Dynamic recrystallization(DRX)in inhomogeneous deformation zones,such as grain boundaries,shear bands,and deformation bands,is critical for texture modification in magnesium alloys during deformation at elevated temper...Dynamic recrystallization(DRX)in inhomogeneous deformation zones,such as grain boundaries,shear bands,and deformation bands,is critical for texture modification in magnesium alloys during deformation at elevated temperatures.This study investigates the DRX mechanisms in AZWX3100 magnesium alloy under plane strain compression at 200℃.Microstructural analysis revealed necklace-type DRX accompanied by evidence of local grain boundary bulging.Additionally,ribbons of recrystallized grains were observed withinfine deformation bands,aligned with theoretical pyramidal I and II slip traces derived from the matrix.The distribution of local misorientation within the deformed microstructure demonstrated a clear association between deformation bands and localized strain.Dislocation analysis of lamellar specimens extracted from two pyramidal slip bands revealed<c+a>dislocations,indicating a connection between<c+a>slip activation and the formation of deformation bands.Crystal plasticity simulations suggest that the orientation of deformation bands is responsible for the unique recrystallization texture of the DRX grains within these bands.The texture characteristics imply a progressive,glide-induced DRX mechanism.A fundamental understanding of the role of deformation bands in texture modification can facilitate future alloy and process design.展开更多
In this paper, we demonstrated a simple method to create either a hydrophilic or hydrophobic surface. With femtosecond laser irradiation at different laser parameters, the water contact angle (WCA) on polystyrene’s s...In this paper, we demonstrated a simple method to create either a hydrophilic or hydrophobic surface. With femtosecond laser irradiation at different laser parameters, the water contact angle (WCA) on polystyrene’s surface can be modified to either 12.7° or 156.2° from its original WCA of 88.2°. With properly spaced micro-pits created, the surface became hydrophilic probably due to the spread of the water droplets into the micro-pits. While with properly spaced micro-grooves created, the surface became rough and more hydrophobic. We investigated the effect of laser parameters on WCAs and analyzed the laser-treated surface roughness, profiles and chemical bonds by surface profilometer, scanning electron microscope (SEM) and X-ray photoelectron spectroscopy (XPS). For the laser-treated surface with low roughness, the polar (such as C—O, C=O, and O—C=O bonds) and non-polar (such as C—C or C—H bonds) groups were found to be responsible for the wettability changes. While for a rough surface, the surface roughness or the surface topography structure played a more significant role in the changes of the surface WCA. The mechanisms involved in the laser surface wettability modification process were discussed.展开更多
基金by the Deutsche Forschungsgemeinschaft(DFG)through projects 420149269,394480829as part of the CRC1394“Structural and Chemical Atomic Complexity-From Defect Phase Diagrams to Material Properties”(project 409476157).
文摘Dynamic recrystallization(DRX)in inhomogeneous deformation zones,such as grain boundaries,shear bands,and deformation bands,is critical for texture modification in magnesium alloys during deformation at elevated temperatures.This study investigates the DRX mechanisms in AZWX3100 magnesium alloy under plane strain compression at 200℃.Microstructural analysis revealed necklace-type DRX accompanied by evidence of local grain boundary bulging.Additionally,ribbons of recrystallized grains were observed withinfine deformation bands,aligned with theoretical pyramidal I and II slip traces derived from the matrix.The distribution of local misorientation within the deformed microstructure demonstrated a clear association between deformation bands and localized strain.Dislocation analysis of lamellar specimens extracted from two pyramidal slip bands revealed<c+a>dislocations,indicating a connection between<c+a>slip activation and the formation of deformation bands.Crystal plasticity simulations suggest that the orientation of deformation bands is responsible for the unique recrystallization texture of the DRX grains within these bands.The texture characteristics imply a progressive,glide-induced DRX mechanism.A fundamental understanding of the role of deformation bands in texture modification can facilitate future alloy and process design.
文摘In this paper, we demonstrated a simple method to create either a hydrophilic or hydrophobic surface. With femtosecond laser irradiation at different laser parameters, the water contact angle (WCA) on polystyrene’s surface can be modified to either 12.7° or 156.2° from its original WCA of 88.2°. With properly spaced micro-pits created, the surface became hydrophilic probably due to the spread of the water droplets into the micro-pits. While with properly spaced micro-grooves created, the surface became rough and more hydrophobic. We investigated the effect of laser parameters on WCAs and analyzed the laser-treated surface roughness, profiles and chemical bonds by surface profilometer, scanning electron microscope (SEM) and X-ray photoelectron spectroscopy (XPS). For the laser-treated surface with low roughness, the polar (such as C—O, C=O, and O—C=O bonds) and non-polar (such as C—C or C—H bonds) groups were found to be responsible for the wettability changes. While for a rough surface, the surface roughness or the surface topography structure played a more significant role in the changes of the surface WCA. The mechanisms involved in the laser surface wettability modification process were discussed.
