A required finite element method（FEM） model applicable for narrow gap CMT and CMT＋P MIX welding was established based on the interactions between arc,base metal and filler metal.A novel method of simplifying wire f...A required finite element method（FEM） model applicable for narrow gap CMT and CMT＋P MIX welding was established based on the interactions between arc,base metal and filler metal.A novel method of simplifying wire feeding pulses and heat input pulses was supposed under the conduction of equivalent input.The method together with composed double-ellipse heat sources was included in the model.The model was employed in the investigation of thermal cycling and the identification of the softened zone of AA7A52 base plates.Low-frequency behavior emerged in the form of low-cooling rate sects,which were not expected under experimental conditions.The softened zone including the quenched zone and averaging zone of the base plate was much wider internal the base plate than that close to the surfaces.The reliability of the predictions in thermal cycling was supported by infrared imaging test results of the thermal cycle process.展开更多
Using the Gleeble 3500 thermal-mechanical system to simulate thermal cycles with different peak temperatures, the hardness and microstructure in the heat-affected zones of two kinds of 100 kg class hot-rolled extra-hi...Using the Gleeble 3500 thermal-mechanical system to simulate thermal cycles with different peak temperatures, the hardness and microstructure in the heat-affected zones of two kinds of 100 kg class hot-rolled extra-high-strength steel were compared. When the peak temperature of the thermal cycle was 800℃ ,incomplete transformation occurred during quenching in both steels, and massive martensite and bainite grains were formed. The hardness was determined by the composition and distribution of the microstructure. The concentration of massive martensite was low, and hence the hardness was low,in steel #1. Conversely,the massive martensite content in steel #2 was high and uniformly distributed,resulting in a high hardness. These findings can provide a reference for improving the mechanical properties in the softened zone.展开更多
Mouthguard thickness is affected by the softened state of the sheet during thermoforming. The aim of this study is to establish an effective method for controlling the softened state of the sheet to prevent the mouthg...Mouthguard thickness is affected by the softened state of the sheet during thermoforming. The aim of this study is to establish an effective method for controlling the softened state of the sheet to prevent the mouthguard thickness from decreasing during mouthguard fabrication using a vacuum-forming machine. Mouthguards were thermoformed using an ethylene-vinyl acetate sheet (thickness: 4.0 mm) and a vacuum-forming machine. The working model was trimmed to the anterior height of 25 mm and the posterior height of 20 mm. The following two heating methods were compared: 1) the sheet was formed when it sagged 15 mm below the level of the sheet frame at the top of the post (condition T);and 2) the sheet frame was lowered to and heated at 50 mm below its usual height and the sheet was formed when it sagged 15 mm below the level of the sheet frame (condition L). For each heating method, the vacuum was applied immediately (T0, L0) or 5 s (T5, L5) after the sheet frame was lowered to the forming unit. The sheet surface temperature immediately before the vacuum was applied under each condition was measured. The differences in mouthguard thickness due to forming conditions were analyzed by one-way ANOVA and Bonferroni’s multiple comparison tests. The temperature difference between the center and the posterior depending on the condition decreased in the order T0 > T5 > L0 > L5, and that was 20<span style="white-space:nowrap;">°</span>C or higher for T0 and T5, and 10<span style="white-space:nowrap;">°</span>C or less for L0 and L5. At the incisal edge and the cusp, L0 and L5 were significantly thicker than T0. No significant differences were observed between conditions L0 and L5 at any measurement points. For the labial and buccal surfaces, significant differences in thicknesses among all conditions, except L0 and L5, were observed and were in the order T0 < T5 < L0 and L5. This study was suggested that the lowering the sheet frame and heating was more effective than adjusting the vacuum timing for uniform softening of the sheet.展开更多
