Microcapsules containing various flavour/fragrance oils with different properties were fabricated using gelatine and gum arabic by complex coacervation.The surface properties(surface polarity and the spreading coeffic...Microcapsules containing various flavour/fragrance oils with different properties were fabricated using gelatine and gum arabic by complex coacervation.The surface properties(surface polarity and the spreading coefficients)of core oils were investigated in order to evaluate their effects on the capsule morphology and encapsulation efficiency based on a spreading coefficient and two component surface energy theory.Contact angles,interfacial tensions,and surface polarities were measured,and results were discussed with respect to the internal structure as well as encapsulation efficiency of different oil microcapsules.The thermodynamic spreading coefficients theory did not give an exactly accurate prediction of capsule morphology using high molecular weight biopolymer as the wall material in this work.Notwithstanding,the morphology predictions for different oil microcapsules are holistically consistent with the values of their encapsulation efficiency.Also,it has been found that the encapsulation efficiency increased with the decreasing surface polarity of the core oil holistically.展开更多
A miniature process for separating the oil phase from dilute oil/water emulsion is developed.This process applies a confined space apparatus,which is a thin flow channel made of two parallel plastic plates.The space b...A miniature process for separating the oil phase from dilute oil/water emulsion is developed.This process applies a confined space apparatus,which is a thin flow channel made of two parallel plastic plates.The space between the two plates is rather narrow to improve the collisions between oil droplets and the plate surface.Oil droplets have an affinity for the plate surface and thus are captured,and then coalesce onto the surface.The droplet size distribution of the residual emulsion resulted from the separation process is remarkably changed.The oil layer on the plate weakens the further separation of oil droplets from the emulsion.Three types of plate materials,polypropylene(PP),polytetrafluoroethylene(PTFE) and nylon 66,were used.It is found that PP is the best in terms of the oil separation efficiency and nylon 66 is the poorest.The interaction between droplets in the emulsion and plate surface is indicated by the spreading coefficient of oil droplet on the plate in aqueous environment,and the influences of formed oil layer and plate material on the separation efficiency are discussed.展开更多
基金the technical supports from the staffs of the School of Chemical Engineering,University of Birmingham,West Midlands,B152 TT,UK.
文摘Microcapsules containing various flavour/fragrance oils with different properties were fabricated using gelatine and gum arabic by complex coacervation.The surface properties(surface polarity and the spreading coefficients)of core oils were investigated in order to evaluate their effects on the capsule morphology and encapsulation efficiency based on a spreading coefficient and two component surface energy theory.Contact angles,interfacial tensions,and surface polarities were measured,and results were discussed with respect to the internal structure as well as encapsulation efficiency of different oil microcapsules.The thermodynamic spreading coefficients theory did not give an exactly accurate prediction of capsule morphology using high molecular weight biopolymer as the wall material in this work.Notwithstanding,the morphology predictions for different oil microcapsules are holistically consistent with the values of their encapsulation efficiency.Also,it has been found that the encapsulation efficiency increased with the decreasing surface polarity of the core oil holistically.
基金Supported by the Eleventh Five-Year Plan of national support (2007BAI26B03-04)
文摘A miniature process for separating the oil phase from dilute oil/water emulsion is developed.This process applies a confined space apparatus,which is a thin flow channel made of two parallel plastic plates.The space between the two plates is rather narrow to improve the collisions between oil droplets and the plate surface.Oil droplets have an affinity for the plate surface and thus are captured,and then coalesce onto the surface.The droplet size distribution of the residual emulsion resulted from the separation process is remarkably changed.The oil layer on the plate weakens the further separation of oil droplets from the emulsion.Three types of plate materials,polypropylene(PP),polytetrafluoroethylene(PTFE) and nylon 66,were used.It is found that PP is the best in terms of the oil separation efficiency and nylon 66 is the poorest.The interaction between droplets in the emulsion and plate surface is indicated by the spreading coefficient of oil droplet on the plate in aqueous environment,and the influences of formed oil layer and plate material on the separation efficiency are discussed.