated by using the hot compression test in the temperature range of 600-800 ℃ and strain rate of 0.01-5 s-1. The hot deformation activation energy, Q, was calculated and the hot compression constitutive equation was established. The processing maps of the alloy were constructed based on the experiment data and the forging process parameters were then optimized based on the generated maps for forging process determination. The flow behavior and the microstructural mechanism of the alloy were studied. The flow stress of the Cu-Ni-Si-P alloy increases with increasing strain rate and decreasing deformation temperature, and the dynamic recrystallization temperature of alloy is around 700 ℃. The hot deformation activation energy for dynamic recrystallization is determined as 485.6 kJ/mol. The processing maps for the alloy obtained at strains of 0.3 and 0.5 were used to predict the instability regimes occurring at the strain rate more than 1 s-1 and low temperature （〈650 ℃）. The optimum range for the alloy hot deformation processing in the safe domain obtained from the processing map is 750-800 ℃ at the strain rate of 0.01-0.1 s i The characteristic microstructures predicted from the processing map agree well with the results of microstructural observations.
基金Project(51271203)supported by the National Natural Science Foundation of ChinaProject(CX2012B037)supported by the Hunan Provincial Innovation Foundation for Postgraduate,China+1 种基金Project(2013zzts017)supported by the Graduate Degree Thesis Innovation Foundation of Central South University,ChinaProject(2012bjjxj015)supported by the Excellent Doctor Degree Thesis Support Foundation of Central South University,China
文摘Hot compression test of a novel nickel-free white alloy Cu?12Mn?15Zn?1.5Al?0.3Ti?0.14B?0.1Ce (mass fraction, %) was conducted on a Gleeble?1500 machine in the temperature range of 600?800 °C and the strain rate range of 0.01?10 s?1. The constitutive equation and hot processing map of the alloy were built up according to its hot deformation behavior and hot working characteristics. The deformation activation energy of the alloy is 203.005 kJ/mol. An instability region appears in the hot deformation temperature of 600?700 °C and the strain rate range of 0.32?10 s?1 when the true strain of the alloy is up to 0.7. Under the optimal hot deformation condition of 800 °C and 10 s?1 the prepared specimen has good surface quality and interior structure. The designed nickel-free alloy has very similar white chromaticity with the traditional white copper alloy (Cu?15Ni?24Zn?1.5Pb), and the color difference between them is less than 1.5, which can hardly be distinguished by human eyes.
基金Project(51301065)supported by the National Natural Science Foundation of ChinaProject(15B063)supported by the Youth Research Foundation of Education Bureau of Hunan Province,China
文摘Hot deformation behavior of extrusion preform of the spray-formed Al-9.0Mg-0.5Mn-0.1Ti alloy was studied using hot compression tests over deformation temperature range of 300-450 ℃ and strain rate range of 0.01-10 s-1. On the basis of experiments and dynamic material model, 2D processing maps and 3D power dissipation maps were developed for identification of exact instability regions and optimization of hot processing parameters. The experimental results indicated that the efficiency factor of energy dissipate （η） lowered to the minimum value when the deformation conditions located at the strain of 0.4, temperature of 300 ° C and strain rate of 1 s-1. The softening mechanism was dynamic recovery, the grain shape was mainly flat, and the portion of high angle grain boundary （〉15°） was 34%. While increasing the deformation temperature to 400 ° C and decreasing the strain rate to 0.1 s-1, a maximum value of η was obtained. It can be found that the main softening mechanism was dynamic recrystallization, the structures were completely recrystallized, and the portion of high angle grain boundary accounted for 86.5%. According to 2D processing maps and 3D power dissipation maps, the optimum processing conditions for the extrusion preform of the spray-formed Al？9.0Mg？0.5Mn？0.1Ti alloy were in the deformation temperature range of 340-450 ° C and the strain rate range of 0.01-0.1 s-1 with the power dissipation efficiency range of 38%？43%.
基金Project(51274184)supported by the National Natural Science Foundation of ChinaProject(2013CB632205)supported by the National Basic Research Program of China
文摘The hot deformation behavior of as-cast Mg-8Zn-1Al-0.5Cu-0.5Mn alloy was studied by hot compression tests at temperatures of 200-350 °C and strain rates of 0.001-1 s-1.The results show that the flow stress increases significantly with increasing strain rate,and decreases as the temperature increases.The flow stress model based on the regression analysis was developed to predict the flow behavior of Mg-8Zn-1Al-0.5Cu-0.5Mn alloy during the hot compression,and the model shows a good agreement with experimental results.Meanwhile,the processing maps were established according to the dynamic materials model.The processing maps show that the increase of strain enlarges the instability domains,and the alloy shows good hot workability at high temperatures and low strain rates.
