To investigate the effect of microstructure evolution on corrosion behavior and strengthening mechanism of Mg-1Zn-1Ca(wt.%)alloys,as-cast Mg-1Zn-1Ca alloys were performed by equal channel angular pressing(ECAP)with 1 ...To investigate the effect of microstructure evolution on corrosion behavior and strengthening mechanism of Mg-1Zn-1Ca(wt.%)alloys,as-cast Mg-1Zn-1Ca alloys were performed by equal channel angular pressing(ECAP)with 1 and 4 passes.The corrosion behavior and mechanical properties of alloys were investigated by optical microscopy(OM),scanning electron microscopy(SEM),electron backscatter diffraction(EBSD),electrochemical tests,immersion tests and tensile tests.The results showed that mechanical properties improved after ECAP 1 pass;however,the corrosion resistance deteriorated due to high-density dislocations and fragmented secondary phases by ECAP.In contrast,synchronous improvement in the mechanical properties and corrosion resistance was achieved though grain refinement after ECAP 4 passes;fine grains led to a significant improvement in the yield strength,ultimate tensile strength,elongation,and corrosion rate of 103 MPa,223 MPa,30.5%,and 1.5843 mm/a,respectively.The enhanced corrosion resistance was attributed to the formation of dense corrosion product films by finer grains and the barrier effect by high-density grain boundaries.These results indicated that Mg-1Zn-1Ca alloy has a promising potential for application in biomedical materials.展开更多
The low ductility and strong mechanical anisotropy of wrought magnesium alloys have hindered their further processing and application.In this study,AZ31 magnesium alloy sheet was prepared by a new asymmetrical angular...The low ductility and strong mechanical anisotropy of wrought magnesium alloys have hindered their further processing and application.In this study,AZ31 magnesium alloy sheet was prepared by a new asymmetrical angular rolling(AAR)process,compared with conventional symmetrical rolling(SR)process and asymmetrical rolling(ASR)process.The effects of three rolling processes on the microstructure,texture and mechanical properties of the alloy sheets were systematically studied.The results show that the AAR sheet exhibits excellent mechanical properties compared to other two rolling processes.It not only achieves the highest ductility of 17.9%,17.9%,and 18.5% in the three directions,but also has the lowest mechanical anisotropy values for yield strength,ultimate tensile strength and elongation.The AAR process significantly reduces the anisotropy of the material by achieving the smallest average grain size of 4.93μm and the most homogeneous grain size distribution.Introduced bi-directional asymmetric shear stresses randomizes grain orientation and activates the non-basal slip system,which also significantly reduces the anisotropy.In addition,the tensile twinning mechanism dominates during the AAR process,which contributes to texture weakening and the activation of the non-basal slip system.Through the synergy of these mechanisms,the AAR sheet is characterized by high ductility and low anisotropy.展开更多
We propose a method to measure the flatness of an object with a petal-like pattern generated by the interference of the measured orbital angular momentum(OAM)beam and the reference OAM beam which carries the opposite ...We propose a method to measure the flatness of an object with a petal-like pattern generated by the interference of the measured orbital angular momentum(OAM)beam and the reference OAM beam which carries the opposite OAM state.By calculating the difference between the petal rotation angle without/with the object,the thickness information of the object,and then the flatness information,can be evaluated.Furthermore,the direction of the object’s flatness can be determined by the petal’s clockwise/counterclockwise rotation.We theoretically analyze the relationship between the object’s thickness and petal rotation angle,and verify the proposed method by experiment.The experimental results show that the proposed method is a high precision flatness measurement and can obtain the convex/concave property of the flatness.For the 1.02 mm glass sample,the mean deviation of the flatness is 1.357×10^(-8) and the variance is 0.242×10^(-16).For the 0.50 mm glass sample,the mean deviation of the flatness is 1.931×10^(-8) and the variance is 2.405×10^(-16).Two different topological charges are adopted for the 2.00 mm glass sample,and their flatness deviations are 0.239×10^(-8)(ℓ=1)and 0.246×10^(-8)(ℓ=2),where their variances are 0.799×10^(-18)(ℓ=1)and 0.775×10^(-18)(ℓ=2),respectively.It is shown that the flatness measured by the proposed method is the same for the same sample when different topological charges are used.All results indicate that the proposed method may provide a high flatness measurement,and will be a promising way to measure the flatness.展开更多
Quantum secure direct communication(QSDC) is a communication method based on quantum mechanics and it is used to transmit secret messages. Unlike quantum key distribution, secret messages can be transmitted directly o...Quantum secure direct communication(QSDC) is a communication method based on quantum mechanics and it is used to transmit secret messages. Unlike quantum key distribution, secret messages can be transmitted directly on a quantum channel with QSDC. Higher channel capacity and noise suppression capabilities are key to achieving longdistance quantum communication. Here, we report a continuous-variable QSDC scheme based on mask-coding and orbital angular momentum, in which the mask-coding is employed to protect the security of the transmitting messages and to suppress the influence of excess noise. The combination of orbital angular momentum and information block transmission effectively improves the secrecy capacity. In the 800 information blocks ×1310 bits length 10-km experiment, the results show a statistical average bit error rate of 0.38%, a system excess noise value of 0.0184 SNU, and a final secrecy capacity of 6.319×10~6 bps. Therefore, this scheme reduces error bits while increasing secrecy capacity, providing a solution for long-distance large-scale quantum communication, which is capable of transmitting text, images and other information of reasonable size.展开更多
