With the increasing complexity of the current electromagnetic environment,excessive microwave radi-ation not only does harm to human health but also forms various electromagnetic interference to so-phisticated electro...With the increasing complexity of the current electromagnetic environment,excessive microwave radi-ation not only does harm to human health but also forms various electromagnetic interference to so-phisticated electronic instruments.Therefore,the design and preparation of electromagnetic absorbing composites represent an efficient approach to mitigate the current hazards of electromagnetic radiation.However,traditional electromagnetic absorbers are difficult to satisfy the demands of actual utilization in the face of new challenges,and emerging absorbents have garnered increasing attention due to their structure and performance-based advantages.In this review,several emerging composites of Mxene-based,biochar-based,chiral,and heat-resisting are discussed in detail,including their synthetic strategy,structural superiority and regulation method,and final optimization of electromagnetic absorption ca-pacity.These insights provide a comprehensive reference for the future development of new-generation electromagnetic-wave absorption composites.Moreover,the potential development directions of these emerging absorbers have been proposed as well.展开更多
Metal composites produced through the liquid metal dealloying(LMD)process feature an advanced matrix-matrix composite structure,where two metallic materials form a continuous,three-dimensional interconnected network.T...Metal composites produced through the liquid metal dealloying(LMD)process feature an advanced matrix-matrix composite structure,where two metallic materials form a continuous,three-dimensional interconnected network.This study investigates the effects of Ti Cu precursor compositions on dealloying behavior and microstructural evolution in liquid Mg,using Ti_(50)Cu_(50)and Ti_(30)Cu_(70)precursors.The initial microstructure of the precursor significantly influences dealloying kinetics and phase transitions.The single-phase Ti_(50)Cu_(50)precursor exhibits a faster initial dealloying rate due to its homogeneous structure,yet complete dealloying requires 90 min.In contrast,the dualphase Ti_(30)Cu_(70)precursor achieves complete dealloying in 30 min,demonstrating the impact of a higher Cu concentration on accelerating the process kinetics.Additionally,the study explores the coarsening behavior and hardness variations during the LMD process,along with the microstructural characteristics of Mg-Ti composites fabricated from these two precursors.The findings highlight the critical role of precursor composition in tailoring the microstructure and properties of Mg-Ti composites produced through the LMD process,demonstrating its potential for advanced composite material manufacturing.展开更多
Brazing filler metals are widely applied,which serve as an industrial adhesive in the joining of dissimilar structures.With the continuous emergence of new structures and materials,the demand for novel brazing filler ...Brazing filler metals are widely applied,which serve as an industrial adhesive in the joining of dissimilar structures.With the continuous emergence of new structures and materials,the demand for novel brazing filler metals is ever-increasing.It is of great significance to investigate the optimized composition design methods and to establish systematic design guidelines for brazing filler metals.This study elucidated the fundamental rules for the composition design of brazing filler metals from a three-dimensional perspective encompassing the basic properties of applied brazing filler metals,formability and processability,and overall cost.The basic properties of brazing filler metals refer to their mechanical properties,physicochemical properties,electromagnetic properties,corrosion resistance,and the wettability and fluidity during brazing.The formability and processability of brazing filler metals include the processes of smelting and casting,extrusion,rolling,drawing and ring-making,as well as the processes of granulation,powder production,and the molding of amorphous and microcrystalline structures.The cost of brazing filler metals corresponds to the sum of materials value and manufacturing cost.Improving the comprehensive properties of brazing filler metals requires a comprehensive and systematic consideration of design indicators.Highlighting the unique characteristics of brazing filler metals should focus on relevant technical indicators.Binary or ternary eutectic structures can effectively enhance the flow spreading ability of brazing filler metals,and solid solution structures contribute to the formability.By employing the proposed design guidelines,typical Ag based,Cu based,Zn based brazing filler metals,and Sn based solders were designed and successfully applied in major scientific and engineering projects.展开更多
This study proposes a pre-strain optimization strategy for carbon fiber structural lithium-ion battery(SLIB) composites to inhibit the interfacial debonding between carbon fibers and solid-state electrolytes due to fi...This study proposes a pre-strain optimization strategy for carbon fiber structural lithium-ion battery(SLIB) composites to inhibit the interfacial debonding between carbon fibers and solid-state electrolytes due to fiber lithiation. Through an analytical shear-lag model and finite element simulations, it is demonstrated that applying tensile pre-strain to carbon fibers before electrode assembly effectively reduces the interfacial shear stress, thereby suppressing debonding. However, the excessive pre-strain can induce the interfacial damage in the unlithiated state, necessitating careful control of the pre-strain within a feasible range. This range is influenced by electrode material properties and geometric parameters. Specifically, the electrodes with the higher solid-state electrolyte elastic modulus and larger electrolyte volume fraction exhibit more significant interfacial damage, making pre-strain application increasingly critical. However, these conditions also impose stricter constraints on the feasible pre-strain range. By elucidating the interplay between pre-strain, material properties, and geometric factors, this study provides valuable insights for optimizing the design of carbon fiber SLIBs.展开更多
Fatigue damage is a primary contributor to the failure of composite structures,underscoring the critical importance of monitoring its progression to ensure structural safety.This paper introduces an innovative approac...Fatigue damage is a primary contributor to the failure of composite structures,underscoring the critical importance of monitoring its progression to ensure structural safety.This paper introduces an innovative approach to fatigue damage monitoring in composite structures,leveraging a hybrid methodology that integrates the Whale Optimization Algorithm(WOA)-Backpropagation(BP)neural network with an ultrasonic guided wave feature selection algorithm.Initially,a network of piezoelectric ceramic sensors is employed to transmit and capture ultrasonic-guided waves,thereby establishing a signal space that correlates with the structural condition.Subsequently,the Relief-F algorithm is applied for signal feature extraction,culminating in the formation of a feature matrix.This matrix is then utilized to train the WOA-BP neural network,which optimizes the fatigue damage identification model globally.The proposed model’s efficacy in quantifying fatigue damage is tested against fatigue test datasets,with its performance benchmarked against the traditional BP neural network algorithm.The findings demonstrate that the WOA-BP neural network model not only surpasses the BP model in predictive accuracy but also exhibits enhanced global search capabilities.The effect of different sensor-receiver path signals on the model damage recognition results is also discussed.The results of the discussion found that the path directly through the damaged area is more accurate in modeling damage recognition compared to the path signals away from the damaged area.Consequently,the proposed monitoring method in the fatigue test dataset is adept at accurately tracking and recognizing the progression of fatigue damage.展开更多