基金Project(51271076)supported by the National Natural Science Foundation of China
文摘Hot compression tests of the extruded 7075Al/15%SiC (volume fraction) particle reinforced composite prepared by spray deposition were performed on Gleeble?1500 system in the temperature range of 300?450 °C and strain rate range of 0.001?1 s?1. The results indicate that the true stress?true strain curve almost exhibits rapid flow softening phenomenon without an obvious work hardening, and the stress decreases with increasing temperature and decreasing strain rate. Moreover, the stress levels are higher at temperature below 400 °C but lower at 450 °C compared with the spray deposited 7075Al alloy. Superplastic deformation characteristics are found at temperature of 450 °C and strain rate range of 0.001?0.1 s?1 with corresponding strain rate sensitivity of 0.72. The optimum parameters of hot working are determined to be temperature of 430?450 °C and strain rate of 0.001?0.05 s?1 based on processing map and optical microstructural observation.
基金Project(XDA02040000)supported by the Strategic Priority Research Program of the Chinese Academy of Sciences
文摘The hot deformation behavior of GH3535 superalloy was investigated by hot compression tests in the temperature range of 1000-1200 °C and strain rate range of 0.01-50 s-1. The activation energy is about 356.3 k J/mol, and the flow curves and processing map were developed on the basis of experimental data. The processing map exhibits a stable domain which occurs in the strain rate range of 0.01-1 s-1 at all the temperatures and a instable domain which occurs in the strain rate range of 1-50 s-1. Microstructural observations reveal that the full dynamic recrystallization（DRX） occurs in the conditions of（1150 °C, 0.01 s-1）,（1200 °C, 0.01 s-1） and（1200 °C, 0.1 s-1） with different grain sizes and undissolved carbides. The flow localization and cracks occur in the regime of flow instability.
基金financially supported by the National Science and Technology Major Project of China(No.2009ZX04005-031-11)the EU Marie Curie Actions–Mat Pro Future Project(No.FP7-PEOPLE-2012-IRSES-318968)the‘‘111"Project of China(No.B08040)
文摘The true stress-strain curves of as-cast 7075 aluminum alloy have been obtained by isothermal compression tests at temperatures of 300 500 ~C and strain rates of 0.01 10 s i. The plastic flow instability map is established based on Gegel B and Murthy instability criteria because the deformed compression samples suggest that the combination of the above two instability criteria has more comprehensive crack prediction ability. And the processing map based on Dynamic Mate- rial Model （DMM） of as-cast 7075 aluminum alloy has been developed through a superposition of the established instability map and power dissipation map. In terms of microstructure of the deformed samples and whether plastic flow is stable or not, the processing map can be divided into five areas： stable area with as-cast grain, stable area with homogeneous grain resulting from dynamic recovery, instability area with as-cast grain, instability area with the second phase and instability area with mixed grains. In consideration of microstructure characteristics in the above five areas of the processing map, the stable area with homogeneous grain resulting from dynamic recovery, namely the temperatures at 425465 ℃ and the strain rates at 0.01^-1 s^-1, is suggested to be suitable processing window for the as-cast 7075 aluminum alloy.
基金the financial support from the Mid-Career Researcher Program through the National Research Foundation of Korea(2016) funded by the Ministry of Education,Science and Technology(No.2016R1A2B4015481)
文摘The effect of the volume fraction of I-phase on the hot compressive behavior and processing maps of the extruded Mg-Zn-Y alloys was examined, and the obtained results were compared with those of the cast alloys in a previous work. The average grain sizes, fractions of dynamically recrystallized(DRXed) grains,and sizes of DRXed grains of the extruded alloys after compressive deformation were significantly smaller,higher and smaller, respectively, than those of the cast alloys after compressive deformation under the same experimental conditions. This was because the microstructures of the extruded alloys, having much more grain boundaries and more refined I-phase particles than the cast alloys, provided a larger number of nucleation sites for dynamic recrystallization than those of the cast alloys. The constitutive equations for high-temperature deformation of the extruded and cast alloys could be derived using the same activation energy for plastic flow, which was close to the activation energy for lattice diffusion in magnesium.Compared with the cast alloys, the onset of the power law breakdown(PLB) occurred at larger ZenerHolloman(Z) parameter values in the extruded alloys. This was because the extruded alloys had finer initial grain sizes and higher fractions of finer DRXed grains compared to the cast alloys, such that the onset of PLB caused by creation of excessive concentrations of deformation-induced vacancies was delayed to a higher strain rate and a lower temperature. The flow-stress difference between the extruded alloys and the cast alloys could be attributed to the difference in the fraction of DRXed grains. According to the processing maps, the extruded alloys exhibited higher power dissipation efficiency and flow stability than the cast alloys. This agreed with the microstructural observations.