In this study,the interaction between deformation and precipitates during multiple equal channel angular pressing(ECAP)deformations and inter-pass aging combination and its effect on the mechanical properties of 7050 ...In this study,the interaction between deformation and precipitates during multiple equal channel angular pressing(ECAP)deformations and inter-pass aging combination and its effect on the mechanical properties of 7050 aluminum alloy are studied.The result show that ECAP induces numerous substructures and dislocations,effectively promoting the precipitation of theηʹphase exhibiting a bimodal structure during inter-pass aging.Following inter-pass aging and subsequent ECAP,the decrease in grain size(4.8μm)is together with the increase in dislocation density(1.24×10^(15) m^(−2))due to the pinning effect of the precipitated phase.Simultaneously,the dislocation motion causes the second phase particles to become even finer and more diffuse.The synergistic effects of precipitation strengthening,fine grain strengthening,and dislocation strengthening collectively enhance the high strength of aluminum alloys,with ultimate tensile strength and yield strength reaching approximately 610 and 565 MPa,respectively.Meanwhile,ductility remains largely unchanged,primarily due to coordinated grain boundary sliding and the uniform and fine dispersion of second phase particles.展开更多
We demonstrate an effective and optimal strategy for generating spatially resolved longitudinal spin angular momentum(LSAM)in optical tweezers by tightly focusing the first-order spirally polarized vector(SPV)beams wi...We demonstrate an effective and optimal strategy for generating spatially resolved longitudinal spin angular momentum(LSAM)in optical tweezers by tightly focusing the first-order spirally polarized vector(SPV)beams with zero intrinsic angular momentum into a refractive index stratified medium.The stratified medium gives rise to a spherically aberrated intensity profile near the focal region of the optical tweezers,with off-axis intensity lobes in the radial direction possessing opposite LSAM(helicities corresponding toσ=+1 and−1)compared to the beam center.We trap mesoscopic birefringent particles in an off-axis intensity lobe as well as at the beam center by modifying the trapping plane and observe particles spinning in opposite directions depending on their location.The direction of rotation depends on the particle size with larger particles spinning either clockwise or anticlockwise depending on the direction of spirality of the polarization of the SPV beam after tight focusing,while smaller particles spin in both directions depending on their spatial locations.Numerical simulations support our experimental observations.Our results introduce new avenues in spin-orbit optomechanics to facilitate novel yet straightforward avenues for exotic and complex particle manipulation in optical tweezers.展开更多
Commercial ZK60 Mg alloy was processed by multi-pass equal-channel angular pressing（ECAP） and subsequent aging to investigate the effect of grain refinement and second-phase redistribution on its corrosion behavior....Commercial ZK60 Mg alloy was processed by multi-pass equal-channel angular pressing（ECAP） and subsequent aging to investigate the effect of grain refinement and second-phase redistribution on its corrosion behavior. Electrochemical tests show that the fine-grained samples after more ECAP passes have higher corrosion current densities（Jcorr） in the polarization curves, lower charge-transfer resistance（Rt） values in the EIS plots. The severe plastic deformation decreases the alloy corrosion resistance besides the well-known strengthening and toughening. Scanning Kelvin probe（SKP） measurement shows that the anodic and cathode sites are homogeneously distributed on the surface of the fine-grained alloy, which inhibits localized corrosion. The SKP potential, having linear relationship with the corrosion potential（φcorr）, decreases with increasing the ECAP pass. Furthermore, the post-ECAP aging can slightly improve the corrosion resistance of the fine-grained ZK60 Mg alloy and enhance the comprehensive performances, due to the stress relief and uniform distribution of second-phase particles.展开更多
To manufacture plate by the combination of equal channel angular processing （ECAP） and porthole die extrusion techniques, a novel technique, namely portholes-equal channel angular processing （P-ECAP）, was studied....To manufacture plate by the combination of equal channel angular processing （ECAP） and porthole die extrusion techniques, a novel technique, namely portholes-equal channel angular processing （P-ECAP）, was studied. Extrusion of AL6005A plate used for the bullet train plate was investigated by finite element method. The relevant porthole dies involving ECAP technique in channels were designed. Dimensional changes in the scrap part of the extrudate obtained after extrusion from the P-ECAP die, with different channel angles, were predicted. Effects of the channel angle and extrusion speed on the maximum temperature of the workpiece and other field variables were evaluated. At the channel angle of 160° of P-ECAP dies, the extrudate exhibited the optimal performance and the least amount of extrudate scrap was obtained. The optimal extrusion speed was 3-5 mm/s. Moreover, with the increase in ram speed from 1 to 9 mm/s, the peak extrusion load increased by about 49% and the maximum temperature was increased by about 70 ℃. The effective strain exhibited ascending trend in the comer of the ECAP deformation zone. In the solder seam and the side of die bearing of extrudate, the maximum principal stresses were tensile stress.展开更多