This study focuses on a new and high-efficiency approach in a unified sense of accurately simulating strength-degrading effects for geomaterials,including non-symmetric hardening-to-softening effects in tension and co...This study focuses on a new and high-efficiency approach in a unified sense of accurately simulating strength-degrading effects for geomaterials,including non-symmetric hardening-to-softening effects in tension and compression as well as non-symmetric tensile and compressive stiffness-degrading effects during unloading.It is intended to bypass both modeling and numerical complexities involved in existing approaches.To this goal,new elastoplastic equations are established with new numerical techniques.With a decoupling technique of treating tension-compression asymmetry,the foregoing complex effects are automatically incorporated as inherent response features of the new elastoplastic equations,thus bypassing usual modeling complexities.A new numerical technique of renormalizing piecewise spline functions is introduced to resolve the central yet tough issue of obtaining accurate and unified expressions for the tensile and compressive strength functions,thus bypassing usual numerical complexities and uncertainties in treating numerous unknown parameters and multiple ad hoc criteria.As such,the new approach is not only of wide applicability for various geomaterials but also of high computational efficiency with no more than three adjustable parameters.Toward validating the efficacy of the new approach,numerical examples for granite,salt rock,and sandstone-concrete combined body as well as plain concrete,high-performance concrete,and ultrahigh-performance concrete are presented by comparing model predictions with multiple data sets for strength-degrading effects in tension and compression.展开更多
Ascorbate(Asc),commonly known as vitamin C,is a vital molecule for plant growth,development,and stress resilience.It is also known to play a crucial role in various physiological processes,including photosynthesis,cel...Ascorbate(Asc),commonly known as vitamin C,is a vital molecule for plant growth,development,and stress resilience.It is also known to play a crucial role in various physiological processes,including photosynthesis,cell division,and differentiation.This article thoroughly explores the processes governing the metabolism of Asc in plants and its roles in physiological functions.It lays down a robust theoretical groundwork for delving into Asc production,transportation,functions,and its potential applications in stress alleviation and horticulture.Furthermore,recent studies indicate that Asc plays a role in regulating fruit development and affecting postharvest storage characteristics,thereby influencing fruit ripening and resilience to stress.Hence,there is a growing importance in studying the synthesis and utilization of Asc in plants.Although the critical role of Asc in controlling plant redox signals has been extensively studied,the precise mechanisms by which it manages cellular redox homeostasis to maintain the equilibrium between reactive oxygen scavenging and cell redox signaling remain elusive.This gap in knowledge presents fresh opportunities to explore how the production of Asc in plants is regulated and how plants react to environmental stressors.Furthermore,this article delves into the potential for a comprehensive investigation into the essential function of Asc in fruits,the development of Asc-rich fruits,and the enhancement of postharvest storage properties.展开更多
Softening of fleshy fruits during ripening and postharvest is a programmed physiological process that substantially impacts fruit quality and shelf life.However,the molecular mechanism underlying peach softening remai...Softening of fleshy fruits during ripening and postharvest is a programmed physiological process that substantially impacts fruit quality and shelf life.However,the molecular mechanism underlying peach softening remains largely unknown.Lateral organ boundary(LOB)domain(LBD)proteins are pivotal regulators of plant growth and development.To date,certain LOB/LBD transcription factors are seemingly implicated in fruit softening.In this study,we identified 42 LOB/LBD genes in the peach genome.Expression analysis showed a significant upregulation of PpLOB1 transcripts toward peach fruit ripening.PpLOB1 was classified into Class II subgroup,and showed high sequence similarity to several softening-related LOB/LBD transcription factors.Transient transformation assays showed that PpLOB1 positively modulates peach softening.Further experiments demonstrated that PpLOB1 directly targets and activates the promoters of pectate lyase 1(PpPL1)and PpPL15,thereby contributing to the regulation of fruit softening.Additionally,PpNAP4 up-regulates PpLOB1 expression by binding to its promoter.Meanwhile,our findings revealed that PpNAP4 and PpNAP6 cooperatively modulate the expression of Pp LOB1.Taken together,our findings revealed a novel regulatory module involving PpNAP4 and PpLOB1 that modulates peach fruit softening.展开更多
