Near-αtitanium alloy and Ti_(2)AlNb alloy powders premixed with different proportions were prepared on the near-αtitanium alloy substrate by laser deposition technique,and the microstructure characteristics were ana...Near-αtitanium alloy and Ti_(2)AlNb alloy powders premixed with different proportions were prepared on the near-αtitanium alloy substrate by laser deposition technique,and the microstructure characteristics were analyzed and discussed.Results show that numerous river-like sub-grain structures are formed inside the equiaxed B2 grains of the laser-deposited premixed titanium alloy powders with the proportion of Ti_(2)AlNb above 40wt%,whereas the needle-like structure within coarse columnarβgrains exist with the proportion of Ti_(2)AlNb below 40wt%.It is noteworthy that the decrease in laser power and scanning speed can accelerate the formation of sub-grain structures.Based on the analysis of experimental results,it can be inferred that the formation of sub-grain structure not only is related to the precipitation of O phase due to composition micro-segregation at sub-grain boundaries,but also is inseparable from the stacking faults caused by the internal stress during the laser deposition.展开更多
X-ray diffraction(XRD),scanning electron microscopy(SEM),energy-dispersive spectroscopy(EDS),electron backscatter diffraction(EBSD),and transmission electron microscopy(TEM)were used to systematically investigate the ...X-ray diffraction(XRD),scanning electron microscopy(SEM),energy-dispersive spectroscopy(EDS),electron backscatter diffraction(EBSD),and transmission electron microscopy(TEM)were used to systematically investigate the impact of rapid cold stamping on microstructural evolution and mechanical properties of spray-formed Al-Zn-Mg-Cu alloys under ambient conditions.The results reveal that the dislocation density increases with successive cold stamping passes,the volume fraction of the secondary phase(Mg(Zn,Cu,Al)_(2))increases from 15.64% to 23.94%,and the average size decreases from 1.41 to 0.75μm.The pinning effect of the secondary phases on dislocations promotes a significant transformation from low-angle grain boundaries to high-angle grain boundaries,resulting in the average grain size decreasing from 5.75 to 0.97μm.The strength and hardness of the samples increase with successive cold stamping passes,which is attributed to the synergistic effects of dislocation strengthening,grain boundary strengthening,and secondary phase strengthening.展开更多
基金National Natural Science Foundation of China(51974259)Xi'an Municipal Bureau of Science and Technology(21ZCZZHXJS-QCY6-0008)Industry-Academic Cooperation Project of Aero Engine Corporation of China(HFZL2020CXY021)。
文摘Near-αtitanium alloy and Ti_(2)AlNb alloy powders premixed with different proportions were prepared on the near-αtitanium alloy substrate by laser deposition technique,and the microstructure characteristics were analyzed and discussed.Results show that numerous river-like sub-grain structures are formed inside the equiaxed B2 grains of the laser-deposited premixed titanium alloy powders with the proportion of Ti_(2)AlNb above 40wt%,whereas the needle-like structure within coarse columnarβgrains exist with the proportion of Ti_(2)AlNb below 40wt%.It is noteworthy that the decrease in laser power and scanning speed can accelerate the formation of sub-grain structures.Based on the analysis of experimental results,it can be inferred that the formation of sub-grain structure not only is related to the precipitation of O phase due to composition micro-segregation at sub-grain boundaries,but also is inseparable from the stacking faults caused by the internal stress during the laser deposition.
基金supported by the National Natural Science Foundation of China(No.52271177).
文摘X-ray diffraction(XRD),scanning electron microscopy(SEM),energy-dispersive spectroscopy(EDS),electron backscatter diffraction(EBSD),and transmission electron microscopy(TEM)were used to systematically investigate the impact of rapid cold stamping on microstructural evolution and mechanical properties of spray-formed Al-Zn-Mg-Cu alloys under ambient conditions.The results reveal that the dislocation density increases with successive cold stamping passes,the volume fraction of the secondary phase(Mg(Zn,Cu,Al)_(2))increases from 15.64% to 23.94%,and the average size decreases from 1.41 to 0.75μm.The pinning effect of the secondary phases on dislocations promotes a significant transformation from low-angle grain boundaries to high-angle grain boundaries,resulting in the average grain size decreasing from 5.75 to 0.97μm.The strength and hardness of the samples increase with successive cold stamping passes,which is attributed to the synergistic effects of dislocation strengthening,grain boundary strengthening,and secondary phase strengthening.
