The implementation of artificial intelligence(AI)in a smart society,in which the analysis of human habits is mandatory,requires automated data scheduling and analysis using smart applications,a smart infrastructure,sm...The implementation of artificial intelligence(AI)in a smart society,in which the analysis of human habits is mandatory,requires automated data scheduling and analysis using smart applications,a smart infrastructure,smart systems,and a smart network.In this context,which is characterized by a large gap between training and operative processes,a dedicated method is required to manage and extract the massive amount of data and the related information mining.The method presented in this work aims to reduce this gap with near-zero-failure advanced diagnostics(AD)for smart management,which is exploitable in any context of Society 5.0,thus reducing the risk factors at all management levels and ensuring quality and sustainability.We have also developed innovative applications for a humancentered management system to support scheduling in the maintenance of operative processes,for reducing training costs,for improving production yield,and for creating a human–machine cyberspace for smart infrastructure design.The results obtained in 12 international companies demonstrate a possible global standardization of operative processes,leading to the design of a near-zero-failure intelligent system that is able to learn and upgrade itself.Our new method provides guidance for selecting the new generation of intelligent manufacturing and smart systems in order to optimize human–machine interactions,with the related smart maintenance and education.展开更多
[Objective]This study was to establish a rapid,specific and simple method for quantitative determination of tetrachlorantraniliprole by 1H NMR.[Method]1H NMR spectroscopy was acquired with deuterium DMSO as the solven...[Objective]This study was to establish a rapid,specific and simple method for quantitative determination of tetrachlorantraniliprole by 1H NMR.[Method]1H NMR spectroscopy was acquired with deuterium DMSO as the solvent and maleic acid as internal standard under the conditions of temperature 25℃,pulses width 8.0μs,delay time 5 s,and scanning times 8.[Result]The hydrogen proton peaks of tetrachlorantraniliprole(δ=10.55)and maleic acid(δ=6.27)were taken as quantitative peaks.The peak area ratio y(As/Ar)and mass ratio x(ms/mr)were linearly regressed,and the correlation coefficient was 0.9999.The RSD value of repeatability test was 0.38%,and the RSD value of stability test was 0.77%.The content of tetrachlorantraniliprole was determined as 99.6%.[Conclusion]1H NMR spectroscopy can be used for quantitative determination of tetrachlorantraniliprole without standard reference,which is rapid,accurate and simple.展开更多
Mercury and its organic compounds have been of severe concern worldwide due to their damage to the ecosystem and human health. The development of effective and affordable technology to monitor and signal the presence ...Mercury and its organic compounds have been of severe concern worldwide due to their damage to the ecosystem and human health. The development of effective and affordable technology to monitor and signal the presence of bioavailable mercury is an urgent need.The Mer gene is a mercury-responsive resistant gene, and a mercury-sensing recombinant luminescent bacterium using the Mer gene was constructed in this study. The mer operon from marine Pseudomonas putida strain SP1 was amplified and fused with prompterless lux CDABE in the p UCD615 plasmid within Escherichia coli cells, resulting in p THE30–E. coli.The recombinant strain showed high sensitivity and specificity. The detection limit of Hg^2＋was 5 nmol/L, and distinct luminescence could be detected in 30 min. Cd^2＋, Cu^2＋, Zn^2＋, Ca^2＋,Pb^2＋, Mg^2＋, Mn^2＋, and Al^3＋did not interfere with the detection over a range of 10-5–1 m M.Application of recombinant luminescent bacteria testing in environmental samples has been a controversial issue： especially for metal-sensing recombinant strains, false negatives caused by high cytotoxicity are one of the most important issues when applying recombinant luminescent bacteria in biomonitoring of heavy metals. In this study, by establishing an internal standard approach, the false negative problem was overcome;furthermore, the method can also help to estimate the suspected mercury concentration,which ensures high detection sensitivity of bioavailable Hg2＋.展开更多