Granular materials exhibit complex macroscopic mechanical behaviors closely related to their microscalemicrostructural features.Traditional macroscopic phenomenological elasto-plastic models,however,usually have compl...Granular materials exhibit complex macroscopic mechanical behaviors closely related to their microscalemicrostructural features.Traditional macroscopic phenomenological elasto-plastic models,however,usually have complex formulations and lack explicit relations to these microstructural features.To avoid these limitations,this study proposes a micromechanics-based softening hyperelastic model for granular materials,integrating softening hyperelasticity withmicrostructural insights to capture strain softening,critical state,and strain localization behaviors.The model has two key advantages:(1)a clear conceptualization,straightforward formulation,and ease of numerical implementation(via Abaqus UMAT subroutine in this study);(2)explicit incorporation of micro-scale features(e.g.,contact stiffness,particle size,porosity)to reveal their influences on macroscopic responses.An isotropic directional distribution density of contacts and three specific microstructures are considered,and their softening hyperelastic constitutive modulus tensors are explicitly derived.By introducing a softening factor and critical failure energy density,the model can describe geomaterial behaviors,simulating residual strength,X-shaped shear bands,and strain localization evolution.Numerical validations in comparison with themacro-scale hyperelastic model,Abaqus Drucker-Prager model,and the experiment confirm its accuracy.Parametric studies reveal critical dependencies:a normal to tangential contact stiffness ratio of 2-8(depending on stiffness magnitude),an internal length of 2-4 mm to ensure shear band formation,and a critical failure energy density(≤10 kJ/m^(3))to trigger strain softening and localization.Influences of the specific microstructures on strain localization and softening are investigated.The model also shows mesh independence due to the introduction of an internal length.The model’s applicability is further demonstrated by slope stability analysis,capturing slip surface evolution,and load-displacement characteristics.This study develops a robust microstructure-aware hyperelastic framework to describe the mechanical behaviors of granular materials,providing multiscale insights for geotechnical engineering applications.展开更多
In this study,a 1400 MPa-grade ultra-high-strength steel thin-plate butt-welded joint was selected as the research object,and the joint was fabricated using the metal inert gas(MIG)welding process with ER307Si filler ...In this study,a 1400 MPa-grade ultra-high-strength steel thin-plate butt-welded joint was selected as the research object,and the joint was fabricated using the metal inert gas(MIG)welding process with ER307Si filler wire.Residual stress distributions were measured via the hole-drilling method,while micro-hardness was assessed using a micro-hardness tester.Simultaneously,both transverse shrinkage and angular distortion of the welded joint were experimentally determined.According to the hardness distribution of the joint,a thermalmetallurgical-mechanical finite element model was developed based on SYSWELD software platform.This model incorporates solid-state phase transformations(SSPT)and softening effect in the HAZ,as well as strain hardening and annealing behaviors in the weld metal.The temperature field,residual stress distribution,and welding deformation of single-pass butt-welded joint were simulated by the developed computational method.The simulation results were validated against experimental measurements,confirming the accuracy and reliability of the proposed computational approach.Furthermore,based on the numerical results,the influence mechanisms of SSPT and material softening on residual stress and deformation were analyzed.The findings indicate that SSPT exhibits considerable influences on the magnitude and distribution of welding residual stress.It reduces the peak longitudinal residual stress from 1620 MPa to 1350 MPa and increases the peak transverse residual stress from 350 MPa to 402 MPa.The results also manifest that the softening effect further reduces the peak longitudinal residual stress by 300 MPa,while exhibits minor effect on transverse residual stress.However,the results show that neither the SSPT nor the softening effect presents obvious influence on welding deformation.展开更多
Characterization of mechanical alterations of shale constituent phases is critical for an in-depth understanding of the underlying mechanisms of shale softening.In this study,a hydro-thermal reaction system is set up ...Characterization of mechanical alterations of shale constituent phases is critical for an in-depth understanding of the underlying mechanisms of shale softening.In this study,a hydro-thermal reaction system is set up to mimic the interactions between shale and water-based fluids under the subsurface environment in shale formations.Using a coupled analysis of grid nanoindentation and in situ mineralogical identification,mechanical alterations of shale constituent mineral phases are revealed.Mechanical degradation of carbonate