The Bayan Har block,one of China's most seismically active regions,has experienced multiple major earthquakes(≥M 7.0)in recent years.It is a key area for investigating the interactions between the Qinghai-Xizang(...The Bayan Har block,one of China's most seismically active regions,has experienced multiple major earthquakes(≥M 7.0)in recent years.It is a key area for investigating the interactions between the Qinghai-Xizang(Qingzang)Plateau and adjacent blocks,plateau uplift,and strong earthquake mechanisms.P-wave velocity and crustal composition provide key constraints on the properties of distinct tectonic units and their evolutionary modification processes.Based on the results of 8 Deep Seismic Sounding(DSS)profiles completed in the Bayan Har block and surrounding areas over the past 20 years,We constructed one-dimensional P-wave velocity models for the crust of Bayan Har block,Qilian fold belt,Qinling fold belt,Alxa block,Ordos block and Sichuan basin.Furthermore,crustal composition models for different tectonic units were established based on these results.The results reveal that the crustal thickness of the Bayan Har block gradually decreases towards the NNE,NE,and SE directions,while the average crustal velocity increases correspondingly.The felsic layer in the crust accounts for more than half of the total crustal thickness.The mafic content within the crust of different tectonic units exhibits notable variations,which may reflect that the Bayan Har block,Qilian fold belt,and Qinling fold belt have experienced more intensive lithospheric evolution processes compared to Ordos basin and Sichuan basin.The seismicity distribution in this region is significantly controlled by crustal velocity and composition heterogeneity across the Bayan Har block and adjacent areas,which demonstrates that earthquakes within and around the Bayan Har block exhibit both high frequency and larger magnitudes.These seismic characteristics primarily result from intense crustal stress accumulation and release during the outward expansion of the Qingzang Plateau.展开更多
In the fabrication and monitoring of parts in composite structures,which are being used more and more in a variety of engineering applications,the prediction and fatigue failure detection in composite materials is a d...In the fabrication and monitoring of parts in composite structures,which are being used more and more in a variety of engineering applications,the prediction and fatigue failure detection in composite materials is a difficult problem.This difficulty arises from several factors,such as the lack of a comprehensive investigation of the fatigue failure phenomena,the lack of a well-defined fatigue damage theory used for fatigue damage prediction,and the inhomogeneity of composites because of their multiple internal borders.This study investigates the fatigue behavior of carbon fiber reinforced with epoxy(CFRE)laminated composite plates under spectrum loading utilizing a uniqueDeep LearningNetwork consisting of a convolutional neural network(CNN).Themethod includes establishing Finite Element Model(FEM)in a plate model under a spectrum fatigue loading.Then,a CNN is trained for fatigue behavior prediction.The training phase produces promising results,showing the model’s performance with 94.21%accuracy,92.63%regression,and 91.55%F-score.To evaluate the model’s reliability,a comparison is made between fatigue data from the CNN and the FEM.It was found that the error band for this comparison is less than 0.3878MPa,affirming the accuracy and reliability of the proposed technique.The proposed method results converge with available experimental results in the literature,thus,the study suggests the broad applicability of this method to other different composite structures.展开更多
To mitigate secondary electromagnetic pollution,there is an urgent need to develop absorption-dominant electromagnetic interference(EMI)shielding materials with low density,reduced thickness,lightweight construction,f...To mitigate secondary electromagnetic pollution,there is an urgent need to develop absorption-dominant electromagnetic interference(EMI)shielding materials with low density,reduced thickness,lightweight construction,flexibility,exceptional mechanical strength,and superior electrothermal and photothermal properties,particularly for flexible and wearable electronics.In this regard,we designed an absorption-based composite film comprising carbon nanotubes(CNT)and α-Fe_(2)O_(3),featuring a CNT layer sandwiched between twoα-Fe_(2)O_(3)layers on the upper and lower surfaces.This composite film was fabricated through an electrodeposition process followed by a thermal annealing procedure to achieve enhanced EMI shielding performance along with improved electrothermal and photothermal properties.The strategically designed sandwich structure allows the rough surface of the upper α-Fe_(2)O_(3)layer to not only improve the impedance mismatch between free space and the composite film,facilitating the penetration of incident electromagnetic(EM)waves into the film and promoting increased EM absorption rather than reflection,but also to enhance electrical conductivity,thereby improving electron mobility and density.Consequently,the average total shielding effectiveness(SE)of the CNT/Fe_(16)-300 composite demonstrates remarkable EMI shielding effectiveness(EMI SE:56.8 dB).Furthermore,the alteration in the absorption-to-reflection ratio(A/R)signifies a transition in the EMI shielding mechanism from reflection(0.69 for the pristine CNT film)to absorption(1.86 for the CNT/Fe_(16)-300)with the incremental deposition of α-Fe_(2)O_(3)nanoparticles.This work presents a feasible manufacturing approach for developing composite films with a sandwich structure that exhibits absorption-dominant EMI shielding capabilities,contributing to advancements in thermal management and multifunctional electromagnetic shielding applications.展开更多
With vigorous developments in nanotechnology,the elaborate regulation of microstructure shows attractive potential in the design of electromagnetic wave absorbers.Herein,a hierarchical porous structure and composite h...With vigorous developments in nanotechnology,the elaborate regulation of microstructure shows attractive potential in the design of electromagnetic wave absorbers.Herein,a hierarchical porous structure and composite heterogeneous interface are constructed successfully to optimize the electromagnetic loss capacity.The macro–micro-synergistic graphene aerogel formed by the ice template‑assisted 3D printing strategy is cut by silicon carbide nanowires(SiC_(nws))grown in situ,while boron nitride(BN)interfacial structure is introduced on graphene nanoplates.The unique composite structure forces multiple scattering of incident EMWs,ensuring the combined effects of interfacial polarization,conduction networks,and magnetic-dielectric synergy.Therefore,the as-prepared composites present a minimum reflection loss value of−37.8 dB and a wide effective absorption bandwidth(EAB)of 9.2 GHz(from 8.8 to 18.0 GHz)at 2.5 mm.Besides,relying on the intrinsic high-temperature resistance of SiC_(nws) and BN,the EAB also remains above 5.0 GHz after annealing in air environment at 600℃ for 10 h.展开更多
As the proportion of composite materials used in aircraft continues to increase, the electromagnetic Shielding Effectiveness (SE) of these materials becomes a critical factor in the electromagnetic safety design of ai...As the proportion of composite materials used in aircraft continues to increase, the electromagnetic Shielding Effectiveness (SE) of these materials becomes a critical factor in the electromagnetic safety design of aircraft structures. The assessment of electromagnetic SE for Slotted Composite Structures(SCSs) is particularly challenging due to their complex geometries and there remains a lack of suitable models for accurately predicting the SE performance of these intricate configurations. To address this issue, this paper introduces SCS-Net, a Deep Neural Network (DNN) method designed to accurately predict the SE of SCS. This method considers the impacts of various structural parameters, material properties and incident wave parameters on the SE of SCSs. In order to better model the SCS, an improved Nicolson-Ross-Weir (NRW) method is introduced in this paper to provide an equivalent flat structure for the SCS and to calculate the electromagnetic parameters of the equivalent structure. Additionally, the prediction of SE via DNNs is limited by insufficient test data, which hinders support for large-sample training. To address the issue of limited measured data, this paper develops a Measurement-Computation Fusion (MCF) dataset construction method. The predictions based on the simulation results show that the proposed method maintains an error of less than 0.07 dB within the 8–10 GHz frequency range. Furthermore, a new loss function based on the weighted L1-norm is established to improve the prediction accuracy for these parameters. Compared with traditional loss functions, the new loss function reduces the maximum prediction error for equivalent electromagnetic parameters by 47%. This method significantly improves the prediction accuracy of SCS-Net for measured data, with a maximum improvement of 23.88%. These findings demonstrate that the proposed method enables precise SE prediction and design for composite structures while reducing the number of test samples needed.展开更多