The internal standard (IS) method is the best method for the analysis of samples, as it is independent of errors in injection volume, changes in sample volumes, and changes in sensitivity of the detector, etc. Use of ...The internal standard (IS) method is the best method for the analysis of samples, as it is independent of errors in injection volume, changes in sample volumes, and changes in sensitivity of the detector, etc. Use of an internal standard allows for the correction of losses due to sample clean-up of complex samples. An ideal IS is a compound that has properties very similar to, and that behaves as the compounds to be analysed. Ideally, only in the last step of analysis (HPLC), the IS should be well separated from the compounds of the mixture to be analysed. After testing several existing compounds with negative results, we decided to synthesise the 19-O-β-D-galactopyranosyl-13-O-β-D-glucopyranosyl-steviol as IS. This is the 19-galactosyl ester of steviolmonoside (13-O-β-D-glucopyranosyl-steviol). The IS was made according to published methods. Steviolmonoside (SM) was made from purified commercial rubusoside (Rub) by refluxing it in 10% KOH for 2 h. SM was precipitated and crystallized from MeOH. The hydroxyls of the glucose unit of SM were protected by acetylation. The acetylated SM was crystallized from acetone and dissolved in 1,2-dichloroethane. Then Ag2CO3 on Celite and tetra-acetylated galactopyranosyl bromide were added and the mixture was refluxed for 2 h. After cooling, BaO in MeOH was added to remove the acetyl groups. The 1,2-dichloroethane fraction was then extracted three times with equal volumes of water and the water fraction containing the IS was further purified on a C18 flash chromatography column. Traces of unreacted SM were removed by preparative HPLC on an Alltima C18 column (250 mm × 22 mm, particle size 10 μm) with AcCN:water (35:65, 20 ml/min). Detection was at 210 nm (KNAUER, “Smartline” UV detector 2500). The collected IS fraction from the HPLC was completely dried. Mixtures of steviol glycosides (SVglys) containing IS could be purified over SPE cartridges without change of the SVgly over IS ratio. The calibration curves for rebaudioside A (RebA) and stevioside (ST) were linear between 0.012 and 0.95 and between 0.013 and 1.13 mM for RebA and ST, respectively. The accuracy was checked by the standard addition method. It was concluded that the IS method gives an excellent precision and accuracy.展开更多
In the independent electro-hydrogen system(IEHS)with hybrid energy storage(HESS),achieving optimal scheduling is crucial.Still,it presents a challenge due to the significant deviations in values ofmultiple optimizatio...In the independent electro-hydrogen system(IEHS)with hybrid energy storage(HESS),achieving optimal scheduling is crucial.Still,it presents a challenge due to the significant deviations in values ofmultiple optimization objective functions caused by their physical dimensions.These deviations seriously affect the scheduling process.A novel standardization fusion method has been established to address this issue by analyzing the variation process of each objective function’s values.The optimal scheduling results of IEHS with HESS indicate that the economy and overall energy loss can be improved 2–3 times under different optimization methods.The proposed method better balances all optimization objective functions and reduces the impact of their dimensionality.When the cost of BESS decreases by approximately 30%,its participation deepens by about 1 time.Moreover,if the price of the electrolyzer is less than 15¥/kWh or if the cost of the fuel cell drops below 4¥/kWh,their participation will increase substantially.This study aims to provide a more reasonable approach to solving multi-objective optimization problems.展开更多
Long tree-ring chronologies can be developed by overlapping data from living trees with data from fossil trees through cross-dating.However,low-frequency climate signals are lost when standardizing tree-ring series du...Long tree-ring chronologies can be developed by overlapping data from living trees with data from fossil trees through cross-dating.However,low-frequency climate signals are lost when standardizing tree-ring series due to the"segment length curse".To alleviate the segment length curse and thus improve the standardization method for developing long tree-ring chronologies,here we first calculated a mean value for all the tree ring series by overlapping all of the tree ring series.The growth trend of the mean tree ring width(i.e.,cumulated average growth trend of all the series)was determined using ensemble empirical mode decomposition.Then the chronology was developed by dividing the mean value by the growth trend of the mean value.Our improved method alleviated the problem of trend distortion.Long-term signals were better preserved using the improved method than in previous detrending methods.The chronologies developed using the improved method were better correlated with climate than those developed using conservative methods.The improved standardization method alleviates trend distortion and retains more of the low-frequency climate signals.展开更多