and clay phases is 10 times greater than quartz,pyrite and organic phases.The KCl additive greatly mitigates mechanical degradation of the clay phase.The high temperature and pressure results in a mechanical degradation of carbonate minerals as much as three times of that occurs at room temperature and atmospheric pressure.Multiscale mechanical models,which are established based on Mori-Tanaka(MT)and self-consistent(SC)schemes,predict more accurate elastic softening of shale composite than the microindentation experiments,due to the microcracks generated in the experiments.Based on the calculation of the multiscale mechanical model,under the subsurface environment of shale formations(e.g.80℃ and 8 MPa),the carbonate dissolution leads to a reduction in Young's modulus of shale composite by about 30%,while the degradation of clay minerals only causes a reduction by up to 9%.展开更多
In the field of rock engineering,the influence of water is a dynamic process that exhibits varying effects over time and across different locations.To further understand how water influences the mechanical properties ...In the field of rock engineering,the influence of water is a dynamic process that exhibits varying effects over time and across different locations.To further understand how water influences the mechanical properties and acoustic emission(AE)behavior of rocks,this study conducted uniaxial compression experiments on sandstones with varying degrees of wetting under both natural conditions and water-chemical environments.In addition,the study combined AE equipment with digital image correlation(DIC)to monitor the entire failure process.Using the sliding window algorithm,the variation in the variance of AE characteristic parameters during the process of sandstone loading to failure is analyzed from the perspective of critical slowing down.This analysis enables the effective identification of the early warning signal before failure.The experimental findings suggest that an increase in wetting height results in a gradual decrease in peak stress,accompanied by a concomitant increase in the percentage of shear cracks.The characteristic parameters,including energy,amplitude,and ringing count,all exhibit critical slowing phenomena.The waveform of AE characteristic parameters of the same sample is similar,and the mutation time of the precursor signal is roughly the same.All signals appear in the irreversible plastic deformation stage of microcrack initiation.The integration of critical slowing down theory and the b-value early warning method facilitates a more comprehensive evaluation of the stability of rock mass,thereby significantly enhancing the efficiency and safety of disaster prevention measures.展开更多
Single-pass and double-pass high-temperature deformation experiments were conducted on 40Cr10Si2Mo steel using a Gleeble-3500 thermal simulator.The static recrystallization(SRX)behavior and recrystallization mechanism...Single-pass and double-pass high-temperature deformation experiments were conducted on 40Cr10Si2Mo steel using a Gleeble-3500 thermal simulator.The static recrystallization(SRX)behavior and recrystallization mechanisms of 40Cr10Si2Mo steel were investigated under deformation temperatures of 900-1100℃,deformation strains of 10%,20%,and 30%,and inter-pass times of 1-120 s.A static recrystallization fraction model was developed.The results showed that the SRX volume fraction increased with higher deformation temperature,larger deformation amount,and longer inter-pass time,with the deformation temperature having the most significant effect on SRX.During the deformation process,different process parameters led to different internal deformation mechanisms of the material.Static recovery and continuous static recrystallization(CSRX)dominated deformation at lower temperatures through progressive lattice rotation.In comparison,at higher temperatures,the deformation mechanism was dominated by CSRX and discontinuous static recrystallization(DSRX).The nucleation mechanisms of the SRX process were grain boundary bulging nucleation and subgrain merging nucleation,with grain boundary bulging present under all conditions.Subgrain merging nucleation could provide an additional nucleation mode at lower deformation temperatures or lower deformation amounts.Based on the traditional Avarmi equation,a modified model coefficient was used to establish the SRX kinetic model for 40Cr10Si2Mo steel.The linear correlation coefficient R^(2) between the predicted and experimental static recrystallization volume fraction was 0.96702,indicating high prediction accuracy.展开更多