Integrating a heterogeneous structure can significantly enhance the strength-ductility synergy of composites.However,the relationship between hetero-deformation induced(HDI)strain hardening and dislocation activity ca...Integrating a heterogeneous structure can significantly enhance the strength-ductility synergy of composites.However,the relationship between hetero-deformation induced(HDI)strain hardening and dislocation activity caused by heterogeneous structures in the magnesium matrix composite remains unclear.In this study,a dual-heterogeneous TiC/AZ61 composite exhibits significantly improved plastic elongation(PEL)by nearly one time compared to uniform FG composite,meanwhile maintaining a high strength(UTS:417 MPa).This is because more severe deformation inhomogeneity in heterogeneous structure leads to more geometrically necessary dislocations(GNDs)accumulation and stronger HDI stress,resulting in higher HDI hardening compared to FG and CG composites.During the early stage of plastic deformation,the pile-up types of GND in the FG zone and CG zone are significantly different.GNDs tend to form substructures in the FG zone instead of the CG zone.They only accumulate at grain boundaries of the CG region,thereby leading to obviously increased back stress in the CG region.In the late deformation stage,the elevated HDI stress activates the new〈c+a〉dislocations in the CG region,resulting in dislocation entanglements and even the formation of substructures,further driving the high hardening in the heterogeneous composite.However,For CG composite,〈c+a〉dislocations are not activated even under large plastic strains,and only〈a〉dislocations pile up at grain boundaries and twin boundaries.Our work provides an in-depth understanding of dislocation variation and HDI hardening in heterogeneous magnesium-based composites.展开更多
Despite the presence of Li F components in the solid electrolyte interphase(SEI)formed on the graphite anode surface by conventional electrolyte,these Li F components primarily exist in an amorphous state,rendering th...Despite the presence of Li F components in the solid electrolyte interphase(SEI)formed on the graphite anode surface by conventional electrolyte,these Li F components primarily exist in an amorphous state,rendering them incapable of effectively inhibiting the exchange reaction between lithium ions and transition metal ions in the electrolyte.Consequently,nearly all lithium ions within the SEI film are replaced by transition metal ions,resulting in an increase in interphacial impedance and a decrease in stability.Herein,we demonstrate that the SEI film,constructed by fluoroethylene carbonate(FEC)additive rich in crystalline Li F,effectively inhibits the undesired Li^(+)/Co^(2+)ion exchange reaction,thereby suppressing the deposition of cobalt compounds and metallic cobalt.Furthermore,the deposited cobalt compounds exhibit enhanced structural stability and reduced catalytic activity with minimal impact on the interphacial stability of the graphite anode.Our findings reveal the crucial influence of SEI film composition and structure on the deposition and hazards associated with transition metal ions,providing valuable guidance for designing next-generation electrolytes.展开更多
The damage distribution of the same type of aircraft in similar service environments should be similar. Based on this assumption, to perform the maintenance and repair of aircraft composite structures, the damage of c...The damage distribution of the same type of aircraft in similar service environments should be similar. Based on this assumption, to perform the maintenance and repair of aircraft composite structures, the damage of composite structures in a certain type of aircraft were investigated. The time-varying damage distribution model was established and verified based on the damage of a 16-aircraft fleet. The results show that the quantitative proportions of structural damage are 74% for skin delamination, 22% for stringer delamination and 3% for stringer-skin interface debonding. The amount of structural damages increases linearly with service time while the proportion of different damages does not change. As the service time increases, the geometric parameter distribution of damage for the same type of aircraft gradually converges, which can be approximated using the same function. There are certain differences in the proportion and geometric parameter distribution of damages among different components and locations, and the differences do not change over time.展开更多
The compression and energy absorption properties of foam geopolymers increase stress wave attenuation under explosion impacts,reducing the vibration effect on the structure.Explosion tests were conducted using several...The compression and energy absorption properties of foam geopolymers increase stress wave attenuation under explosion impacts,reducing the vibration effect on the structure.Explosion tests were conducted using several composite structure models,including a concrete lining structure(CLS)without foam geopolymer and six foam geopolymer composite structures(FGCS)with different backfill parameters,to study the dynamic response and wave dissipation mechanisms of FGCS under explosive loading.Pressure,strain,and vibration responses at different locations were synchronously tested.The damage modes and dynamic responses of different models were compared,and how wave elimination and energy absorption efficiencies were affected by foam geopolymer backfill parameters was analyzed.The results showed that the foam geopolymer absorbed and dissipated the impact energy through continuous compressive deformation under high strain rates and dynamic loading,reducing the strain in the liner structure by 52%and increasing the pressure attenuation rate by 28%.Additionally,the foam geopolymer backfill reduced structural vibration and liner deformation,with the FGCS structure showing 35%less displacement and 70%less acceleration compared to the CLS.The FGCS model with thicker,less dense foam geopolymer backfill,having more pores and higher porosity,demonstrated better compression and energy absorption under dynamic impact,increasing stress wave attenuation efficiency.By analyzing the stress wave propagation and the compression characteristics of the porous medium,it was concluded that the stress transfer ratio of FGCS-ρ-579 was 77%lower than that of CLS,and the transmitted wave energy was 90%lower.The results of this study provide a scientific basis for optimizing underground composite structure interlayer parameters.展开更多
The emerging interfacial polarization strategy exhibits applicative potential in piezoelectric enhancement.However,there is an ongoing effort to address the inherent limitations arising from charge bridging phenomena ...The emerging interfacial polarization strategy exhibits applicative potential in piezoelectric enhancement.However,there is an ongoing effort to address the inherent limitations arising from charge bridging phenomena and stochastic interface disorder that plague the improvement of piezoelectric performance.Here,we report a dual structure reinforced MXene/PVDF-TrFE piezoelectric composite,whose piezoelectricity is enhanced under the coupling effect of interfacial polarization and structural design.Synergistically,molecular dynamics simulations,density functional theory calculations and experimental validation revealed the details of interfacial interactions,which promotes the net spontaneous polarization of PVDF-TrFE from the 0.56 to 31.41 Debye.The oriented MXene distribution and porous structure not only tripled the piezoelectric response but also achieved an eightfold increase in sensitivity within the low-pressure region,along with demonstrating cyclic stability exceeding 20,000 cycles.The properties reinforcement originating from dual structure is elucidated through the finite element simulation and experimental validation.Attributed to the excellent piezoelectric response and deep learning algorithm,the sensor can effectively recognize the signals of artery pulse and finger flexion.Finally,a 3×3 sensor array is fabricated to monitor the pressure distribution wirelessly.This study provides an innovative methodology for reinforcing interfacial polarized piezoelectric materials and insight into structural designs.展开更多