基金financially supported by the National Natural Science Foundation of China(Nos.51404166,51704209 and51701060)the Shanxi Scholarship Council of China(No.2014-023)+4 种基金the Scientific and Technological Innovation Programs of Higher Education Institutions in Shanxi(No.2014017)the Shanxi Province Science Foundation for Youths(No.2016021063)the Natural Science Foundation of Hebei Province(No.E2016202130)the Research Foundation from Education Department of Hebei(No.QN2015035)the Outstanding Youth Scholar Science and Technology Innovation Program of Hebei University of Technology(No.2015002)
文摘The hot deformation behavior of a fine-grained Mg–8 Sn–2 Zn–2 Al(TZA822, in wt%) alloy was investigated in the temperature range of 150–350°C and the strain rate of 0.01–10 s^-1 employing thermomechanical simulator. In most of the cases, the material showed typical dynamic recrystallization(DRX) features i.e., a signal peak value followed by a gradual decrease or to reach a steady state. The work hardening rate was found to increase with decreasing temperature and increasing strain rate, while strain rates had great effects on work hardening behavior. Meanwhile, the constitutive analysis indicated that cross-slip of dislocations was likely to be the dominant deformation mechanism. In addition, the processing map at the strain of 0.1–0.7 showed two stability domains with high power dissipation efficiencies and the optimum hot working parameters for the studied alloy was determined to be 350°C/0.01 s^-1 and 350°C/10 s^-1, at which continuous DRX(CDRX) and discontinuous DRX(DDRX) as main softening mechanism. The instability regions occurred at 200–250°C/10 s^-1 and the main flow instability mechanism was twinning and/or flow localization bands, which were prone to induce cracks and caused in-consistent mechanical properties of the alloy.
文摘The hot deformation behaviour of 7075 aluminium alloy reinforced with 10%of SiC particles was studied by employing both"processing maps"and microstructural observations.The composite was characterized by employing optical microscope to evaluate the microstructural transformations and instability phenomena.The material investigated was deformed by compression in the temperature and strain rate ranges of 300-500℃and 0.001-1.0 s-1,respectively.The deformation efficiency was calculated by strain rate sensitivity(m)values obtained by hot compression tests.The power dissipation efficiency and instability parameters were evaluated and processing maps were constructed for strain of 0.5.The optimum domains and instability zone were obtained for the composites.The optimum processing conditions are obtained in the strain rate range of 0.1-0.9 s-1and temperature range of 390-440 ℃with the efficiency of 30%.
基金Project(51301209) supported by the National Natural Science Foundation of China
文摘The hot deformation behavior of AA2014forging aluminum alloy was investigated by isothermal compression tests attemperatures of350-480°C and strain rates of0.001-1s-1on a Gleeble-3180simulator.The corresponding microstructures of thealloys under different deformation conditions were studied using optical microscopy(OM),electron back scattered diffraction(EBSD)and transmission electron microscopy(TEM).The processing maps were constructed with strains of0.1,0.3,0.5and0.7.The results showed that the instability domain was more inclined to occur at strain rates higher than0.1s-1and manifested in theform of local non-uniform deformation.At the strain of0.7,the processing map showed two stability domains:domain I(350-430°C,0.005-0.1s-1)and domain II(450-480°C,0.001-0.05s-1).The predominant softening mechanisms in both of the twodomains were dynamic recovery.Uniform microstructures were obtained in domain I,and an extended recovery occurred in domainII,which would lead to the potential sub-grain boundaries progressively transforming into new high-angle grain boundaries.Theoptimum hot working parameters for the AA2014forging aluminum alloy were determined to be370-420°C and0.008-0.08s-1.
基金supported by the Project of National Key Laboratory for Precision Hot Processing of Metals, Harbin Institute of Technology, China (No. 6142909190207)Shaanxi Key Laboratory of High-performance Precision Forming Technology and Equipment (SKL-HPFTE), China (No. PETE-2019-KF-01)。
文摘High strength β titanium alloys are widely used in large load bearing components in the aerospace field. At present, large parts are generally formed by die forging. Different initial microstructures and deformation process parameters will significantly affect the flow behavior. To precisely control the microstructures, researchers have conducted many studies to analyze the microstructure evolution law and deformation mechanism during hot compression. This review focuses on the microstructure evolution of high strength β titanium alloys during hot deformation, including dynamic recrystallization and dynamic recovery in the single-phase region and the dynamic evolution of the α phase in the two-phase region. Furthermore, the optimal hot processing regions, instability regions,and the relationship between the efficiency of power dissipation and the deformation mechanism in the hot processing map are summarized. Finally, the problems and development direction of using hot processing maps to optimize process parameters are also emphasized.