Plastic equipment used in cell culture processes contains styrene residues and 2-chloroethanol, a byproduct of ethylene oxide sterilization. Both compounds can have long-term effects on the quality and safety of the c...Plastic equipment used in cell culture processes contains styrene residues and 2-chloroethanol, a byproduct of ethylene oxide sterilization. Both compounds can have long-term effects on the quality and safety of the cells in plastic equipment. GB/T 43778-2024, which establishes a gas chromatography-mass spectrometry(GC-MS) method for the simultaneous detection of st yrene and 2-chloroethanol in cell culture media, includes several technical requirements that need to be thoroughly interpreted. This paper provides a detailed explanation of the internal standard calibration method used for detecting styrene and 2-chloroethanol, covering the overall framework and innovation aspects of the standard. Additionally, it elucidates the principles and rationale of each step, including sample processing, detection parameters, preparation of standard solutions, and the determination of detection and quantification limits, to assist testing technical staff in applying the method effectively.展开更多
The cephalopod beak is a vital hard structure with a stable configuration and has been widely used for the identification of cephalopod species. This study was conducted to determine the best standardization method fo...The cephalopod beak is a vital hard structure with a stable configuration and has been widely used for the identification of cephalopod species. This study was conducted to determine the best standardization method for identifying different species by measuring 12 morphological variables of the beaks of Illex argentinus, Ommastrephes bartramii, and Dosidicus gigas that were collected by Chinese jigging vessels. To remove the effects of size, these morphometric variables were standardized using three methods. The average ratios of the upper beak morphological variables and upper crest length of O. bartramii and D. gigas were found to be greater than those of I. argentinus. However, for lower beaks, only the average of LRL(lower rostrum length)/LCL(lower crest length), LRW(lower rostrum width)/LCL, and LLWL(lower lateral wall length)/LCL of O. bartramii and D. gigas were greater than those of I. argentinus. The ratios of beak morphological variables and crest length were found to be all significantly different among the three species(P < 0.001). Among the three standardization methods, the correct classification rate of stepwise discriminant analysis(SDA) was the highest using the ratios of beak morphological variables and crest length. Compared with hood length, the correct classification rate was slightly higher when using beak variables standardized by crest length using an allometric model. The correct classification rate of the lower beak was also found to be greater than that of the upper beak. This study indicates that the ratios of beak morphological variables to crest length could be used for interspecies and intraspecies identification. Meanwhile, the lower beak variables were found to be more effective than upper beak variables in classifying beaks found in the stomachs of predators.展开更多
The matters of equipment optimization development are usually discrete,fuzzy and non-quantitative.It is difficult directly to optimize the equipment development with a mathematical model.A set of methods for designing...The matters of equipment optimization development are usually discrete,fuzzy and non-quantitative.It is difficult directly to optimize the equipment development with a mathematical model.A set of methods for designing the equipment optimization development with six dimensions and eight main elements is established based on the theory and method of standardization.The top-tier design space of systematic development of equipment is built up by the relations of basic models,series and model spectrums.The relations of time and space for equipment optimization development are established.The design processes of a six dimension systematic space are expounded.The connotation of each plan in the main system space is analyzed.A design method for an entire equipment is established with standardization theory.The coordinating design methods of equipment technical system and the optimization design methods of equipment integration are discussed.The design methods for universalization and serialization of components and parts are established.The design methods of equipment optimization development highlight the relations of the basic model of platform,the serialization of platform basic models,the modularization of equipment functions,the model spectrum of variant equipment,and the universalization and serialization of components and parts.展开更多
This paper analyses the current common problems of material code standardization in the implementation of MRP Ⅱ, and puts forward the basic ideas and methods for solving the problems, which has some reference value ...This paper analyses the current common problems of material code standardization in the implementation of MRP Ⅱ, and puts forward the basic ideas and methods for solving the problems, which has some reference value for the popularization of application o展开更多