In comparison with the conventional equal channel angular pressing（ECAP） process,a comprehensive study of influence of twist extrusion（TE） process on consolidating pure aluminum powder in tubes（PITs） by equal ch...In comparison with the conventional equal channel angular pressing（ECAP） process,a comprehensive study of influence of twist extrusion（TE） process on consolidating pure aluminum powder in tubes（PITs） by equal channel angular pressing and torsion（ECAPT） was conducted via three-dimensional（3D） finite element simulation,experimental investigation and theoretical analysis.Simulation results revealed that during the consolidation of aluminum powder particles by ECAPT,TE process played a significant role of back pressure.Due to the torsional shear and high hydrostatic pressure exerted by twist channel,both the magnitude and homogeneity of the effective strain were increased markedly.After one pass of ECAPT process using a square channel with an inner angle of 90° and a twist slope angle of 36.5° at 200℃,commercial pure aluminum powder particles were successfully consolidated to nearly full density.Simulation and experimental results showed good agreement.In the microstructure observations,grains were greatly refined.At the same time,porosities were effectively eliminated by shrinking in size and breaking into small ones.Microhardness test indicated that strain distribution of ECAPT-processed billet was more homogeneous with respect to the ECAP-processed one.All these improvements may be attributed to the extreme intense shear strain induced during ECAPT and the increase in self-diffusion coefficient of aluminum due to the back pressure exerted by TE process.展开更多
Microstructure evolution and texture development and their effects on mechanical properties of a Mg-Gd-Y-Zr alloy during equal channel angular pressing（ECAP） were investigated.It is found that the microstructure is ...Microstructure evolution and texture development and their effects on mechanical properties of a Mg-Gd-Y-Zr alloy during equal channel angular pressing（ECAP） were investigated.It is found that the microstructure is still inhomogeneous after four passes,and two zones,namely the fine grain zone（FGZ） and the coarse grain zone（CGZ） are formed.The grain refinement occurs mainly by particle-stimulated nucleation（PSN） mechanism,which led to a more random texture after four passes of ECAP.In the ECAP-processed alloy,the strength did not increase while the ductility was enhanced dramatically compared with the as-received condition.The change of ductility of this alloy was discussed in terms of texture and second phase particles.展开更多
Consolidation of pure Alpowder was conducted at 200 ℃ by equal channel angular pressing and torsion （ECAPT） method. The grain refinement and consolidation behavior were deeply investigated by scan electronic micros...Consolidation of pure Alpowder was conducted at 200 ℃ by equal channel angular pressing and torsion （ECAPT） method. The grain refinement and consolidation behavior were deeply investigated by scan electronic microscopy （SEM） and transmission electronic microscopy （TEM）. The density, hardness and room temperature compression properties of the deformed samples were measured. The experiment results show that ECAPT is an effective method of consolidating powders at relatively low temperatures. Pure A1 particles are successfully consolidated into dense bulk material after 4 passes of ECAPT at 200 ℃. The consolidated material possesses fine grain structure and excellent mechanical properties. The refinement and consolidation mechanisms were analyzed. ECAPT is a promising method to produce the high-performance bulk materials from particles.展开更多
Uniaxial compressive experiments of ultrafine-grained Al fabricated by equal channel angular pressing(ECAP) method were performed at wide temperature and strain rate range. The influence of temperature on flow stress,...Uniaxial compressive experiments of ultrafine-grained Al fabricated by equal channel angular pressing(ECAP) method were performed at wide temperature and strain rate range. The influence of temperature on flow stress, strain hardening rate and strain rate sensitivity was investigated experimentally. The results show that both the effect of temperature on flow stress and its strain rate sensitivity of ECAPed Al is much larger than those of the coarse-grained Al. The temperature sensitivity of ultrafine-grained Al is comparatively weaker than that of the coarse-grained Al. Based on the experimental results, the apparent activation volume was estimated at different temperatures and strain rates. The forest dislocation interactions is the dominant thermally activated mechanism for ECAPed Al compressed at quasi-static strain rates, while the viscous drag plays an important role at high strain rates.展开更多
An experimental study of the microstructures in pure copper billets processed by 8 passes of equal channel angular extrusion （ECAE） via an extended range of processing routes with a 90° die is carried out. Each...An experimental study of the microstructures in pure copper billets processed by 8 passes of equal channel angular extrusion （ECAE） via an extended range of processing routes with a 90° die is carried out. Each processing route is defined according to the inter-pass billet rotation angle （χ）, which varies from 0° to 180°. According to the generation of high-angle boundaries and reduction of grain size by electron backscatter diffraction （EBSD） measurements, the grain refinement is found to be most efficient for route with χ=90°and least efficient with χ=180°, among the seven routes studied. This trend is supported by supplementary transmission electron microscopy （TEM） measurements. Comparison of the EBSD and TEM data reveals the importance of considering the non-equiaxity of grain structures in quantitative assessment of microstructural differences in ECAE-processed materials.展开更多