It has long been hypothesized that an increase in the extracellular matrix(ECM)stiffness mechanoactivates malignant phenotypes of breast tumor cells by regulating an array of processes underlying cancer biology.Althou...It has long been hypothesized that an increase in the extracellular matrix(ECM)stiffness mechanoactivates malignant phenotypes of breast tumor cells by regulating an array of processes underlying cancer biology.Although the contribution of substrate stiffening to drive malignant phenotype traits and other biological functions of a tumor is increasingly understood,the functional role of substrate softening on breast cancer cellular responses has rarely been investigated.Herein,we employed matrix metalloproteinase(MMP)-sensitive film to perform assays to explore the consequences of lowering stiffness on the biological behaviors of breast cancer cell MDA-MB-231.We demonstrated that cells underwent dramatic changes in migration,cellular conjunction,and expression of malignance-associated proteins and genes when the substrate stiffness decreased.Based on RNA sequencing and analysis,we found that hub genes including TP53,CCND1,MYC,CTNNB1,and YAP were validated to play central parts in regulating stiffness-dependent cellular manner change.Moreover,through visualization of differentially expressed genes(DEGs),cells on dynamically softened substrate appeared less influenced by transfer to tissue culture polystyrene(TCPS).These results suggest substrates with decreasing stiffness could normalize breast tumor malignant phenotype and help cells store the mechanical memory of the consequential weaker malignance.展开更多
This study examined the feasibility of utilizing high-pressure processing(HPP)with enzymatic impregnation to soften vegetables.Freeze-thaw(FT)processing was used as a positive control to compare the hardness,physicoch...This study examined the feasibility of utilizing high-pressure processing(HPP)with enzymatic impregnation to soften vegetables.Freeze-thaw(FT)processing was used as a positive control to compare the hardness,physicochemical characteristics,and cell microstructure of vegetables.Carrot and broccoli samples were subjected to 200 MPa pressure for 15 min and then impregnated using a Viscozyme L enzyme solution.Compared with the hardness of fresh samples,the hardness of the carrot and broccoli samples that underwent HPP and enzymatic impregnation decreased by 84.6%and 95.5%,respectively,and the hardness of the carrot and broccoli samples that underwent FT processed decreased by 73.6%and 91.3%,respectively.In particular,HPP with enzymatic impregnation reduced the content of insoluble dietary fibers(18%),increased the content of soluble dietary fibers(3%),and considerably increased the concentration of carotene(1.9 times)and isothiocyanate(4.5 times)in carrots and broccoli,respectively.Scanning electron microscopy reveals that HPP physically damaged the intercellular compartments of the vegetables,thereby increasing the impregnation of enzymes.In addition,the level of HPP and the holding time increased,and the amount of vegetable residue and the degree of moisture retention substantially decreased,indicating a negative correlation between damage and hardness.Moreover,HPP pretreatment require a short processing time then FT,which promoted the penetration of enzymes and the internal microstructural biodegradation of vegetables,and it also helped these vegetables release more soluble nutrients.Overall,HPP can be used with enzymatic impregnation to obtain texture-modified vegetables for older consumers with mastication difficulties.展开更多
In this paper,the work hardening and softening behavior of AZ31 magnesium alloy sheets by hard plate accumulative roll bonding(HP-ARB)process in a specific temperature range was studied for the first time,and the cycl...In this paper,the work hardening and softening behavior of AZ31 magnesium alloy sheets by hard plate accumulative roll bonding(HP-ARB)process in a specific temperature range was studied for the first time,and the cyclic stress relaxation test,EBSD,TEM and other characterization methods were used.When the rolling temperature is 350℃,the grain size of magnesium sheets is refined to 4.32(±0.36)μm on average,and it shows an excellent combination of strength and plasticity.The tensile strength reaches 307(±8.52)MPa and the elongation is 12.73(±0.84)%.At this time,the curve of work hardening rate decreases smoothly and the degree of hardening is the lowest,and the amplitude of stress drop △σ_(p) in work softening test is the smallest with the increase of cycle times,which shows that the well coordination between work hardening and softening behavior has been achieved.Research has found that the combined effect of grain boundary strengthening and fine grain strengthening enhances the yield and tensile strength of magnesium sheets after three passes HP-ARB process at 350℃.This is attributed to the high degree of dislocation slip opening in the pyramidal surfaceand<c+a>,which not only coordinates the c-axis strain of the entire grain,but also promotes the slip transfer of dislocations in the fine-grained region,significantly improving the elongation of the sheets.This study provides a new idea for the forming and manufacturing of high performance magnesium alloy sheets.展开更多