Laser ablation coupled with inductively coupled plasma-mass spectrometry (LA-ICP-MS) calibration was conducted with multiple spot analyses on eleven intact rock samples using both an internal standard (IS) method and ...Laser ablation coupled with inductively coupled plasma-mass spectrometry (LA-ICP-MS) calibration was conducted with multiple spot analyses on eleven intact rock samples using both an internal standard (IS) method and a modified constant-sum (MCS) method. Methods were then compared for reported bulk elemental composition of the rocks. The MCS method was based on the sum of eight major elements, which is spatially more stable than one single major ele-ment as used in the IS method, and is quite constant among different rock samples. Calibrations were performed with standard reference materials NIST SRM 610, 612, 614, and 616. Little difference was found between using a single standard and a set of standards, because of the good linearity shown by the reference materials. Comparison of the two calibration methods shows that the MCS method produced better and more stable results than the IS method for heterogeneous samples. With the MCS method, approximately 94% to 95% of the total measurements are within the range of ±100% relative deviation, compared with 82% to 86% with the IS method. The IS method resulted insubstantial overestimations for some rock samples (e.g., 648% for Basalt BCR-2 using NIST SRM 610 as the calibration standard), while the largest deviation with the MCS method was 216% for U in Eagle Ford shale #80 sample. For Quartz latite QLO-1, a relative homogeneous sample, the IS method generated slightly better results than the MCS method. Regardless of method, spatially heterogeneous distribution of elements in the intact rock at the scale of the laser spot is considered to be the main reason for the large relative deviations seen in our work compared to published results.展开更多
dual-standard addition method was proposed and the principle of simultaneous determination for a interfering binary mixtures was discussed. The proposed procedure was applied to spectroscopic analyses for the simultan...dual-standard addition method was proposed and the principle of simultaneous determination for a interfering binary mixtures was discussed. The proposed procedure was applied to spectroscopic analyses for the simultaneous determination of uranium and thorium without prior separation. Various molar ratios of uranium/thorium, from 0.5∶1 to 10∶1, can be determined with satisfactory precision and accuracy. Uranium and thorium content in a phosphate ore and simulated sample were determined, the recoveries were 98.4%～102.5% for uranium and 96.8%～102.3% for thorium, the relative standard deviations (R.S.D) were 1.5%～2.3% for uranium and 2.1%～3.1% for thorium.展开更多
A method of Standard Site Method (SSM) in the American National Standards Institute’s ANSI C63.5 is described in the frequency ranges from 30 MHz to 1000 MHz. And a measurement system is set up for determining antenn...A method of Standard Site Method (SSM) in the American National Standards Institute’s ANSI C63.5 is described in the frequency ranges from 30 MHz to 1000 MHz. And a measurement system is set up for determining antenna factors (AF) of antennas on an Open Area Test Sites (OATS). AF of antennas including log-periodic antenna and biconical antenna is measured with SSM method by Shanghai Institute of Measurement and Testing Technology (SIMT), which shows good agreement to data measured by National Institute of Metrology (NIM). In the end, it analyzes the measurement uncertainty of SIMT in the 30 MHz to 1000 MHz frequency band and does comparison to that of NIM.展开更多
Objective: to study the effect of improved standard collection method in sputum bacterial test. Methods: 82 patients with acute attack of bronchitis received in our hospital from October 2018 to October 2019 were sele...Objective: to study the effect of improved standard collection method in sputum bacterial test. Methods: 82 patients with acute attack of bronchitis received in our hospital from October 2018 to October 2019 were selected for sputum bacterial test.Based on the order of admission, 41 cases in the reference group were given routine expectoration collection method;41 cases in the observation group were treated with improved standard collection method, and the test results of the two groups were compared. Results: ① The qualified rate of sputum samples in the observation group was statistically different from that in the reference group (P < 0.05).② The positive rate of sputum culture in the observation group was significantly different from that in the reference group (P < 0.05).③ There were differences in the collection time of samples and the operation time of sputum bacteriological test between the two groups (P < 0.05).Conclusion: the application of improved standard collection method in sputum bacterial test can improve the positive rate and shorten the time of practical operation.展开更多
