This study involved the development of an interpretable prediction framework to access the stretch formability of AZ31 magnesium alloys through the combination of the extreme gradient boosting(XGBoost)model with the s...This study involved the development of an interpretable prediction framework to access the stretch formability of AZ31 magnesium alloys through the combination of the extreme gradient boosting(XGBoost)model with the sparrow search algorithm(SSA).Eleven features were extracted from the microstructures(e.g.,grain size(GS),maximum pole intensity(I_(max)),degree of texture dispersion(μ),radius of maximum pole position(r),and angle of maximum pole position(A)),mechanical properties(e.g.,tensile yield strength(TYS),ultimate tensile strength(UTS),elongation-to-failure(EL),and strength difference(∆S))and test conditions(e.g.,sheet thickness(t)and punch speed(v))in the data collected from the literature and experiments.Pearson correlation coefficient and exhaustive screening methods identified ten key features(not including UTS)as the final inputs,and they enhanced the prediction accuracy of Index Erichsen(IE),which served as the model’s output.The newly developed SSA-XGBoost model exhibited an improved prediction performance,with a goodness of fit(R^(2))of 0.91 compared with traditional machine learning models.A new dataset(four samples)was prepared to validate the reliability and generalization capacity of this model,and below 5%errors were observed between predicted and experimental IE values.Based on this result,the quantitative relationship between the key features and IE values was established via Shapley additive explanation method and XGBoost feature importance analysis.I_(max),TYS,EL,r,GS,andΔS showed a crucial influence on the IE of 10 input features.This work offers a reliable and accurate tool for the prediction of the stretch formability of AZ31 magnesium alloys and provides insights into the development of high-formable magnesium alloys.展开更多
To develop a new magnesium alloy with excellent formability at room temperature, the effect of Y, Ce, and Gd addition on texture and stretch formability of Mg-1.5Zn alloys was carried out. The result shows that Y, Ce,...To develop a new magnesium alloy with excellent formability at room temperature, the effect of Y, Ce, and Gd addition on texture and stretch formability of Mg-1.5Zn alloys was carried out. The result shows that Y, Ce, and Gd addition in Mg-1.5Zn alloys can effectively weaken and modify the basal plane texture, characterized by TD-split texture in which the position of basal is titled from normal direction （ND） toward transverse direction （TD）. When Mg-1.5Zn alloy with Gd addition appears low texture intensity and TD-split texture, where the position of basal poles is tilted by about 4-35° from ND toward to TD, the largest Erichsen value of 7.0 and the elongation rate reaches 29.1% in TD direction. However, Y and Ce addition in Mg-1.5Zn alloys promote a large number of second phase particles, which cancel the contribution of the unique basal texture to stretch formability and ductility.展开更多
The AM50,AM50-0.1 Ca,AM50-0.3 Ca and AM50-0.5 Ca(wt.%) alloys were hot-rolled and their mechanical properties were determined for the purpose of investigating the effect of trace Ca addition on the texture and stretch...The AM50,AM50-0.1 Ca,AM50-0.3 Ca and AM50-0.5 Ca(wt.%) alloys were hot-rolled and their mechanical properties were determined for the purpose of investigating the effect of trace Ca addition on the texture and stretch formability of AM50 alloy.The results show that the addition of trace Ca can effectively modify the basal texture,which is characterized by the split of basal poles deviated from the normal direction(ND) after the hot rolling,while a broad spread of the basal planes toward the transverse direction(TD) after the annealing.Such change of the basal texture is related to the prior formation of massive compression twins and the decrease of the c/a ratio.Erichsen value increases from 2.25 to 4.21 mm with the increase of Ca content.The enhancement of stretch formability is ascribed to the weakened basal texture,which results in the increase of n-value and the decrease of r-value.展开更多