The effect of annealing temperature on the martensitic transformation of a Ti49.2Ni50.8 alloy processed by equal channel angular pressing （ECAP） was investigated by X-ray diffraction （XRD）, transmission electron m...The effect of annealing temperature on the martensitic transformation of a Ti49.2Ni50.8 alloy processed by equal channel angular pressing （ECAP） was investigated by X-ray diffraction （XRD）, transmission electron microscopy （TEM） and differential scanning calorimetry （DSC）. The as-ECAP processed and subsequently annealed Ti49.2Ni50.8 alloys consist of B2 parent phase, Ti4Ni2O phase and B19′ martensite at room temperature. Upon cooling, all samples show B2→R→B19′ two-stage transformation. Upon heating, when the annealing temperature is less than 400℃, the samples show B19′→R→B2 two-stage transformation; when the annealing temperature is higher than 500 ℃, the samples show B19′→B2 single-stage transformation. The B2-R transformation is characterized by wide interval due to the dislocations introduced during ECAP.展开更多
Angular unconformity is one of the most direct and strongest evidences for approving the tectonic movements of the earth's crust. Its dynamic genesis process has been understood to be mainly related to the compres...Angular unconformity is one of the most direct and strongest evidences for approving the tectonic movements of the earth's crust. Its dynamic genesis process has been understood to be mainly related to the compressional setting for a long time. Especially, in a detailed structural analysis for a specific region, when an angular unconformity is discovered people would regard it as the result of orogenic movements of a certain period or a certain episode and neglect the extensional facts. Based on a dialectical point of view of extension-compression, this paper has proved that angular unconformities can be formed not only in compressional settings, but also in extensional ones. Further more, their geological features are compared and he possible genetic mechanisms for angular unconformity under different dynamic settings are studied.展开更多
Ultra-fine grained （UFG） cylindrical tubes were produced via recently developed tubular channel angular pressing （TCAP） process through different passes from as-cast AZ91 magnesium alloy. The microstructure and me...Ultra-fine grained （UFG） cylindrical tubes were produced via recently developed tubular channel angular pressing （TCAP） process through different passes from as-cast AZ91 magnesium alloy. The microstructure and mechanical properties of processed tube through one to four passes of TCAP process at 200℃ were investigated. Microhardness of the processed tube was increased to 98.5 HV after one pass from an initial value of 67 Hr. An increase in the number of passes from one to higher number of passes has no more effect on the microhardness. Yield and ultimate strengths were increased by 4.3 and 1.4 times compared to those in as-cast condition. Notable increase in the strength was achieved after one pass of TCAP while higher number of passes has no more effect. Microstructural investigation shows notable decrease in the grain size to around 500 nm from the primary value of - 150 μm. Dissolution and distribution of hard MglTAI12 phase in the grain boundaries of dynamically recrystallized UFG AZ91 with a mean grain size of - 500 nm was an interesting issue of TCAP processing at 200 ℃ compared to other severe plastic deformation processes.展开更多
A combination of extrusion and equal channel angular pressing （ECAP） was used to deform a plain low carbon steel. This process consists of two successive deformations by extrusion and ECAP in a single die （Ex-ECAP...A combination of extrusion and equal channel angular pressing （ECAP） was used to deform a plain low carbon steel. This process consists of two successive deformations by extrusion and ECAP in a single die （Ex-ECAP）. Cylindrical samples were heated to predefined temperatures （650 and 850 ℃） and then pressed through a die channel with crosshead speed of 10 mm/s. Microstructure and resultant mechanical properties of processed material were studied. The results showed that pressing temperature has a significant effect on the resultant microstructure. While at 650 ℃, the cold worked structure with elongated ferrite grains were obtained, and at 850 ℃ the microstructure consisted of elongated ferrite grains and very fine grains at their boundaries as a consequence of continuous dynamic recrystallization （CDRX） of ferrite phase. Also at 850 ℃, a particular microstructure consisted of cold worked ferrite and static recrystallized grains on shear bands was obtained.展开更多
Microstructure evolution of processed Mg-Al-Zn alloy by equal channel angularextrusion(ECAE) in semi-solid isothermal treatment was investigated. The results show that withincreasing semi-solid isothermal treatment te...Microstructure evolution of processed Mg-Al-Zn alloy by equal channel angularextrusion(ECAE) in semi-solid isothermal treatment was investigated. The results show that withincreasing semi-solid isothermal treatment temperature, the a phase solid grain size of processedMg-Al-Zn alloy by ECAE increases firstly due to coarsening of a phase solid grains, then decreasesdue to melting of a phase solid grains. With the increase of extrusion passes during ECAE, the aphase solid grain size in the following semi-solid isothermal treatment decreases. The a phase solidgrain size of processed Mg-Al-Zn alloy by ECAE under route B_C is the smallest, while the a phasesolid grain size of processed material by ECAE under route A is the largest. The primary mechanismof spheroid formation depends on the melting of recrystallizing boundaries and diffusion of soluteatoms in the semi-solid state.展开更多