Mongolian Terms Commonly Used in Meteorological Services that was issued by the China Meteorological Administration is China s first traditional Mongolian standard in meteorological industry. In the process of formula...Mongolian Terms Commonly Used in Meteorological Services that was issued by the China Meteorological Administration is China s first traditional Mongolian standard in meteorological industry. In the process of formulation, the compilation unit fully complied with the principles of scientificity, practicability, universality and versatility, and used literal translation, free translation, and the combination of literal translation and free translation to translate and compile 71 mongolian terms commonly used in meteorological services. The standard fills the blank of standardization construction of basic traditional Mongolian language in the meteorological industry of China.展开更多
文摘The implementation of artificial intelligence(AI)in a smart society,in which the analysis of human habits is mandatory,requires automated data scheduling and analysis using smart applications,a smart infrastructure,smart systems,and a smart network.In this context,which is characterized by a large gap between training and operative processes,a dedicated method is required to manage and extract the massive amount of data and the related information mining.The method presented in this work aims to reduce this gap with near-zero-failure advanced diagnostics(AD)for smart management,which is exploitable in any context of Society 5.0,thus reducing the risk factors at all management levels and ensuring quality and sustainability.We have also developed innovative applications for a humancentered management system to support scheduling in the maintenance of operative processes,for reducing training costs,for improving production yield,and for creating a human–machine cyberspace for smart infrastructure design.The results obtained in 12 international companies demonstrate a possible global standardization of operative processes,leading to the design of a near-zero-failure intelligent system that is able to learn and upgrade itself.Our new method provides guidance for selecting the new generation of intelligent manufacturing and smart systems in order to optimize human–machine interactions,with the related smart maintenance and education.
文摘[Objective]This study was to establish a rapid,specific and simple method for quantitative determination of tetrachlorantraniliprole by 1H NMR.[Method]1H NMR spectroscopy was acquired with deuterium DMSO as the solvent and maleic acid as internal standard under the conditions of temperature 25℃,pulses width 8.0μs,delay time 5 s,and scanning times 8.[Result]The hydrogen proton peaks of tetrachlorantraniliprole(δ=10.55)and maleic acid(δ=6.27)were taken as quantitative peaks.The peak area ratio y(As/Ar)and mass ratio x(ms/mr)were linearly regressed,and the correlation coefficient was 0.9999.The RSD value of repeatability test was 0.38%,and the RSD value of stability test was 0.77%.The content of tetrachlorantraniliprole was determined as 99.6%.[Conclusion]1H NMR spectroscopy can be used for quantitative determination of tetrachlorantraniliprole without standard reference,which is rapid,accurate and simple.
基金supported by the National Natural Science Foundation of China (No. 21377065)the 863 National High-Tech Research and Development Program (No. 2014AA06A506)
文摘Mercury and its organic compounds have been of severe concern worldwide due to their damage to the ecosystem and human health. The development of effective and affordable technology to monitor and signal the presence of bioavailable mercury is an urgent need.The Mer gene is a mercury-responsive resistant gene, and a mercury-sensing recombinant luminescent bacterium using the Mer gene was constructed in this study. The mer operon from marine Pseudomonas putida strain SP1 was amplified and fused with prompterless lux CDABE in the p UCD615 plasmid within Escherichia coli cells, resulting in p THE30–E. coli.The recombinant strain showed high sensitivity and specificity. The detection limit of Hg^2＋was 5 nmol/L, and distinct luminescence could be detected in 30 min. Cd^2＋, Cu^2＋, Zn^2＋, Ca^2＋,Pb^2＋, Mg^2＋, Mn^2＋, and Al^3＋did not interfere with the detection over a range of 10-5–1 m M.Application of recombinant luminescent bacteria testing in environmental samples has been a controversial issue： especially for metal-sensing recombinant strains, false negatives caused by high cytotoxicity are one of the most important issues when applying recombinant luminescent bacteria in biomonitoring of heavy metals. In this study, by establishing an internal standard approach, the false negative problem was overcome;furthermore, the method can also help to estimate the suspected mercury concentration,which ensures high detection sensitivity of bioavailable Hg2＋.