The magnesium alloy has a unique advantage in 3C fields due to its high specific strength and excellent electromagnetic shielding characteristic.However,it is difficult to deform homogeneously because of hexagonal clo...The magnesium alloy has a unique advantage in 3C fields due to its high specific strength and excellent electromagnetic shielding characteristic.However,it is difficult to deform homogeneously because of hexagonal close-packed structure.In the present work,the microstructure,mechanical properties and stretch formability of magnesium alloy sheets with different alloying elements were investigated.It was indicated that a trace addition of Zn or/and Er made a key role in modifying texture,activating shear bands formation and precipitating nanoscale second phases,respectively,which resulted in an obvious improvement in both stretch formability and mechanical properties.The results suggested that the Mg-0.5 Zn-0.5 Er alloy sheet exhibited higher tensile strength along the rolling direction,i.e.,yield strength of 180 MPa and ultimate tensile strength of 201 MPa,accompanying with superior Erichsen value of 7.0 mm at room temperature.The good performances of the sheet were ascribed to weakening basal texture intensity,formation of shear bands and precipitation of nanoscale W-phase(Mg_(3)Zn_(3)Er_(2)).展开更多
Bending and tension deformations were performed on Mg-1.3 wt%Zn-0.2 wt%RE-0.3 wt%Zr(ZEK100)alloy sheets that initially had a transverse direction(TD)-split texture.The effects of bending and tension deformations on th...Bending and tension deformations were performed on Mg-1.3 wt%Zn-0.2 wt%RE-0.3 wt%Zr(ZEK100)alloy sheets that initially had a transverse direction(TD)-split texture.The effects of bending and tension deformations on the texture formation and room-temperature formability of specimens were investigated.The specimen subjected to 3-pass bending and tension deformations exhibited an excellent Erichsen value of 9.6 mm.However,the Erichsen value deterioration was observed in the specimen subjected to 7-pass deformations.The rolling direction-split texture developed on the surface with an increasing pass number of deformations.Conversely,the clear TD-split texture remained at the central part.As a result,a quadrupole texture was macroscopically developed with an increasing pass number of deformations.The reduction in anisotropy by the formation of the quadrupole texture is suggested to be the main reason for the improvement in stretch formability.By contrast,the generation of coarse grains near the surface is suggested to be the direct cause for the deterioration of the stretch formability of the specimen subjected to 7-pass deformations.展开更多
Obviously planar anisotropy due to‘TD split’orthotropic texture(TD indicates Transverse direction)always exist in the Rare-earth(RE)or Ca containing Mg alloy sheets,which is likely caused by the lowreduction rolling...Obviously planar anisotropy due to‘TD split’orthotropic texture(TD indicates Transverse direction)always exist in the Rare-earth(RE)or Ca containing Mg alloy sheets,which is likely caused by the lowreduction rolling(and annealing)as revealed in our previous research.In this work,the as-cast billets of a ZWK100 alloy were subjected to final-pass heavy reduction rolling(FHRR)at 500°C with different reductions(30%-70%)after rough rolling,aiming to investigate the reduction effect on the microstructure and texture formation.The results show that FHRR with higher reductions above 50%is in favor of shear banding formation but has little effect on the as-deformed texture components,and the excellent formability with single-pass reduction up to 70%is mainly ascribed to the activation of prismatic slip.FHRR with reduction above 50%and annealing can generate uniform grain structures of~10μm and symmetrical‘oblique-line split’texture in(0001)pole figures,with basal poles tilting by about 50°from ND(Normal direction)towards some oblique-line of TD and RD(Rolling direction)as well as uniform distribution of counter lines as an annular shape,resulting in excellent elongation to failure of~50%and ultra-low planar anisotropyΔr_of~0.1 and high stretch formability(Erichsen value:8.1).The formation‘oblique-line split’texture in(0001)pole figures is mainly correlated with the preferred growth tendency of grains with■//RD,which was suggested to relate to the high mobility of some special boundaries such as 40°-45°■.The influences of starting textures on the mechanical properties,planar anisotropy and related deformation modes,as well as their correlations with the stretch formability were comparatively investigated with the‘TD split’orthotropic texture as a counterpoint.展开更多
In this study, the effect of various factors on the hole expansion ratio and hence on the edge formability of two hot rolled multiphase steels, one with a ferrite–martensite microstructure and the other with a ferrit...In this study, the effect of various factors on the hole expansion ratio and hence on the edge formability of two hot rolled multiphase steels, one with a ferrite–martensite microstructure and the other with a ferrite-bainite microstructure, was investigated through systematic microstructural and mechanical characterization. The study revealed that the microstructure of the steels, which determines their strain hardening capacity and fracture resistance, is the principal factor controlling edge formability. The influence of other factors such as tensile strength, ductility, anisotropy, and thickness, though present, are secondary. A critical evaluation of the available empirical models for hole expansion ratio prediction is also presented.展开更多