基金financially supported by the National Natural Science Foundation of China(No.52374395)the Natural Science Foundation of Shanxi Province,China(Nos.20210302123135,202303021221143)+5 种基金the Scientific and Technological Achievements Transformation Guidance Special Project of Shanxi Province,China(Nos.202104021301022,202204021301009)the Central Government Guided Local Science and Technology Development Projects,China(No.YDZJSX20231B003)the Ministry of Science and Higher Education of the Russian Federation for financial support under the Megagrant(No.075-15-2022-1133)the National Research Foundation(NRF)grant funded by the Ministry of Science and ICT of Korea through the Research Institute of Advanced Materials(No.2015R1A2A1A01006795)the China Postdoctoral Science Foundation(No.2022M710541)the Research Project supported by Shanxi Scholarship Council of China(No.2022-038)。
文摘To investigate the effect of microstructure evolution on corrosion behavior and strengthening mechanism of Mg-1Zn-1Ca(wt.%)alloys,as-cast Mg-1Zn-1Ca alloys were performed by equal channel angular pressing(ECAP)with 1 and 4 passes.The corrosion behavior and mechanical properties of alloys were investigated by optical microscopy(OM),scanning electron microscopy(SEM),electron backscatter diffraction(EBSD),electrochemical tests,immersion tests and tensile tests.The results showed that mechanical properties improved after ECAP 1 pass;however,the corrosion resistance deteriorated due to high-density dislocations and fragmented secondary phases by ECAP.In contrast,synchronous improvement in the mechanical properties and corrosion resistance was achieved though grain refinement after ECAP 4 passes;fine grains led to a significant improvement in the yield strength,ultimate tensile strength,elongation,and corrosion rate of 103 MPa,223 MPa,30.5%,and 1.5843 mm/a,respectively.The enhanced corrosion resistance was attributed to the formation of dense corrosion product films by finer grains and the barrier effect by high-density grain boundaries.These results indicated that Mg-1Zn-1Ca alloy has a promising potential for application in biomedical materials.
基金financially supported by Fund Program for Research Project Supported by Shanxi Scholarship Council of China(No.20230007)(jie bang guashuai)‘Open Competition’project:Preparation technology and product development of key new materials for 5G communication(No.20231207)+3 种基金Projects of the Patent Conversion Program in Shanxi Province(No.20241140)Research and Innovation Projects in Shanxi Province(No.2023KY633)Graduate Education Innovation Project at Taiyuan University of Science and Technology(No.BY2023003)Basic Research Plan Free Exploration of General Program in Shanxi Province(No.202303021221143).
文摘The low ductility and strong mechanical anisotropy of wrought magnesium alloys have hindered their further processing and application.In this study,AZ31 magnesium alloy sheet was prepared by a new asymmetrical angular rolling(AAR)process,compared with conventional symmetrical rolling(SR)process and asymmetrical rolling(ASR)process.The effects of three rolling processes on the microstructure,texture and mechanical properties of the alloy sheets were systematically studied.The results show that the AAR sheet exhibits excellent mechanical properties compared to other two rolling processes.It not only achieves the highest ductility of 17.9%,17.9%,and 18.5% in the three directions,but also has the lowest mechanical anisotropy values for yield strength,ultimate tensile strength and elongation.The AAR process significantly reduces the anisotropy of the material by achieving the smallest average grain size of 4.93μm and the most homogeneous grain size distribution.Introduced bi-directional asymmetric shear stresses randomizes grain orientation and activates the non-basal slip system,which also significantly reduces the anisotropy.In addition,the tensile twinning mechanism dominates during the AAR process,which contributes to texture weakening and the activation of the non-basal slip system.Through the synergy of these mechanisms,the AAR sheet is characterized by high ductility and low anisotropy.
基金supported by the National Natural Science Foundation of China(Grant No.62375140)the Open Research Fund of National Laboratory of Solid State Microstructures(Grant No.M36055).
文摘We propose a method to measure the flatness of an object with a petal-like pattern generated by the interference of the measured orbital angular momentum(OAM)beam and the reference OAM beam which carries the opposite OAM state.By calculating the difference between the petal rotation angle without/with the object,the thickness information of the object,and then the flatness information,can be evaluated.Furthermore,the direction of the object’s flatness can be determined by the petal’s clockwise/counterclockwise rotation.We theoretically analyze the relationship between the object’s thickness and petal rotation angle,and verify the proposed method by experiment.The experimental results show that the proposed method is a high precision flatness measurement and can obtain the convex/concave property of the flatness.For the 1.02 mm glass sample,the mean deviation of the flatness is 1.357×10^(-8) and the variance is 0.242×10^(-16).For the 0.50 mm glass sample,the mean deviation of the flatness is 1.931×10^(-8) and the variance is 2.405×10^(-16).Two different topological charges are adopted for the 2.00 mm glass sample,and their flatness deviations are 0.239×10^(-8)(ℓ=1)and 0.246×10^(-8)(ℓ=2),where their variances are 0.799×10^(-18)(ℓ=1)and 0.775×10^(-18)(ℓ=2),respectively.It is shown that the flatness measured by the proposed method is the same for the same sample when different topological charges are used.All results indicate that the proposed method may provide a high flatness measurement,and will be a promising way to measure the flatness.