Flow boiling in open microchannels offers highly efficient heat transfer performance and has attracted increasing attention in the fields of heat transfer and thermalmanagement of electronic devices in recent years.Ho...Flow boiling in open microchannels offers highly efficient heat transfer performance and has attracted increasing attention in the fields of heat transfer and thermalmanagement of electronic devices in recent years.However,the continuous rise in power density of electronic components imposesmore stringent requirements on the heat transfer capability of microchannel flow boiling.HFE-7100,a dielectric coolant with favorable thermophysical properties,has become a focal point of research for enhancing flow boiling performance in open microchannels.The flow boiling heat transfer performance ofHFE-7100 was investigated in this study by fabricating micro-nano composite structures on the bottom surface of open microchannels using laser ablation technology.Based on visualization results,a comparative analysis was conducted on the bubble dynamics and flow pattern characteristics of HFE-7100 flow boiling in micronano structured open microchannels(MNSOMC)and smooth-surface open microchannels(SSOMC),to elucidate the enhancement mechanism of micro-nano structures on flow boiling heat transfer in open microchannels.The results indicate that the surface structures and strong wettability of MNSOMC accelerated bubble nucleation and departure.Moreover,bubbles in the channel tended to coalesce along the flow direction,forming elongated slug bubbles with high aspect ratios,which enabled efficient thin film evaporation in conjunction with intense nucleate boiling,thereby significantly enhancing flow boiling heat transfer.Under the experimental conditions of this study,the maximum enhancements in the heat transfer coefficient(HTC)and critical heat flux(CHF)of HFE-7100 inMNSOMC were 33.4%and 133.1%,respectively,with the CHF reaching up to 1542.3 kW⋅m^(−2).Furthermore,due to the superior wettability and capillary wicking capability of the micro-nano composite structures,the significant enhancement in flow boiling heat transfer was achieved without incurring a noticeable pressure drop penalty.展开更多
In order to obtain high-density dual-scale ceramic particles(8.5 wt.%SiC+1.5 wt.%TiC)reinforced Al-Mg Sc-Zr composites with uniform microstructure,50 nm TiC and 7μm SiC particles were pre-dispersed into 15−53μm alum...In order to obtain high-density dual-scale ceramic particles(8.5 wt.%SiC+1.5 wt.%TiC)reinforced Al-Mg Sc-Zr composites with uniform microstructure,50 nm TiC and 7μm SiC particles were pre-dispersed into 15−53μm aluminum alloy powders by low-speed ball milling and mechanical mixing technology,respectively.Then,the effects of laser energy density,power and scanning rate on the density of the composites were investigated based on selective laser melting(SLM)technology.The effect of micron-sized SiC and nano-sized TiC particles on solidification structure,mechanical properties and fracture behaviors of the composites was revealed and analyzed in detail.Interfacial reaction and phase variations in the composites with varying reinforced particles were emphatically considered.Results showed that SiC-TiC particles could significantly improve forming quality and density of the SLMed composites,and the optimal relative density was up to 100%.In the process of laser melting,a strong chemical reaction occurs between SiC and aluminum matrix,and micron-scale acicular Al_(4)SiC_(4) bands were formed in situ.There was no interfacial reaction between TiC particles and aluminum matrix.TiC/Al semi-coherent interface had good bonding strength.Pinning effect of TiC particles in grain boundaries could prevent the equiaxial crystals from growing and transforming into columnar crystals,resulting in grain refinement.The optimal ultimate tensile strength(UTS),yield strength(YS),elongation(EL)and elastic modulus of the SiC-TiC/Al-Mg-Sc-Zr composite were~394 MPa,~262 MPa,~8.2%and~86 GPa,respectively.The fracture behavior of the composites included ductile fracture of Al matrix and brittle cleavage fracture of Al_(4)SiC_(4) phases.A large number of cross-distributed acicular Al_(4)SiC_(4) bands were the main factors leading to premature failure and fracture of SiC-TiC/Al-Mg-Sc-Zr composites.展开更多
Achieving high-level integration of composite micro-nano structures with different structural characteristics through a minimalist and universal process has long been the goal pursued by advanced manufacturing researc...Achieving high-level integration of composite micro-nano structures with different structural characteristics through a minimalist and universal process has long been the goal pursued by advanced manufacturing research but is rarely explored due to the absence of instructive mechanisms.Here,we revealed a controllable ultrafast laser-induced focal volume light field and experimentally succeeded in highly efficient one-step composite structuring in multiple transparent solids.A pair of spatially coupled twin periodic structures reflecting light distribution in the focal volume are simultaneously created and independently tuned by engineering ultrafast laser-matter interaction.We demonstrated that the generated composite micro-nano structures are applicable to multi-dimensional information integration,nonlinear diffractive elements,and multi-functional optical modulation.This work presents the experimental verification of highly universal all-optical fabrication of composite micro-nano structures with independent controllability in multiple degrees of freedom,expands the current cognition of ultrafast laser-based material modification in transparent solids,and establishes a new scientific aspect of strong-field optics,namely,focal volume optics for composite structuring transparent solids.展开更多
To assess the high-temperature creep properties of titanium matrix composites for aircraft skin,the TA15 alloy,TiB/TA15 and TiB/(TA15−Si)composites with network structure were fabricated using low-energy milling and v...To assess the high-temperature creep properties of titanium matrix composites for aircraft skin,the TA15 alloy,TiB/TA15 and TiB/(TA15−Si)composites with network structure were fabricated using low-energy milling and vacuum hot pressing sintering techniques.The results show that introducing TiB and Si can reduce the steady-state creep rate by an order of magnitude at 600℃ compared to the alloy.However,the beneficial effect of Si can be maintained at 700℃ while the positive effect of TiB gradually diminishes due to the pores near TiB and interface debonding.The creep deformation mechanism of the as-sintered TiB/(TA15−Si)composite is primarily governed by dislocation climbing.The high creep resistance at 600℃ can be mainly attributed to the absence of grain boundaryαphases,load transfer by TiB whisker,and the hindrance of dislocation movement by silicides.The low steady-state creep rate at 700℃ is mainly resulted from the elimination of grain boundaryαphases as well as increased dynamic precipitation of silicides andα_(2).展开更多
Bioinspired nacre-like structured high-density soft magnetic composites(SMCs)have been successfully constructed using flaky-Fe_(73.8)Si_(13.5)B_(8.7)Cu_(1)Nb_(3) powders in the supercooled liquid region(SCLR).These de...Bioinspired nacre-like structured high-density soft magnetic composites(SMCs)have been successfully constructed using flaky-Fe_(73.8)Si_(13.5)B_(8.7)Cu_(1)Nb_(3) powders in the supercooled liquid region(SCLR).These densely arranged particles with a consistent planar orientation significantly enhance the soft magnetic properties of SMCs,including high permeability and low magnetic losses.The internal structures of the composites and microstructure evolution of the flaky nanocrystalline particles during the hot-pressing process have been thoroughly studied.Moreover,systematic investigations into the effects of coatings and particle sizes on the maximum permeability and magnetic losses of the composites are conducted.The SMC prepared using the coated particles with a size of 0-100μm exhibits a high maximum perme-ability of 2170(at 1000 Hz)and low magnetic loss of 41.61 W kg^(-1)(at 1000 Hz and 1.0 T).The losses and permeability analysis reveal that the superior performance of these soft magnetic materials is attributed to their laminated structure,insulation coating,and the reduced planar demagnetizing factor.Compared to the traditional silicon steel,this novel SMCs exhibits high magnetic permeability and reduced magnetic losses at frequencies above 1000 Hz,which possess immense application potential within high-frequency electric machines.展开更多
基金supported by the Surface Project of Local De-velopment in Science and Technology Guided by Central Govern-ment(No.2021ZYD0041)the National Natural Science Founda-tion of China(Nos.52377026 and 52301192)+3 种基金the Natural Science Foundation of Shandong Province(No.ZR2019YQ24)the Taishan Scholars and Young Experts Program of Shandong Province(No.tsqn202103057)the Special Financial of Shandong Province(Struc-tural Design of High-efficiency Electromagnetic Wave-absorbing Composite Materials and Construction of Shandong Provincial Tal-ent Teams)the“Sanqin Scholars”Innovation Teams Project of Shaanxi Province(Clean Energy Materials and High-Performance Devices Innovation Team of Shaanxi Dongling Smelting Co.,Ltd.).