The grain orientation control via twinning activity on deformation features is of great significance to offer a key insight into understanding the deformation mechanism of Mg alloy sheets.The{10–12}twinning were perf...The grain orientation control via twinning activity on deformation features is of great significance to offer a key insight into understanding the deformation mechanism of Mg alloy sheets.The{10–12}twinning were performed by pre-strain paths,i.e.,tension(6%)and compression(5%)perpendicular to the c-axis along extrusion direction(ED),to investigate the microstructural evolution and mechanical properties of AZ31 Mg alloy sheets.The distinction in the texture evolution and strain hardening behavior was illustrated in connection with the pre-strain paths for the activities of twinning and slip.The result shows that the activation of the deformation mode was closely bound up with the grain orientation and the additional applied load direction.The{10–12}twin-texture components with c-axis//ED were generated by precompression,which can provide an appropriate alternative to accommodate the thin sheet thickness strain and enhance the room temperature formability of Mg alloy sheet.展开更多
Mg-3Al-lZn alloy sheets have been deformed by continuous bending（CB）to investigate the effects of pro-cessing parameters（bending angle and repetitive passes）on the texture and formability.The samples exhibited a b...Mg-3Al-lZn alloy sheets have been deformed by continuous bending（CB）to investigate the effects of pro-cessing parameters（bending angle and repetitive passes）on the texture and formability.The samples exhibited a bimodal microstructure with abnormal growth grains in the surface region and fine grains distributed in the center after CB process followed by annealing.The texture evolution measured by XRD indicated that the basal poles were rotated from ND toward RD,and the texture intensity decreased with the bending angle decreasing and repetitive passes increasing.Compared with the as-received sample,the yield strength of CBA-120-2 sample significantly decreased from 183 to 112 MPa,and a smaller r-value and a larger n-value were obtained.The formability of CB processed samples in annealing condition was significantly enhanced with the highest of Erichsen value of 5.4 mm,increased by about 135%.The improvement of formability was likely attributed to the weakened and RD-tilt basal texture and coarse grains in the surface part.展开更多
基金funded by the National Natural Science Foundation of China(No.52204407)the Natural Science Foundation of Jiangsu Province,China(No.BK20220595)+1 种基金the China Postdoctoral Science Foundation(No.2022M 723689)the Postgraduate Research&Practice Innovation Program of Jiangsu Province,China(No.SJCX23_1913).
文摘This study involved the development of an interpretable prediction framework to access the stretch formability of AZ31 magnesium alloys through the combination of the extreme gradient boosting(XGBoost)model with the sparrow search algorithm(SSA).Eleven features were extracted from the microstructures(e.g.,grain size(GS),maximum pole intensity(I_(max)),degree of texture dispersion(μ),radius of maximum pole position(r),and angle of maximum pole position(A)),mechanical properties(e.g.,tensile yield strength(TYS),ultimate tensile strength(UTS),elongation-to-failure(EL),and strength difference(∆S))and test conditions(e.g.,sheet thickness(t)and punch speed(v))in the data collected from the literature and experiments.Pearson correlation coefficient and exhaustive screening methods identified ten key features(not including UTS)as the final inputs,and they enhanced the prediction accuracy of Index Erichsen(IE),which served as the model’s output.The newly developed SSA-XGBoost model exhibited an improved prediction performance,with a goodness of fit(R^(2))of 0.91 compared with traditional machine learning models.A new dataset(four samples)was prepared to validate the reliability and generalization capacity of this model,and below 5%errors were observed between predicted and experimental IE values.Based on this result,the quantitative relationship between the key features and IE values was established via Shapley additive explanation method and XGBoost feature importance analysis.I_(max),TYS,EL,r,GS,andΔS showed a crucial influence on the IE of 10 input features.This work offers a reliable and accurate tool for the prediction of the stretch formability of AZ31 magnesium alloys and provides insights into the development of high-formable magnesium alloys.