基金Project supported by the National Natural Science Foundation of China (Grant Nos. 62071381 and 62301430)Shaanxi Fundamental Science Research Project for Mathematics and Physics (Grant No. 23JSY014)+1 种基金Scientific Research Plan Project of Shaanxi Education Department (Natural Science Special Project (Grant No. 23JK0680)Young Talent Fund of Xi’an Association for Science and Technology (Grant No. 959202313011)。
文摘Quantum secure direct communication(QSDC) is a communication method based on quantum mechanics and it is used to transmit secret messages. Unlike quantum key distribution, secret messages can be transmitted directly on a quantum channel with QSDC. Higher channel capacity and noise suppression capabilities are key to achieving longdistance quantum communication. Here, we report a continuous-variable QSDC scheme based on mask-coding and orbital angular momentum, in which the mask-coding is employed to protect the security of the transmitting messages and to suppress the influence of excess noise. The combination of orbital angular momentum and information block transmission effectively improves the secrecy capacity. In the 800 information blocks ×1310 bits length 10-km experiment, the results show a statistical average bit error rate of 0.38%, a system excess noise value of 0.0184 SNU, and a final secrecy capacity of 6.319×10~6 bps. Therefore, this scheme reduces error bits while increasing secrecy capacity, providing a solution for long-distance large-scale quantum communication, which is capable of transmitting text, images and other information of reasonable size.
基金Project(52275350)supported by the National Natural Science Foundation of ChinaProject(0301006)supported by the International Cooperative Scientific Research Platform of SUES,China。
文摘In this study,the interaction between deformation and precipitates during multiple equal channel angular pressing(ECAP)deformations and inter-pass aging combination and its effect on the mechanical properties of 7050 aluminum alloy are studied.The result show that ECAP induces numerous substructures and dislocations,effectively promoting the precipitation of theηʹphase exhibiting a bimodal structure during inter-pass aging.Following inter-pass aging and subsequent ECAP,the decrease in grain size(4.8μm)is together with the increase in dislocation density(1.24×10^(15) m^(−2))due to the pinning effect of the precipitated phase.Simultaneously,the dislocation motion causes the second phase particles to become even finer and more diffuse.The synergistic effects of precipitation strengthening,fine grain strengthening,and dislocation strengthening collectively enhance the high strength of aluminum alloys,with ultimate tensile strength and yield strength reaching approximately 610 and 565 MPa,respectively.Meanwhile,ductility remains largely unchanged,primarily due to coordinated grain boundary sliding and the uniform and fine dispersion of second phase particles.
基金the SERB,Department of Science and Technology,Government of India(Project No.EMR/2017/001456)aIISER Kolkata IPh.D fellowship for research.
文摘We demonstrate an effective and optimal strategy for generating spatially resolved longitudinal spin angular momentum(LSAM)in optical tweezers by tightly focusing the first-order spirally polarized vector(SPV)beams with zero intrinsic angular momentum into a refractive index stratified medium.The stratified medium gives rise to a spherically aberrated intensity profile near the focal region of the optical tweezers,with off-axis intensity lobes in the radial direction possessing opposite LSAM(helicities corresponding toσ=+1 and−1)compared to the beam center.We trap mesoscopic birefringent particles in an off-axis intensity lobe as well as at the beam center by modifying the trapping plane and observe particles spinning in opposite directions depending on their location.The direction of rotation depends on the particle size with larger particles spinning either clockwise or anticlockwise depending on the direction of spirality of the polarization of the SPV beam after tight focusing,while smaller particles spin in both directions depending on their spatial locations.Numerical simulations support our experimental observations.Our results introduce new avenues in spin-orbit optomechanics to facilitate novel yet straightforward avenues for exotic and complex particle manipulation in optical tweezers.
基金Project(BK20131373)supported by the Natural Science Foundation of Jiangsu ProvinceChina
文摘Commercial ZK60 Mg alloy was processed by multi-pass equal-channel angular pressing（ECAP） and subsequent aging to investigate the effect of grain refinement and second-phase redistribution on its corrosion behavior. Electrochemical tests show that the fine-grained samples after more ECAP passes have higher corrosion current densities（Jcorr） in the polarization curves, lower charge-transfer resistance（Rt） values in the EIS plots. The severe plastic deformation decreases the alloy corrosion resistance besides the well-known strengthening and toughening. Scanning Kelvin probe（SKP） measurement shows that the anodic and cathode sites are homogeneously distributed on the surface of the fine-grained alloy, which inhibits localized corrosion. The SKP potential, having linear relationship with the corrosion potential（φcorr）, decreases with increasing the ECAP pass. Furthermore, the post-ECAP aging can slightly improve the corrosion resistance of the fine-grained ZK60 Mg alloy and enhance the comprehensive performances, due to the stress relief and uniform distribution of second-phase particles.