文摘With the increasing complexity of the current electromagnetic environment,excessive microwave radi-ation not only does harm to human health but also forms various electromagnetic interference to so-phisticated electronic instruments.Therefore,the design and preparation of electromagnetic absorbing composites represent an efficient approach to mitigate the current hazards of electromagnetic radiation.However,traditional electromagnetic absorbers are difficult to satisfy the demands of actual utilization in the face of new challenges,and emerging absorbents have garnered increasing attention due to their structure and performance-based advantages.In this review,several emerging composites of Mxene-based,biochar-based,chiral,and heat-resisting are discussed in detail,including their synthetic strategy,structural superiority and regulation method,and final optimization of electromagnetic absorption ca-pacity.These insights provide a comprehensive reference for the future development of new-generation electromagnetic-wave absorption composites.Moreover,the potential development directions of these emerging absorbers have been proposed as well.
基金supported by the National Research Foundation of Korea(NRF)grants funded by the Korea government(MSIT)(Nos.RS-2024–00351052 and RS-2024–00450561)。
文摘Metal composites produced through the liquid metal dealloying(LMD)process feature an advanced matrix-matrix composite structure,where two metallic materials form a continuous,three-dimensional interconnected network.This study investigates the effects of Ti Cu precursor compositions on dealloying behavior and microstructural evolution in liquid Mg,using Ti_(50)Cu_(50)and Ti_(30)Cu_(70)precursors.The initial microstructure of the precursor significantly influences dealloying kinetics and phase transitions.The single-phase Ti_(50)Cu_(50)precursor exhibits a faster initial dealloying rate due to its homogeneous structure,yet complete dealloying requires 90 min.In contrast,the dualphase Ti_(30)Cu_(70)precursor achieves complete dealloying in 30 min,demonstrating the impact of a higher Cu concentration on accelerating the process kinetics.Additionally,the study explores the coarsening behavior and hardness variations during the LMD process,along with the microstructural characteristics of Mg-Ti composites fabricated from these two precursors.The findings highlight the critical role of precursor composition in tailoring the microstructure and properties of Mg-Ti composites produced through the LMD process,demonstrating its potential for advanced composite material manufacturing.
基金National Natural Science Foundation of China(U22A20191)。
文摘Brazing filler metals are widely applied,which serve as an industrial adhesive in the joining of dissimilar structures.With the continuous emergence of new structures and materials,the demand for novel brazing filler metals is ever-increasing.It is of great significance to investigate the optimized composition design methods and to establish systematic design guidelines for brazing filler metals.This study elucidated the fundamental rules for the composition design of brazing filler metals from a three-dimensional perspective encompassing the basic properties of applied brazing filler metals,formability and processability,and overall cost.The basic properties of brazing filler metals refer to their mechanical properties,physicochemical properties,electromagnetic properties,corrosion resistance,and the wettability and fluidity during brazing.The formability and processability of brazing filler metals include the processes of smelting and casting,extrusion,rolling,drawing and ring-making,as well as the processes of granulation,powder production,and the molding of amorphous and microcrystalline structures.The cost of brazing filler metals corresponds to the sum of materials value and manufacturing cost.Improving the comprehensive properties of brazing filler metals requires a comprehensive and systematic consideration of design indicators.Highlighting the unique characteristics of brazing filler metals should focus on relevant technical indicators.Binary or ternary eutectic structures can effectively enhance the flow spreading ability of brazing filler metals,and solid solution structures contribute to the formability.By employing the proposed design guidelines,typical Ag based,Cu based,Zn based brazing filler metals,and Sn based solders were designed and successfully applied in major scientific and engineering projects.
基金supported by the National Natural Science Foundation of China(Nos.12172205,12072183,12102244,and 12472174)。
文摘This study proposes a pre-strain optimization strategy for carbon fiber structural lithium-ion battery(SLIB) composites to inhibit the interfacial debonding between carbon fibers and solid-state electrolytes due to fiber lithiation. Through an analytical shear-lag model and finite element simulations, it is demonstrated that applying tensile pre-strain to carbon fibers before electrode assembly effectively reduces the interfacial shear stress, thereby suppressing debonding. However, the excessive pre-strain can induce the interfacial damage in the unlithiated state, necessitating careful control of the pre-strain within a feasible range. This range is influenced by electrode material properties and geometric parameters. Specifically, the electrodes with the higher solid-state electrolyte elastic modulus and larger electrolyte volume fraction exhibit more significant interfacial damage, making pre-strain application increasingly critical. However, these conditions also impose stricter constraints on the feasible pre-strain range. By elucidating the interplay between pre-strain, material properties, and geometric factors, this study provides valuable insights for optimizing the design of carbon fiber SLIBs.
基金funded by the Key Program of the National Natural Science Foundation of China(U2341235)Youth Fund for Basic Research Program of Jiangnan University(JUSRP123003)+2 种基金Postgraduate Research&Practice Innovation Program of Jiangsu Province(SJCX23_1237)the National Key R&D Program of China(2018YFA0702800)Key Technologies R&D Program of CNBM(2023SJYL01).
文摘Fatigue damage is a primary contributor to the failure of composite structures,underscoring the critical importance of monitoring its progression to ensure structural safety.This paper introduces an innovative approach to fatigue damage monitoring in composite structures,leveraging a hybrid methodology that integrates the Whale Optimization Algorithm(WOA)-Backpropagation(BP)neural network with an ultrasonic guided wave feature selection algorithm.Initially,a network of piezoelectric ceramic sensors is employed to transmit and capture ultrasonic-guided waves,thereby establishing a signal space that correlates with the structural condition.Subsequently,the Relief-F algorithm is applied for signal feature extraction,culminating in the formation of a feature matrix.This matrix is then utilized to train the WOA-BP neural network,which optimizes the fatigue damage identification model globally.The proposed model’s efficacy in quantifying fatigue damage is tested against fatigue test datasets,with its performance benchmarked against the traditional BP neural network algorithm.The findings demonstrate that the WOA-BP neural network model not only surpasses the BP model in predictive accuracy but also exhibits enhanced global search capabilities.The effect of different sensor-receiver path signals on the model damage recognition results is also discussed.The results of the discussion found that the path directly through the damaged area is more accurate in modeling damage recognition compared to the path signals away from the damaged area.Consequently,the proposed monitoring method in the fatigue test dataset is adept at accurately tracking and recognizing the progression of fatigue damage.