基金supported by the Ministry of Science and Technology ‘‘Twelfth Five-Year’’ Plan for Science & Technology Support(No.2011BAE22B00)
文摘To develop a new magnesium alloy with excellent formability at room temperature, the effect of Y, Ce, and Gd addition on texture and stretch formability of Mg-1.5Zn alloys was carried out. The result shows that Y, Ce, and Gd addition in Mg-1.5Zn alloys can effectively weaken and modify the basal plane texture, characterized by TD-split texture in which the position of basal is titled from normal direction （ND） toward transverse direction （TD）. When Mg-1.5Zn alloy with Gd addition appears low texture intensity and TD-split texture, where the position of basal poles is tilted by about 4-35° from ND toward to TD, the largest Erichsen value of 7.0 and the elongation rate reaches 29.1% in TD direction. However, Y and Ce addition in Mg-1.5Zn alloys promote a large number of second phase particles, which cancel the contribution of the unique basal texture to stretch formability and ductility.
基金Projects(51801186,51974281)supported by the National Natural Science Foundation of ChinaProject(SKLSP201814)supported by the Fund of the State Key Laboratory of Solidification Processing in Northwestern Polytechnical University,China
文摘The AM50,AM50-0.1 Ca,AM50-0.3 Ca and AM50-0.5 Ca(wt.%) alloys were hot-rolled and their mechanical properties were determined for the purpose of investigating the effect of trace Ca addition on the texture and stretch formability of AM50 alloy.The results show that the addition of trace Ca can effectively modify the basal texture,which is characterized by the split of basal poles deviated from the normal direction(ND) after the hot rolling,while a broad spread of the basal planes toward the transverse direction(TD) after the annealing.Such change of the basal texture is related to the prior formation of massive compression twins and the decrease of the c/a ratio.Erichsen value increases from 2.25 to 4.21 mm with the increase of Ca content.The enhancement of stretch formability is ascribed to the weakened basal texture,which results in the increase of n-value and the decrease of r-value.
基金financially supported by Beijing Natural Science Foundation(No.2172013)the National Key Research and Development Program(No.2016YFB0301101)+1 种基金Beijing Municipal Commission of Education Key Science,Technology Projects(No.KZ201810005005)the National Natural Science Foundation of China(No.51801048)。
文摘The magnesium alloy has a unique advantage in 3C fields due to its high specific strength and excellent electromagnetic shielding characteristic.However,it is difficult to deform homogeneously because of hexagonal close-packed structure.In the present work,the microstructure,mechanical properties and stretch formability of magnesium alloy sheets with different alloying elements were investigated.It was indicated that a trace addition of Zn or/and Er made a key role in modifying texture,activating shear bands formation and precipitating nanoscale second phases,respectively,which resulted in an obvious improvement in both stretch formability and mechanical properties.The results suggested that the Mg-0.5 Zn-0.5 Er alloy sheet exhibited higher tensile strength along the rolling direction,i.e.,yield strength of 180 MPa and ultimate tensile strength of 201 MPa,accompanying with superior Erichsen value of 7.0 mm at room temperature.The good performances of the sheet were ascribed to weakening basal texture intensity,formation of shear bands and precipitation of nanoscale W-phase(Mg_(3)Zn_(3)Er_(2)).
文摘Bending and tension deformations were performed on Mg-1.3 wt%Zn-0.2 wt%RE-0.3 wt%Zr(ZEK100)alloy sheets that initially had a transverse direction(TD)-split texture.The effects of bending and tension deformations on the texture formation and room-temperature formability of specimens were investigated.The specimen subjected to 3-pass bending and tension deformations exhibited an excellent Erichsen value of 9.6 mm.However,the Erichsen value deterioration was observed in the specimen subjected to 7-pass deformations.The rolling direction-split texture developed on the surface with an increasing pass number of deformations.Conversely,the clear TD-split texture remained at the central part.As a result,a quadrupole texture was macroscopically developed with an increasing pass number of deformations.The reduction in anisotropy by the formation of the quadrupole texture is suggested to be the main reason for the improvement in stretch formability.By contrast,the generation of coarse grains near the surface is suggested to be the direct cause for the deterioration of the stretch formability of the specimen subjected to 7-pass deformations.