Large interfacial strains in particles are crucial for promoting bonding in cold spraying(CS),initiated either by adiabatic shear instability(ASI)due to softening prevailing over strain hardening or by hydrostatic pla...Large interfacial strains in particles are crucial for promoting bonding in cold spraying(CS),initiated either by adiabatic shear instability(ASI)due to softening prevailing over strain hardening or by hydrostatic plasticity,which is claimed to promote bonding even without ASI.A thorough microstructural analysis is vital to fully understand the bonding mechanisms at play during microparticle impacts and throughout the CS process.In this study,the HEA CoCrFeMnNi,known for its relatively high strain hardening and resistance to softening,was selected to investigate the microstructure characteristics and bonding mech-anisms in CS.This study used characterization techniques covering a range of length scales,including electron channeling contrast imaging(ECCI),electron backscatter diffraction(EBSD),and high-resolution transmission microscopy(HR-TEM),to explore the microstructure characteristics of bonding and overall structure development of CoCrFeMnNi microparticles after impact in CS.HR-TEM lamellae were prepared using focused ion beam milling.Additionally,the effects of deformation field variables on microstructure development were determined through finite element modeling(FEM)of microparticle impacts.The ECCI,EBSD,and HR-TEM analyses revealed an interplay between dislocation-driven processes and twinning,leading to the development of four distinct deformation microstructures.Significant grain refinement occurs at the interface through continuous dynamic recrystallization(CDRX)due to high strain and temperature rise from adiabatic deformation,signs of softening,and ASI.Near the interface,a necklace-like structure of refined grains forms around grain boundaries,along with elongated grains,resulting from the coexistence of dynamic recovery and discontinuous dynamic recrystallization(DDRX)due to lower temperature rise and strain.Towards the particle or substrate interior,concurrent twinning and dislocation-mediated mechanisms refine the structure,forming straight,curved,and intersected twins.At the top of the particles,only deformed grains with a low dislocation density are observed.Our results showed that DRX induces microstructure softening in highly strained interface areas,facilitating atomic bonding in CoCrFeMnNi.HR-TEM investigation confirms the formation of atomic bonds between particles and substrate,with a gradual change in crystal lattice orientation from the particle to the substrate and the occurrence of some misfit dislocations and vacancies at the interface.Finally,the findings of this research suggest that softening and ASI,even in materials resistant to softening,are required to establish bonding in CS.展开更多
To obtain the Ti_(p)with different aspect ratios,the Ti_(p)/Mg-5Zn-0.3Ca composite prepared by semi-solid stir casting was subjected to extrusion at 220℃,180℃,and 140℃,respectively.Then,the effect of the Ti_(p)’s ...To obtain the Ti_(p)with different aspect ratios,the Ti_(p)/Mg-5Zn-0.3Ca composite prepared by semi-solid stir casting was subjected to extrusion at 220℃,180℃,and 140℃,respectively.Then,the effect of the Ti_(p)’s aspect ratio on the microstructure,mechanical properties,work hardening and softening behaviors of Ti_(p)/Mg-5Zn-0.3Ca composites was investigated.The results indicated that the Ti_(p)could be elongated obviously after low-temperature extrusion,and the aspect ratio of which would reach to 13.7:1 as the extrusion temperature deceased to 140℃.Then the“Ti/Mg”layer-like structure was formed in the Ti_(p)/Mg-5Zn-0.3Ca composite.Accompanied with the elongation of Ti_(p),the dynamic recrystallized grains and dynamic precipitates were both refined significantly,however,the dynamic recrystallization rate changed a little.The elongated Ti_(p)endowed the Ti_(p)/Mg-5Zn-0.3Ca composites with better matching of strength and toughness without the sacrifice of elongation and bending strain.Both the work hardening rate and softening rate of Ti_(p)/Mg-5Zn-0.3Ca composites increased with the increasing aspect ratio of Ti_(p).The formation of“Ti/Mg”layer-like structure contributed to the redistribution of strain from large aggregations to a network-like distribution,which effectively suppresses the initiation and propagation of micro-cracks,thus enhancing the plasticity of the Ti_(p)/Mg-5Zn-0.3Ca composites.展开更多