基金supported by the National Key R&D Program of China(No.2023YFC3012002)the National Natural Science Foundation of China(42374073)。
文摘The Bayan Har block,one of China's most seismically active regions,has experienced multiple major earthquakes(≥M 7.0)in recent years.It is a key area for investigating the interactions between the Qinghai-Xizang(Qingzang)Plateau and adjacent blocks,plateau uplift,and strong earthquake mechanisms.P-wave velocity and crustal composition provide key constraints on the properties of distinct tectonic units and their evolutionary modification processes.Based on the results of 8 Deep Seismic Sounding(DSS)profiles completed in the Bayan Har block and surrounding areas over the past 20 years,We constructed one-dimensional P-wave velocity models for the crust of Bayan Har block,Qilian fold belt,Qinling fold belt,Alxa block,Ordos block and Sichuan basin.Furthermore,crustal composition models for different tectonic units were established based on these results.The results reveal that the crustal thickness of the Bayan Har block gradually decreases towards the NNE,NE,and SE directions,while the average crustal velocity increases correspondingly.The felsic layer in the crust accounts for more than half of the total crustal thickness.The mafic content within the crust of different tectonic units exhibits notable variations,which may reflect that the Bayan Har block,Qilian fold belt,and Qinling fold belt have experienced more intensive lithospheric evolution processes compared to Ordos basin and Sichuan basin.The seismicity distribution in this region is significantly controlled by crustal velocity and composition heterogeneity across the Bayan Har block and adjacent areas,which demonstrates that earthquakes within and around the Bayan Har block exhibit both high frequency and larger magnitudes.These seismic characteristics primarily result from intense crustal stress accumulation and release during the outward expansion of the Qingzang Plateau.
文摘In the fabrication and monitoring of parts in composite structures,which are being used more and more in a variety of engineering applications,the prediction and fatigue failure detection in composite materials is a difficult problem.This difficulty arises from several factors,such as the lack of a comprehensive investigation of the fatigue failure phenomena,the lack of a well-defined fatigue damage theory used for fatigue damage prediction,and the inhomogeneity of composites because of their multiple internal borders.This study investigates the fatigue behavior of carbon fiber reinforced with epoxy(CFRE)laminated composite plates under spectrum loading utilizing a uniqueDeep LearningNetwork consisting of a convolutional neural network(CNN).Themethod includes establishing Finite Element Model(FEM)in a plate model under a spectrum fatigue loading.Then,a CNN is trained for fatigue behavior prediction.The training phase produces promising results,showing the model’s performance with 94.21%accuracy,92.63%regression,and 91.55%F-score.To evaluate the model’s reliability,a comparison is made between fatigue data from the CNN and the FEM.It was found that the error band for this comparison is less than 0.3878MPa,affirming the accuracy and reliability of the proposed technique.The proposed method results converge with available experimental results in the literature,thus,the study suggests the broad applicability of this method to other different composite structures.
基金financially supported by the National Natural Science Foundation of China(Nos.52222202 and 51772310)Chinese Academy of Sciences Key Research Program of Frontier Sciences(No.QYZDY-SSWJSC031)Shanghai Pilot Program for Basic Research-Chinese Academy of Science,Shanghai Branch(No.JCYJ-SHFY-2021-001).
文摘To mitigate secondary electromagnetic pollution,there is an urgent need to develop absorption-dominant electromagnetic interference(EMI)shielding materials with low density,reduced thickness,lightweight construction,flexibility,exceptional mechanical strength,and superior electrothermal and photothermal properties,particularly for flexible and wearable electronics.In this regard,we designed an absorption-based composite film comprising carbon nanotubes(CNT)and α-Fe_(2)O_(3),featuring a CNT layer sandwiched between twoα-Fe_(2)O_(3)layers on the upper and lower surfaces.This composite film was fabricated through an electrodeposition process followed by a thermal annealing procedure to achieve enhanced EMI shielding performance along with improved electrothermal and photothermal properties.The strategically designed sandwich structure allows the rough surface of the upper α-Fe_(2)O_(3)layer to not only improve the impedance mismatch between free space and the composite film,facilitating the penetration of incident electromagnetic(EM)waves into the film and promoting increased EM absorption rather than reflection,but also to enhance electrical conductivity,thereby improving electron mobility and density.Consequently,the average total shielding effectiveness(SE)of the CNT/Fe_(16)-300 composite demonstrates remarkable EMI shielding effectiveness(EMI SE:56.8 dB).Furthermore,the alteration in the absorption-to-reflection ratio(A/R)signifies a transition in the EMI shielding mechanism from reflection(0.69 for the pristine CNT film)to absorption(1.86 for the CNT/Fe_(16)-300)with the incremental deposition of α-Fe_(2)O_(3)nanoparticles.This work presents a feasible manufacturing approach for developing composite films with a sandwich structure that exhibits absorption-dominant EMI shielding capabilities,contributing to advancements in thermal management and multifunctional electromagnetic shielding applications.
基金sponsored by National Natural Science Foundation of China(No.52302121,No.52203386)Shanghai Sailing Program(No.23YF1454700)+1 种基金Shanghai Natural Science Foundation(No.23ZR1472700)Shanghai Post-doctoral Excellent Program(No.2022664).
文摘With vigorous developments in nanotechnology,the elaborate regulation of microstructure shows attractive potential in the design of electromagnetic wave absorbers.Herein,a hierarchical porous structure and composite heterogeneous interface are constructed successfully to optimize the electromagnetic loss capacity.The macro–micro-synergistic graphene aerogel formed by the ice template‑assisted 3D printing strategy is cut by silicon carbide nanowires(SiC_(nws))grown in situ,while boron nitride(BN)interfacial structure is introduced on graphene nanoplates.The unique composite structure forces multiple scattering of incident EMWs,ensuring the combined effects of interfacial polarization,conduction networks,and magnetic-dielectric synergy.Therefore,the as-prepared composites present a minimum reflection loss value of−37.8 dB and a wide effective absorption bandwidth(EAB)of 9.2 GHz(from 8.8 to 18.0 GHz)at 2.5 mm.Besides,relying on the intrinsic high-temperature resistance of SiC_(nws) and BN,the EAB also remains above 5.0 GHz after annealing in air environment at 600℃ for 10 h.
基金supported by the National Natural Science Foundation of China(Nos.62101020 and 62141405)the Special Scientific Research Project of Civil Aircraft,China(No.MJZ5-2N22).
文摘As the proportion of composite materials used in aircraft continues to increase, the electromagnetic Shielding Effectiveness (SE) of these materials becomes a critical factor in the electromagnetic safety design of aircraft structures. The assessment of electromagnetic SE for Slotted Composite Structures(SCSs) is particularly challenging due to their complex geometries and there remains a lack of suitable models for accurately predicting the SE performance of these intricate configurations. To address this issue, this paper introduces SCS-Net, a Deep Neural Network (DNN) method designed to accurately predict the SE of SCS. This method considers the impacts of various structural parameters, material properties and incident wave parameters on the SE of SCSs. In order to better model the SCS, an improved Nicolson-Ross-Weir (NRW) method is introduced in this paper to provide an equivalent flat structure for the SCS and to calculate the electromagnetic parameters of the equivalent structure. Additionally, the prediction of SE via DNNs is limited by insufficient test data, which hinders support for large-sample training. To address the issue of limited measured data, this paper develops a Measurement-Computation Fusion (MCF) dataset construction method. The predictions based on the simulation results show that the proposed method maintains an error of less than 0.07 dB within the 8–10 GHz frequency range. Furthermore, a new loss function based on the weighted L1-norm is established to improve the prediction accuracy for these parameters. Compared with traditional loss functions, the new loss function reduces the maximum prediction error for equivalent electromagnetic parameters by 47%. This method significantly improves the prediction accuracy of SCS-Net for measured data, with a maximum improvement of 23.88%. These findings demonstrate that the proposed method enables precise SE prediction and design for composite structures while reducing the number of test samples needed.