基金financially supported by Basic and Applied Basic Research Fund of Guangdong Province of China(No.2019A1515110573)National Natural Science Foundation of China(No.51901047)+2 种基金Special Innovation Projects of Universities in Guangdong Province(2018KTSCX240)Key Project of Department of Education of Guangdong Province(No.2016GCZX008)Project of Engineering Research Center of Foshan(No.20172010018)。
文摘Obviously planar anisotropy due to‘TD split’orthotropic texture(TD indicates Transverse direction)always exist in the Rare-earth(RE)or Ca containing Mg alloy sheets,which is likely caused by the lowreduction rolling(and annealing)as revealed in our previous research.In this work,the as-cast billets of a ZWK100 alloy were subjected to final-pass heavy reduction rolling(FHRR)at 500°C with different reductions(30%-70%)after rough rolling,aiming to investigate the reduction effect on the microstructure and texture formation.The results show that FHRR with higher reductions above 50%is in favor of shear banding formation but has little effect on the as-deformed texture components,and the excellent formability with single-pass reduction up to 70%is mainly ascribed to the activation of prismatic slip.FHRR with reduction above 50%and annealing can generate uniform grain structures of~10μm and symmetrical‘oblique-line split’texture in(0001)pole figures,with basal poles tilting by about 50°from ND(Normal direction)towards some oblique-line of TD and RD(Rolling direction)as well as uniform distribution of counter lines as an annular shape,resulting in excellent elongation to failure of~50%and ultra-low planar anisotropyΔr_of~0.1 and high stretch formability(Erichsen value:8.1).The formation‘oblique-line split’texture in(0001)pole figures is mainly correlated with the preferred growth tendency of grains with■//RD,which was suggested to relate to the high mobility of some special boundaries such as 40°-45°■.The influences of starting textures on the mechanical properties,planar anisotropy and related deformation modes,as well as their correlations with the stretch formability were comparatively investigated with the‘TD split’orthotropic texture as a counterpoint.
文摘In this study, the effect of various factors on the hole expansion ratio and hence on the edge formability of two hot rolled multiphase steels, one with a ferrite–martensite microstructure and the other with a ferrite-bainite microstructure, was investigated through systematic microstructural and mechanical characterization. The study revealed that the microstructure of the steels, which determines their strain hardening capacity and fracture resistance, is the principal factor controlling edge formability. The influence of other factors such as tensile strength, ductility, anisotropy, and thickness, though present, are secondary. A critical evaluation of the available empirical models for hole expansion ratio prediction is also presented.
基金National Natural Science Foundation of China(51701033,51701035)Chongqing Municipal Education Commission(KJQN201901504,KJZD-K202001502)Chongqing Science and Technology Commission(cstc2018jcyjAX0022).
文摘The grain orientation control via twinning activity on deformation features is of great significance to offer a key insight into understanding the deformation mechanism of Mg alloy sheets.The{10–12}twinning were performed by pre-strain paths,i.e.,tension(6%)and compression(5%)perpendicular to the c-axis along extrusion direction(ED),to investigate the microstructural evolution and mechanical properties of AZ31 Mg alloy sheets.The distinction in the texture evolution and strain hardening behavior was illustrated in connection with the pre-strain paths for the activities of twinning and slip.The result shows that the activation of the deformation mode was closely bound up with the grain orientation and the additional applied load direction.The{10–12}twin-texture components with c-axis//ED were generated by precompression,which can provide an appropriate alternative to accommodate the thin sheet thickness strain and enhance the room temperature formability of Mg alloy sheet.
基金financially supported by the National Natural Science Foundation of China (Nos. 51671041 and 51531002)the National Key Research and Development Plan (No. 2016YFB0301104)+1 种基金Demonstrative Project of Chongqing Science and Technology Commission (No. CSCT2014FAZKTJCSF50004)Fundamental Research Funds for the Central Universities (No. 106112017CDJPT280001)
文摘Mg-3Al-lZn alloy sheets have been deformed by continuous bending（CB）to investigate the effects of pro-cessing parameters（bending angle and repetitive passes）on the texture and formability.The samples exhibited a bimodal microstructure with abnormal growth grains in the surface region and fine grains distributed in the center after CB process followed by annealing.The texture evolution measured by XRD indicated that the basal poles were rotated from ND toward RD,and the texture intensity decreased with the bending angle decreasing and repetitive passes increasing.Compared with the as-received sample,the yield strength of CBA-120-2 sample significantly decreased from 183 to 112 MPa,and a smaller r-value and a larger n-value were obtained.The formability of CB processed samples in annealing condition was significantly enhanced with the highest of Erichsen value of 5.4 mm,increased by about 135%.The improvement of formability was likely attributed to the weakened and RD-tilt basal texture and coarse grains in the surface part.