文摘The internal standard (IS) method is the best method for the analysis of samples, as it is independent of errors in injection volume, changes in sample volumes, and changes in sensitivity of the detector, etc. Use of an internal standard allows for the correction of losses due to sample clean-up of complex samples. An ideal IS is a compound that has properties very similar to, and that behaves as the compounds to be analysed. Ideally, only in the last step of analysis (HPLC), the IS should be well separated from the compounds of the mixture to be analysed. After testing several existing compounds with negative results, we decided to synthesise the 19-O-β-D-galactopyranosyl-13-O-β-D-glucopyranosyl-steviol as IS. This is the 19-galactosyl ester of steviolmonoside (13-O-β-D-glucopyranosyl-steviol). The IS was made according to published methods. Steviolmonoside (SM) was made from purified commercial rubusoside (Rub) by refluxing it in 10% KOH for 2 h. SM was precipitated and crystallized from MeOH. The hydroxyls of the glucose unit of SM were protected by acetylation. The acetylated SM was crystallized from acetone and dissolved in 1,2-dichloroethane. Then Ag2CO3 on Celite and tetra-acetylated galactopyranosyl bromide were added and the mixture was refluxed for 2 h. After cooling, BaO in MeOH was added to remove the acetyl groups. The 1,2-dichloroethane fraction was then extracted three times with equal volumes of water and the water fraction containing the IS was further purified on a C18 flash chromatography column. Traces of unreacted SM were removed by preparative HPLC on an Alltima C18 column (250 mm × 22 mm, particle size 10 μm) with AcCN:water (35:65, 20 ml/min). Detection was at 210 nm (KNAUER, “Smartline” UV detector 2500). The collected IS fraction from the HPLC was completely dried. Mixtures of steviol glycosides (SVglys) containing IS could be purified over SPE cartridges without change of the SVgly over IS ratio. The calibration curves for rebaudioside A (RebA) and stevioside (ST) were linear between 0.012 and 0.95 and between 0.013 and 1.13 mM for RebA and ST, respectively. The accuracy was checked by the standard addition method. It was concluded that the IS method gives an excellent precision and accuracy.
基金sponsored by R&D Program of Beijing Municipal Education Commission(KM202410009013).
文摘In the independent electro-hydrogen system(IEHS)with hybrid energy storage(HESS),achieving optimal scheduling is crucial.Still,it presents a challenge due to the significant deviations in values ofmultiple optimization objective functions caused by their physical dimensions.These deviations seriously affect the scheduling process.A novel standardization fusion method has been established to address this issue by analyzing the variation process of each objective function’s values.The optimal scheduling results of IEHS with HESS indicate that the economy and overall energy loss can be improved 2–3 times under different optimization methods.The proposed method better balances all optimization objective functions and reduces the impact of their dimensionality.When the cost of BESS decreases by approximately 30%,its participation deepens by about 1 time.Moreover,if the price of the electrolyzer is less than 15¥/kWh or if the cost of the fuel cell drops below 4¥/kWh,their participation will increase substantially.This study aims to provide a more reasonable approach to solving multi-objective optimization problems.
文摘Long tree-ring chronologies can be developed by overlapping data from living trees with data from fossil trees through cross-dating.However,low-frequency climate signals are lost when standardizing tree-ring series due to the"segment length curse".To alleviate the segment length curse and thus improve the standardization method for developing long tree-ring chronologies,here we first calculated a mean value for all the tree ring series by overlapping all of the tree ring series.The growth trend of the mean tree ring width(i.e.,cumulated average growth trend of all the series)was determined using ensemble empirical mode decomposition.Then the chronology was developed by dividing the mean value by the growth trend of the mean value.Our improved method alleviated the problem of trend distortion.Long-term signals were better preserved using the improved method than in previous detrending methods.The chronologies developed using the improved method were better correlated with climate than those developed using conservative methods.The improved standardization method alleviates trend distortion and retains more of the low-frequency climate signals.