基金support from the National Natural Science Foundation of China(No:52061040)China Postdoctoral Science Foundation(No:2021M692512)+1 种基金Opening Project of Material Corrosion and Protection Key Laboratory of Sichuan Province(No:2023CL01)Open Projects of Key Laboratory of Advanced Technologies of Materials,Ministry of Education China,Southwest Jiaotong University(No:KLATM202003).
文摘Integrating a heterogeneous structure can significantly enhance the strength-ductility synergy of composites.However,the relationship between hetero-deformation induced(HDI)strain hardening and dislocation activity caused by heterogeneous structures in the magnesium matrix composite remains unclear.In this study,a dual-heterogeneous TiC/AZ61 composite exhibits significantly improved plastic elongation(PEL)by nearly one time compared to uniform FG composite,meanwhile maintaining a high strength(UTS:417 MPa).This is because more severe deformation inhomogeneity in heterogeneous structure leads to more geometrically necessary dislocations(GNDs)accumulation and stronger HDI stress,resulting in higher HDI hardening compared to FG and CG composites.During the early stage of plastic deformation,the pile-up types of GND in the FG zone and CG zone are significantly different.GNDs tend to form substructures in the FG zone instead of the CG zone.They only accumulate at grain boundaries of the CG region,thereby leading to obviously increased back stress in the CG region.In the late deformation stage,the elevated HDI stress activates the new〈c+a〉dislocations in the CG region,resulting in dislocation entanglements and even the formation of substructures,further driving the high hardening in the heterogeneous composite.However,For CG composite,〈c+a〉dislocations are not activated even under large plastic strains,and only〈a〉dislocations pile up at grain boundaries and twin boundaries.Our work provides an in-depth understanding of dislocation variation and HDI hardening in heterogeneous magnesium-based composites.
基金supported by the National Natural Science Foundation of China(21972049,21573080)。
文摘Despite the presence of Li F components in the solid electrolyte interphase(SEI)formed on the graphite anode surface by conventional electrolyte,these Li F components primarily exist in an amorphous state,rendering them incapable of effectively inhibiting the exchange reaction between lithium ions and transition metal ions in the electrolyte.Consequently,nearly all lithium ions within the SEI film are replaced by transition metal ions,resulting in an increase in interphacial impedance and a decrease in stability.Herein,we demonstrate that the SEI film,constructed by fluoroethylene carbonate(FEC)additive rich in crystalline Li F,effectively inhibits the undesired Li^(+)/Co^(2+)ion exchange reaction,thereby suppressing the deposition of cobalt compounds and metallic cobalt.Furthermore,the deposited cobalt compounds exhibit enhanced structural stability and reduced catalytic activity with minimal impact on the interphacial stability of the graphite anode.Our findings reveal the crucial influence of SEI film composition and structure on the deposition and hazards associated with transition metal ions,providing valuable guidance for designing next-generation electrolytes.
文摘The damage distribution of the same type of aircraft in similar service environments should be similar. Based on this assumption, to perform the maintenance and repair of aircraft composite structures, the damage of composite structures in a certain type of aircraft were investigated. The time-varying damage distribution model was established and verified based on the damage of a 16-aircraft fleet. The results show that the quantitative proportions of structural damage are 74% for skin delamination, 22% for stringer delamination and 3% for stringer-skin interface debonding. The amount of structural damages increases linearly with service time while the proportion of different damages does not change. As the service time increases, the geometric parameter distribution of damage for the same type of aircraft gradually converges, which can be approximated using the same function. There are certain differences in the proportion and geometric parameter distribution of damages among different components and locations, and the differences do not change over time.
基金financially supported by the National Natural Science Foundation of China(Grant Nos.52378401,12202494)the Fundamental Research Funds for the Central Universities(Grant No.30922010918)。
文摘The compression and energy absorption properties of foam geopolymers increase stress wave attenuation under explosion impacts,reducing the vibration effect on the structure.Explosion tests were conducted using several composite structure models,including a concrete lining structure(CLS)without foam geopolymer and six foam geopolymer composite structures(FGCS)with different backfill parameters,to study the dynamic response and wave dissipation mechanisms of FGCS under explosive loading.Pressure,strain,and vibration responses at different locations were synchronously tested.The damage modes and dynamic responses of different models were compared,and how wave elimination and energy absorption efficiencies were affected by foam geopolymer backfill parameters was analyzed.The results showed that the foam geopolymer absorbed and dissipated the impact energy through continuous compressive deformation under high strain rates and dynamic loading,reducing the strain in the liner structure by 52%and increasing the pressure attenuation rate by 28%.Additionally,the foam geopolymer backfill reduced structural vibration and liner deformation,with the FGCS structure showing 35%less displacement and 70%less acceleration compared to the CLS.The FGCS model with thicker,less dense foam geopolymer backfill,having more pores and higher porosity,demonstrated better compression and energy absorption under dynamic impact,increasing stress wave attenuation efficiency.By analyzing the stress wave propagation and the compression characteristics of the porous medium,it was concluded that the stress transfer ratio of FGCS-ρ-579 was 77%lower than that of CLS,and the transmitted wave energy was 90%lower.The results of this study provide a scientific basis for optimizing underground composite structure interlayer parameters.
基金supported by the National Natural Science Foundation of China(No.52303328)the Postdoctoral Innovation Talents Support Program(No.BX20220257)the Sichuan Science and Technology Program(No.2023NSFSC0313).
文摘The emerging interfacial polarization strategy exhibits applicative potential in piezoelectric enhancement.However,there is an ongoing effort to address the inherent limitations arising from charge bridging phenomena and stochastic interface disorder that plague the improvement of piezoelectric performance.Here,we report a dual structure reinforced MXene/PVDF-TrFE piezoelectric composite,whose piezoelectricity is enhanced under the coupling effect of interfacial polarization and structural design.Synergistically,molecular dynamics simulations,density functional theory calculations and experimental validation revealed the details of interfacial interactions,which promotes the net spontaneous polarization of PVDF-TrFE from the 0.56 to 31.41 Debye.The oriented MXene distribution and porous structure not only tripled the piezoelectric response but also achieved an eightfold increase in sensitivity within the low-pressure region,along with demonstrating cyclic stability exceeding 20,000 cycles.The properties reinforcement originating from dual structure is elucidated through the finite element simulation and experimental validation.Attributed to the excellent piezoelectric response and deep learning algorithm,the sensor can effectively recognize the signals of artery pulse and finger flexion.Finally,a 3×3 sensor array is fabricated to monitor the pressure distribution wirelessly.This study provides an innovative methodology for reinforcing interfacial polarized piezoelectric materials and insight into structural designs.
基金funded by the National Natural Science Foundation of China(Grant No.52276047)the Open Fund of NationalKey Laboratory of SpacecraftThermal Control(Grant No.NKLST-JJ-202401011)the Beijing Municipal Science&Technology Commission(Grant No.Z231100006123010).