基金Project(B08040)supported by the Program of Introducing Talents of Discipline to Universities(111 Project),ChinaProject(2009ZX04005-031-11)supported by the National Science and Technology Special Program,China
文摘To manufacture plate by the combination of equal channel angular processing （ECAP） and porthole die extrusion techniques, a novel technique, namely portholes-equal channel angular processing （P-ECAP）, was studied. Extrusion of AL6005A plate used for the bullet train plate was investigated by finite element method. The relevant porthole dies involving ECAP technique in channels were designed. Dimensional changes in the scrap part of the extrudate obtained after extrusion from the P-ECAP die, with different channel angles, were predicted. Effects of the channel angle and extrusion speed on the maximum temperature of the workpiece and other field variables were evaluated. At the channel angle of 160° of P-ECAP dies, the extrudate exhibited the optimal performance and the least amount of extrudate scrap was obtained. The optimal extrusion speed was 3-5 mm/s. Moreover, with the increase in ram speed from 1 to 9 mm/s, the peak extrusion load increased by about 49% and the maximum temperature was increased by about 70 ℃. The effective strain exhibited ascending trend in the comer of the ECAP deformation zone. In the solder seam and the side of die bearing of extrudate, the maximum principal stresses were tensile stress.
基金Project(51401177)supported by the National Natural Science Foundation of ChinaProject(13KJD430005)supported by the Natural Science Foundation of Jiangsu Higher Education Institutions of ChinaProject(JSKLEDC201309)supported by Jiangsu Key Laboratory of Large Engineering Equipment Detection and Control,China
文摘In comparison with the conventional equal channel angular pressing（ECAP） process,a comprehensive study of influence of twist extrusion（TE） process on consolidating pure aluminum powder in tubes（PITs） by equal channel angular pressing and torsion（ECAPT） was conducted via three-dimensional（3D） finite element simulation,experimental investigation and theoretical analysis.Simulation results revealed that during the consolidation of aluminum powder particles by ECAPT,TE process played a significant role of back pressure.Due to the torsional shear and high hydrostatic pressure exerted by twist channel,both the magnitude and homogeneity of the effective strain were increased markedly.After one pass of ECAPT process using a square channel with an inner angle of 90° and a twist slope angle of 36.5° at 200℃,commercial pure aluminum powder particles were successfully consolidated to nearly full density.Simulation and experimental results showed good agreement.In the microstructure observations,grains were greatly refined.At the same time,porosities were effectively eliminated by shrinking in size and breaking into small ones.Microhardness test indicated that strain distribution of ECAPT-processed billet was more homogeneous with respect to the ECAP-processed one.All these improvements may be attributed to the extreme intense shear strain induced during ECAPT and the increase in self-diffusion coefficient of aluminum due to the back pressure exerted by TE process.
文摘Microstructure evolution and texture development and their effects on mechanical properties of a Mg-Gd-Y-Zr alloy during equal channel angular pressing（ECAP） were investigated.It is found that the microstructure is still inhomogeneous after four passes,and two zones,namely the fine grain zone（FGZ） and the coarse grain zone（CGZ） are formed.The grain refinement occurs mainly by particle-stimulated nucleation（PSN） mechanism,which led to a more random texture after four passes of ECAP.In the ECAP-processed alloy,the strength did not increase while the ductility was enhanced dramatically compared with the as-received condition.The change of ductility of this alloy was discussed in terms of texture and second phase particles.
基金Project(50875072)supported by the National Natural Science Foundation of ChinaProject(121053)supported by Fok Ying Tong Education FoundationProject(20100111110003)supported by Specialized Research Fund for the Doctoral Program of Higher Education,China
文摘Consolidation of pure Alpowder was conducted at 200 ℃ by equal channel angular pressing and torsion （ECAPT） method. The grain refinement and consolidation behavior were deeply investigated by scan electronic microscopy （SEM） and transmission electronic microscopy （TEM）. The density, hardness and room temperature compression properties of the deformed samples were measured. The experiment results show that ECAPT is an effective method of consolidating powders at relatively low temperatures. Pure A1 particles are successfully consolidated into dense bulk material after 4 passes of ECAPT at 200 ℃. The consolidated material possesses fine grain structure and excellent mechanical properties. The refinement and consolidation mechanisms were analyzed. ECAPT is a promising method to produce the high-performance bulk materials from particles.
基金Projects(11272267,11102168,10932008)supported by the National Natural Science Foundation of ChinaProject(B07050)supported by Northwestern Polytechnical University
文摘Uniaxial compressive experiments of ultrafine-grained Al fabricated by equal channel angular pressing(ECAP) method were performed at wide temperature and strain rate range. The influence of temperature on flow stress, strain hardening rate and strain rate sensitivity was investigated experimentally. The results show that both the effect of temperature on flow stress and its strain rate sensitivity of ECAPed Al is much larger than those of the coarse-grained Al. The temperature sensitivity of ultrafine-grained Al is comparatively weaker than that of the coarse-grained Al. Based on the experimental results, the apparent activation volume was estimated at different temperatures and strain rates. The forest dislocation interactions is the dominant thermally activated mechanism for ECAPed Al compressed at quasi-static strain rates, while the viscous drag plays an important role at high strain rates.
基金Project(50871040)supported by the National Natural Science Foundation of ChinaProject(NCET-06-0741)supported by the Program for New Century Excellent Talents of China
文摘An experimental study of the microstructures in pure copper billets processed by 8 passes of equal channel angular extrusion （ECAE） via an extended range of processing routes with a 90° die is carried out. Each processing route is defined according to the inter-pass billet rotation angle （χ）, which varies from 0° to 180°. According to the generation of high-angle boundaries and reduction of grain size by electron backscatter diffraction （EBSD） measurements, the grain refinement is found to be most efficient for route with χ=90°and least efficient with χ=180°, among the seven routes studied. This trend is supported by supplementary transmission electron microscopy （TEM） measurements. Comparison of the EBSD and TEM data reveals the importance of considering the non-equiaxity of grain structures in quantitative assessment of microstructural differences in ECAE-processed materials.