基金funded by National Key Research and Development Project (No. 2018YFA0108403)Provincial University Basic Research Operating Expenses Project (No. 21SBYB08)
文摘Plastic equipment used in cell culture processes contains styrene residues and 2-chloroethanol, a byproduct of ethylene oxide sterilization. Both compounds can have long-term effects on the quality and safety of the cells in plastic equipment. GB/T 43778-2024, which establishes a gas chromatography-mass spectrometry(GC-MS) method for the simultaneous detection of st yrene and 2-chloroethanol in cell culture media, includes several technical requirements that need to be thoroughly interpreted. This paper provides a detailed explanation of the internal standard calibration method used for detecting styrene and 2-chloroethanol, covering the overall framework and innovation aspects of the standard. Additionally, it elucidates the principles and rationale of each step, including sample processing, detection parameters, preparation of standard solutions, and the determination of detection and quantification limits, to assist testing technical staff in applying the method effectively.
基金supported by the National Natural Science Foundation of China(Nos.41306127 and 41276156)the National Science Foundation of Shanghai(No.13ZR1419700)+3 种基金the Innovation Program of Shanghai Municipal Education Commission(No.13YZ091)the Shanghai Leading Academic Discipline Project(Fisheries Discipline)supported by Shanghai Ocean University(SHOU)International Center for Marine StudiesShanghai Visiting 1000 Talent Program
文摘The cephalopod beak is a vital hard structure with a stable configuration and has been widely used for the identification of cephalopod species. This study was conducted to determine the best standardization method for identifying different species by measuring 12 morphological variables of the beaks of Illex argentinus, Ommastrephes bartramii, and Dosidicus gigas that were collected by Chinese jigging vessels. To remove the effects of size, these morphometric variables were standardized using three methods. The average ratios of the upper beak morphological variables and upper crest length of O. bartramii and D. gigas were found to be greater than those of I. argentinus. However, for lower beaks, only the average of LRL(lower rostrum length)/LCL(lower crest length), LRW(lower rostrum width)/LCL, and LLWL(lower lateral wall length)/LCL of O. bartramii and D. gigas were greater than those of I. argentinus. The ratios of beak morphological variables and crest length were found to be all significantly different among the three species(P < 0.001). Among the three standardization methods, the correct classification rate of stepwise discriminant analysis(SDA) was the highest using the ratios of beak morphological variables and crest length. Compared with hood length, the correct classification rate was slightly higher when using beak variables standardized by crest length using an allometric model. The correct classification rate of the lower beak was also found to be greater than that of the upper beak. This study indicates that the ratios of beak morphological variables to crest length could be used for interspecies and intraspecies identification. Meanwhile, the lower beak variables were found to be more effective than upper beak variables in classifying beaks found in the stomachs of predators.
文摘The matters of equipment optimization development are usually discrete,fuzzy and non-quantitative.It is difficult directly to optimize the equipment development with a mathematical model.A set of methods for designing the equipment optimization development with six dimensions and eight main elements is established based on the theory and method of standardization.The top-tier design space of systematic development of equipment is built up by the relations of basic models,series and model spectrums.The relations of time and space for equipment optimization development are established.The design processes of a six dimension systematic space are expounded.The connotation of each plan in the main system space is analyzed.A design method for an entire equipment is established with standardization theory.The coordinating design methods of equipment technical system and the optimization design methods of equipment integration are discussed.The design methods for universalization and serialization of components and parts are established.The design methods of equipment optimization development highlight the relations of the basic model of platform,the serialization of platform basic models,the modularization of equipment functions,the model spectrum of variant equipment,and the universalization and serialization of components and parts.