文摘Flow boiling in open microchannels offers highly efficient heat transfer performance and has attracted increasing attention in the fields of heat transfer and thermalmanagement of electronic devices in recent years.However,the continuous rise in power density of electronic components imposesmore stringent requirements on the heat transfer capability of microchannel flow boiling.HFE-7100,a dielectric coolant with favorable thermophysical properties,has become a focal point of research for enhancing flow boiling performance in open microchannels.The flow boiling heat transfer performance ofHFE-7100 was investigated in this study by fabricating micro-nano composite structures on the bottom surface of open microchannels using laser ablation technology.Based on visualization results,a comparative analysis was conducted on the bubble dynamics and flow pattern characteristics of HFE-7100 flow boiling in micronano structured open microchannels(MNSOMC)and smooth-surface open microchannels(SSOMC),to elucidate the enhancement mechanism of micro-nano structures on flow boiling heat transfer in open microchannels.The results indicate that the surface structures and strong wettability of MNSOMC accelerated bubble nucleation and departure.Moreover,bubbles in the channel tended to coalesce along the flow direction,forming elongated slug bubbles with high aspect ratios,which enabled efficient thin film evaporation in conjunction with intense nucleate boiling,thereby significantly enhancing flow boiling heat transfer.Under the experimental conditions of this study,the maximum enhancements in the heat transfer coefficient(HTC)and critical heat flux(CHF)of HFE-7100 inMNSOMC were 33.4%and 133.1%,respectively,with the CHF reaching up to 1542.3 kW⋅m^(−2).Furthermore,due to the superior wettability and capillary wicking capability of the micro-nano composite structures,the significant enhancement in flow boiling heat transfer was achieved without incurring a noticeable pressure drop penalty.
基金Project(2022J318)supported by the Natural Science Foundation of Ningbo,ChinaProject(2021A1515110525)supported by the Guangdong Basic and Applied Basic Research Foundation,ChinaProject(2022QN05023)supported by the Inner Mongolia Natural Science Foundation Youth Project,China。
文摘In order to obtain high-density dual-scale ceramic particles(8.5 wt.%SiC+1.5 wt.%TiC)reinforced Al-Mg Sc-Zr composites with uniform microstructure,50 nm TiC and 7μm SiC particles were pre-dispersed into 15−53μm aluminum alloy powders by low-speed ball milling and mechanical mixing technology,respectively.Then,the effects of laser energy density,power and scanning rate on the density of the composites were investigated based on selective laser melting(SLM)technology.The effect of micron-sized SiC and nano-sized TiC particles on solidification structure,mechanical properties and fracture behaviors of the composites was revealed and analyzed in detail.Interfacial reaction and phase variations in the composites with varying reinforced particles were emphatically considered.Results showed that SiC-TiC particles could significantly improve forming quality and density of the SLMed composites,and the optimal relative density was up to 100%.In the process of laser melting,a strong chemical reaction occurs between SiC and aluminum matrix,and micron-scale acicular Al_(4)SiC_(4) bands were formed in situ.There was no interfacial reaction between TiC particles and aluminum matrix.TiC/Al semi-coherent interface had good bonding strength.Pinning effect of TiC particles in grain boundaries could prevent the equiaxial crystals from growing and transforming into columnar crystals,resulting in grain refinement.The optimal ultimate tensile strength(UTS),yield strength(YS),elongation(EL)and elastic modulus of the SiC-TiC/Al-Mg-Sc-Zr composite were~394 MPa,~262 MPa,~8.2%and~86 GPa,respectively.The fracture behavior of the composites included ductile fracture of Al matrix and brittle cleavage fracture of Al_(4)SiC_(4) phases.A large number of cross-distributed acicular Al_(4)SiC_(4) bands were the main factors leading to premature failure and fracture of SiC-TiC/Al-Mg-Sc-Zr composites.
基金financially supported by the National Key Research and Development Program of China(No.2021YFB2802001)the National Natural Science Foundation of China(Grant Nos.12304349,U20A20211,62275233)the Postdoctoral Fellowship Program of CPSF(GZB20230628,GZC20241465)。
文摘Achieving high-level integration of composite micro-nano structures with different structural characteristics through a minimalist and universal process has long been the goal pursued by advanced manufacturing research but is rarely explored due to the absence of instructive mechanisms.Here,we revealed a controllable ultrafast laser-induced focal volume light field and experimentally succeeded in highly efficient one-step composite structuring in multiple transparent solids.A pair of spatially coupled twin periodic structures reflecting light distribution in the focal volume are simultaneously created and independently tuned by engineering ultrafast laser-matter interaction.We demonstrated that the generated composite micro-nano structures are applicable to multi-dimensional information integration,nonlinear diffractive elements,and multi-functional optical modulation.This work presents the experimental verification of highly universal all-optical fabrication of composite micro-nano structures with independent controllability in multiple degrees of freedom,expands the current cognition of ultrafast laser-based material modification in transparent solids,and establishes a new scientific aspect of strong-field optics,namely,focal volume optics for composite structuring transparent solids.
基金financially supported by the National Key R&D Program of China(No.2022YFB3707405)the National Natural Science Foundation of China(Nos.U22A20113,52171137,52071116)+1 种基金Heilongjiang Provincial Natural Science Foundation,China(No.TD2020E001)Heilongjiang Touyan Team Program,China.
文摘To assess the high-temperature creep properties of titanium matrix composites for aircraft skin,the TA15 alloy,TiB/TA15 and TiB/(TA15−Si)composites with network structure were fabricated using low-energy milling and vacuum hot pressing sintering techniques.The results show that introducing TiB and Si can reduce the steady-state creep rate by an order of magnitude at 600℃ compared to the alloy.However,the beneficial effect of Si can be maintained at 700℃ while the positive effect of TiB gradually diminishes due to the pores near TiB and interface debonding.The creep deformation mechanism of the as-sintered TiB/(TA15−Si)composite is primarily governed by dislocation climbing.The high creep resistance at 600℃ can be mainly attributed to the absence of grain boundaryαphases,load transfer by TiB whisker,and the hindrance of dislocation movement by silicides.The low steady-state creep rate at 700℃ is mainly resulted from the elimination of grain boundaryαphases as well as increased dynamic precipitation of silicides andα_(2).
基金supported by the National Natural Science Foundation of China(Grant No.52071294)the National Key Research and Development Program(Grant No.2022YFE0109800)the Natural Science Foundation of Zhejiang Province(Grant No.LY20E020015).
文摘Bioinspired nacre-like structured high-density soft magnetic composites(SMCs)have been successfully constructed using flaky-Fe_(73.8)Si_(13.5)B_(8.7)Cu_(1)Nb_(3) powders in the supercooled liquid region(SCLR).These densely arranged particles with a consistent planar orientation significantly enhance the soft magnetic properties of SMCs,including high permeability and low magnetic losses.The internal structures of the composites and microstructure evolution of the flaky nanocrystalline particles during the hot-pressing process have been thoroughly studied.Moreover,systematic investigations into the effects of coatings and particle sizes on the maximum permeability and magnetic losses of the composites are conducted.The SMC prepared using the coated particles with a size of 0-100μm exhibits a high maximum perme-ability of 2170(at 1000 Hz)and low magnetic loss of 41.61 W kg^(-1)(at 1000 Hz and 1.0 T).The losses and permeability analysis reveal that the superior performance of these soft magnetic materials is attributed to their laminated structure,insulation coating,and the reduced planar demagnetizing factor.Compared to the traditional silicon steel,this novel SMCs exhibits high magnetic permeability and reduced magnetic losses at frequencies above 1000 Hz,which possess immense application potential within high-frequency electric machines.