文摘The hot deformation characteristics of the Ti-5.7Al-2.1Sn-3.9Zr-2Mo-0.1Si(Ti-6242S)alloy with an acicular starting microstructure were analyzed using processing map.The uniaxial hot compression tests were performed at temperatures ranging from 850 to 1000℃and at strain rates of 0.001-1 s-1.The developed processing map was used to determine the safe and unsafe deformation conditions of the alloy in association with the microstructural evolution by SEM and OM.It was recognized that the flow stress revealed differences in flow softening behavior by deformation at 1000℃compared to the lower deformation temperatures,which was attributed to microstructural changes.The processing map developed for typical strain of 0.7 in two-phase field exhibited high efficiency value of power dissipation of about 55%at 950℃and 0.001 s-1,basically due to extensive globularization.An increase in strain rate and a decrease in temperature resulted in a decrease in globularization ofαlamellae,whileαlamellar kinking increased.Eventually,the instability domain of flow behavior was identified in the temperature range of 850-900℃and at the strain rate higher than 0.01 s-1 reflecting the flow localization and adiabatic shear banding.By considering the power efficiency domains and the microstructural observations,the deformation in the temperature range of 950-1000℃and strain rate range of 0.001-0.01 s-1 was desirable leading to high efficiencies.It was realized that(950℃,0.001 s-1)was the optimum deformation condition for the alloy.
基金financially supported by the National Natural Science Foundation of China(No.51101052)the National Science Foundation(No.IRES 1358088)
文摘Hot deformation behavior of the Cu-Cr-Zr alloy was investigated using hot compressive tests in the tem- perature range of 650-850℃ and strain rate range of 0.001-10 s-1. The constitutive equation of the alloy based on the hyperbolic-sine equation was established to characterize the flow stress as a function of strain rate and deformation temperature. The critical conditions for the occurrence of dynamic recrystallization were determined based on the alloy strain hardening rate curves. Based on the dynamic material model, the processing maps at the strains of 0.3, 0.4 and 0.5 were obtained. When the true strain was 0.5, greater power dissipation efficiency was observed at 800-850 ℃ and under 0.001-0.1 s-1, with the peak efficiency of 47%. The evolution of DRX microstructure strongly depends on the deformation temperature and the strain rate. Based on the processing maps and microstructure evolution, the optimal hot working conditions for the Cu-Cr-Zr alloy are in the temperature range of 800-850 ℃ and the strain rate range of 0.001-0.1 s-1.
基金financially supported by the National Key Research and Development Program of China (Grant No.2016YFB0300205)the National Natural Science Foundation of China (Grant Nos.51501188 and 51771199)+2 种基金the State KeyProgram of National Natural Science of China (Grant No.51631009)Shenzhen-Hong Kong Technology Cooperation Funding Scheme (SGLH20150213143207910)Shenzhen Science and Technology Research Funding (JCYJ20160608153641020)
文摘The hot deformation behavior and processing map of Cu-bearing 2205 duplex stainless steel(2205-Cu DSS)were investigated at temperatures of 950-1150℃ and strain rates of 0.01-10 s^-1.The effects of Cu addition and different deformation parameters on deformation behavior were,respectively,characterized by analyzing flow curves,constitutive equations and microstructures.The results indicated that the shapes of flow curves strongly depended on the volume fraction of two phases.When deformed at low strain rate,DRV in ferrite was prompted with increase in the temperature and was further developed to continuous DRX.At high strain rate,flow localization preferentially occurred in ferrite at low deformation temperature due to the strain partitioning and relatively less fraction of ferrite.The activation energy for 2205-Cu DSS was 452 kJ/mol and was found to connect with the variation of strain,strain rate and deformation temperature.The optimum hot deformation parameters for 2205-Cu DSS were obtained in the temperature range of 1100-1150℃ and strain rate range of 0.1-1 s^-1 with a peak power dissipation efficiency of 41%.Flow localization was the main way to lead to flow instability.Meanwhile,the Cu-rich precipitates were generated within a few ferrite grains when deformed at temperature lower than 1000℃.The interaction between dislocations and Cu-rich precipitates at high strain rate,as well as the limited DRV in ferrite and DRX in austenite,contributed to the complex microstructure and flow behavior.
基金financially supported by the National Natural Science Foundation of China(No.51175431)
文摘The hot deformation behavior of Ti22A125 Nb was investigated by hot compression test.The flow stressstrain curves can be divided into two types：conventional dynamic recrystallization（DRX） and discontinuous DRX.The different softening mechanism and micro structure observation of conventional DRX and discontinuous DRX were analyzed.The processing map（PM） of Ti22A125 Nb was built to predict the safe deformation region.The optimal low strain rate domain（DOM I） with high power dissipation efficiency indicates the complete DRX.Additionally,in the high strain rate and low-temperature domain（DOM Ⅲ）,the power dissipation efficiency is low and some adiabatic shear bands and glide bands are observed,which are unsafe and should be avoided.Finally,the DRX map was established.In DOM I,it reveals low dislocation density and high DRX content,which is in agreement with PM.