文摘This paper analyses the current common problems of material code standardization in the implementation of MRP Ⅱ, and puts forward the basic ideas and methods for solving the problems, which has some reference value for the popularization of application o
文摘Laser ablation coupled with inductively coupled plasma-mass spectrometry (LA-ICP-MS) calibration was conducted with multiple spot analyses on eleven intact rock samples using both an internal standard (IS) method and a modified constant-sum (MCS) method. Methods were then compared for reported bulk elemental composition of the rocks. The MCS method was based on the sum of eight major elements, which is spatially more stable than one single major ele-ment as used in the IS method, and is quite constant among different rock samples. Calibrations were performed with standard reference materials NIST SRM 610, 612, 614, and 616. Little difference was found between using a single standard and a set of standards, because of the good linearity shown by the reference materials. Comparison of the two calibration methods shows that the MCS method produced better and more stable results than the IS method for heterogeneous samples. With the MCS method, approximately 94% to 95% of the total measurements are within the range of ±100% relative deviation, compared with 82% to 86% with the IS method. The IS method resulted insubstantial overestimations for some rock samples (e.g., 648% for Basalt BCR-2 using NIST SRM 610 as the calibration standard), while the largest deviation with the MCS method was 216% for U in Eagle Ford shale #80 sample. For Quartz latite QLO-1, a relative homogeneous sample, the IS method generated slightly better results than the MCS method. Regardless of method, spatially heterogeneous distribution of elements in the intact rock at the scale of the laser spot is considered to be the main reason for the large relative deviations seen in our work compared to published results.
文摘dual-standard addition method was proposed and the principle of simultaneous determination for a interfering binary mixtures was discussed. The proposed procedure was applied to spectroscopic analyses for the simultaneous determination of uranium and thorium without prior separation. Various molar ratios of uranium/thorium, from 0.5∶1 to 10∶1, can be determined with satisfactory precision and accuracy. Uranium and thorium content in a phosphate ore and simulated sample were determined, the recoveries were 98.4%～102.5% for uranium and 96.8%～102.3% for thorium, the relative standard deviations (R.S.D) were 1.5%～2.3% for uranium and 2.1%～3.1% for thorium.
文摘A method of Standard Site Method (SSM) in the American National Standards Institute’s ANSI C63.5 is described in the frequency ranges from 30 MHz to 1000 MHz. And a measurement system is set up for determining antenna factors (AF) of antennas on an Open Area Test Sites (OATS). AF of antennas including log-periodic antenna and biconical antenna is measured with SSM method by Shanghai Institute of Measurement and Testing Technology (SIMT), which shows good agreement to data measured by National Institute of Metrology (NIM). In the end, it analyzes the measurement uncertainty of SIMT in the 30 MHz to 1000 MHz frequency band and does comparison to that of NIM.
文摘Objective: to study the effect of improved standard collection method in sputum bacterial test. Methods: 82 patients with acute attack of bronchitis received in our hospital from October 2018 to October 2019 were selected for sputum bacterial test.Based on the order of admission, 41 cases in the reference group were given routine expectoration collection method;41 cases in the observation group were treated with improved standard collection method, and the test results of the two groups were compared. Results: ① The qualified rate of sputum samples in the observation group was statistically different from that in the reference group (P < 0.05).② The positive rate of sputum culture in the observation group was significantly different from that in the reference group (P < 0.05).③ There were differences in the collection time of samples and the operation time of sputum bacteriological test between the two groups (P < 0.05).Conclusion: the application of improved standard collection method in sputum bacterial test can improve the positive rate and shorten the time of practical operation.
文摘Mongolian Terms Commonly Used in Meteorological Services that was issued by the China Meteorological Administration is China s first traditional Mongolian standard in meteorological industry. In the process of formulation, the compilation unit fully complied with the principles of scientificity, practicability, universality and versatility, and used literal translation, free translation, and the combination of literal translation and free translation to translate and compile 71 mongolian terms commonly used in meteorological services. The standard fills the blank of standardization construction of basic traditional Mongolian language in the meteorological industry of China.