基金Project(51001035)supported by the National Natural Science Foundation of ChinaProject(LBH-Q14035)supported by the Postdoctoral Funds for Scientific Research Initiation of Heilongjiang Province,ChinaProject(HEUCF20151002)supported by the Fundamental Research Funds for the Central Universities,China
文摘The effect of annealing temperature on the martensitic transformation of a Ti49.2Ni50.8 alloy processed by equal channel angular pressing （ECAP） was investigated by X-ray diffraction （XRD）, transmission electron microscopy （TEM） and differential scanning calorimetry （DSC）. The as-ECAP processed and subsequently annealed Ti49.2Ni50.8 alloys consist of B2 parent phase, Ti4Ni2O phase and B19′ martensite at room temperature. Upon cooling, all samples show B2→R→B19′ two-stage transformation. Upon heating, when the annealing temperature is less than 400℃, the samples show B19′→R→B2 two-stage transformation; when the annealing temperature is higher than 500 ℃, the samples show B19′→B2 single-stage transformation. The B2-R transformation is characterized by wide interval due to the dislocations introduced during ECAP.
基金the National Natural Science Foundation(grant 40373005)the Foundation of Sichuan Province for Training Outstanding Young Leaders of V arious Disciplines(No.02ZQ026-046)the Foundation of Sichuan Province for Training Scientific and Technological Leaders in the Year 2003(No.2200336)
文摘Angular unconformity is one of the most direct and strongest evidences for approving the tectonic movements of the earth's crust. Its dynamic genesis process has been understood to be mainly related to the compressional setting for a long time. Especially, in a detailed structural analysis for a specific region, when an angular unconformity is discovered people would regard it as the result of orogenic movements of a certain period or a certain episode and neglect the extensional facts. Based on a dialectical point of view of extension-compression, this paper has proved that angular unconformities can be formed not only in compressional settings, but also in extensional ones. Further more, their geological features are compared and he possible genetic mechanisms for angular unconformity under different dynamic settings are studied.
基金financially supported by Iran National Science Foundation(INSF)
文摘Ultra-fine grained （UFG） cylindrical tubes were produced via recently developed tubular channel angular pressing （TCAP） process through different passes from as-cast AZ91 magnesium alloy. The microstructure and mechanical properties of processed tube through one to four passes of TCAP process at 200℃ were investigated. Microhardness of the processed tube was increased to 98.5 HV after one pass from an initial value of 67 Hr. An increase in the number of passes from one to higher number of passes has no more effect on the microhardness. Yield and ultimate strengths were increased by 4.3 and 1.4 times compared to those in as-cast condition. Notable increase in the strength was achieved after one pass of TCAP while higher number of passes has no more effect. Microstructural investigation shows notable decrease in the grain size to around 500 nm from the primary value of - 150 μm. Dissolution and distribution of hard MglTAI12 phase in the grain boundaries of dynamically recrystallized UFG AZ91 with a mean grain size of - 500 nm was an interesting issue of TCAP processing at 200 ℃ compared to other severe plastic deformation processes.
文摘A combination of extrusion and equal channel angular pressing （ECAP） was used to deform a plain low carbon steel. This process consists of two successive deformations by extrusion and ECAP in a single die （Ex-ECAP）. Cylindrical samples were heated to predefined temperatures （650 and 850 ℃） and then pressed through a die channel with crosshead speed of 10 mm/s. Microstructure and resultant mechanical properties of processed material were studied. The results showed that pressing temperature has a significant effect on the resultant microstructure. While at 650 ℃, the cold worked structure with elongated ferrite grains were obtained, and at 850 ℃ the microstructure consisted of elongated ferrite grains and very fine grains at their boundaries as a consequence of continuous dynamic recrystallization （CDRX） of ferrite phase. Also at 850 ℃, a particular microstructure consisted of cold worked ferrite and static recrystallized grains on shear bands was obtained.
基金Projects(50475029,50605015) supported by the National Natural Science Foundation of China
文摘Microstructure evolution of processed Mg-Al-Zn alloy by equal channel angularextrusion(ECAE) in semi-solid isothermal treatment was investigated. The results show that withincreasing semi-solid isothermal treatment temperature, the a phase solid grain size of processedMg-Al-Zn alloy by ECAE increases firstly due to coarsening of a phase solid grains, then decreasesdue to melting of a phase solid grains. With the increase of extrusion passes during ECAE, the aphase solid grain size in the following semi-solid isothermal treatment decreases. The a phase solidgrain size of processed Mg-Al-Zn alloy by ECAE under route B_C is the smallest, while the a phasesolid grain size of processed material by ECAE under route A is the largest. The primary mechanismof spheroid formation depends on the melting of recrystallizing boundaries and diffusion of soluteatoms in the semi-solid state.