With the generation of both localised thermal and vibration in incremental sheet forming(ISF)by novel tool designs,rotational vibration assisted ISF(RV-ISF)can achieve significant force reduction and material softenin...With the generation of both localised thermal and vibration in incremental sheet forming(ISF)by novel tool designs,rotational vibration assisted ISF(RV-ISF)can achieve significant force reduction and material softening.However,the combined thermal and vibration softening in RV-ISF is unclear.By evaluating the similarities and differences of friction stir ISF(FS-ISF)and RV-ISF,this study develops a novel approach to decouple and quantify the thermal and vibration softening effects in RV-ISF of AZ31B-H24,providing new insights into underlying thermal and vibration softening mechanism.Experimental results reveal that in RV-ISF of AZ31B-H24 the thermal softening due to frictional heating dominates with 45∼65%of softening,while the vibration effect only contributes up to 15%of softening,from the conventional ISF,depending on the tool designs and tool rotational speed.The double-offset tool(T2)produces greater vibration softening than the three-groove tool(T3)owing to the higher vibration amplitude of the T2 tool.An increase in tool rotational speed primarily enhances thermal softening with only marginal changes to the vibration effect.Microstructural analysis suggests that with average grain size of 0.94μm at the top layer,RV-ISF with T3 and 3000 rpm is more effective for microstructure refinement than that by FS-ISF,especially on the tool-sheet contact surface,which confirms the occurrence of surface shearing.This refinement is a result of the reduced recrystallisation degree,71.8%at the top bottom layer.Compared with FS-ISF,RV-ISF can lead to not only higher geometrically necessary dislocation density,but also higher fraction of low-angle grain boundaries,indicating that softening mechanism due to localised vibration effect is resulted from the enhanced rearrangement and annihilation of dislocations.These findings contribute to new understanding of the thermal and vibration softening effects in RV-ISF of AZ31B-H24 and offer a theoretical foundation for the tool design and process optimisation.展开更多
In order to obtain a lower frequency band gap,this paper proposes a novel locally resonant meta-beam incorporating a softening nonlinear factor.An improved camroller structure is designed in this meta-beam to achieve ...In order to obtain a lower frequency band gap,this paper proposes a novel locally resonant meta-beam incorporating a softening nonlinear factor.An improved camroller structure is designed in this meta-beam to achieve the softening nonlinear stiffness of the local oscillators.Firstly,based on Hamilton's principle and the Galerkin method,the control equations for the coupled system are established.The theoretical band gap boundary is then derived with the modal analysis method.The theoretical results reveal that the band gap of the meta-beam shifts towards lower frequencies due to the presence of a softening nonlinear factor,distinguishing it from both linear metamaterials and those with hardening nonlinear characteristics.Then,the vibration attenuation characteristics of a finite size meta-beam are investigated through numerical calculation,and are verified by the theoretical results.Furthermore,parameter studies indicate that the reasonable design of the local oscillator parameters based on lightweight principles helps to achieve further broadband and efficient vibration reduction in the low-frequency region.Finally,a prototype of the meta-beam is fabricated and assembled,and the formations of the low-frequency band gap and the amplitude-induced band gap phenomenon are verified through experiments.展开更多
Rubbery waste at the end of the cycle often constitutes a threat for the environment because of their encumbrance and low biodeterioration.The purpose of the research presented is to develop the rubber fine powder as ...Rubbery waste at the end of the cycle often constitutes a threat for the environment because of their encumbrance and low biodeterioration.The purpose of the research presented is to develop the rubber fine powder as a pavement.It is interested primarily in the behavior of two types of bitumen 40/50 modified by the addition of two varieties of rubber fine powders of different grading,resulting from the crushing of the rubbery products intended for the clothes industry of soles of shoes.The objective of the experimentation is to study the influence of the added polymer on the physical properties of the ordinary road bitumen with the incorporation of the fine powder.The experimental approach is carried out using the two tests of characterization of the bitumen i.e.the softening point test and the penetration test which remain the most used to define and classify the road bitumen.It will be noted however,that the experimental investigation which is based on several tests according to the type and the content of fine powders,leads on a whole of interesting correlations.展开更多
In clinical dermatology,approximately 15%of patients suffer from nail disorders.Different nail diseases may present with similar clinical manifestations.When clinical diagnosis based on symptoms,dermoscopy,and fungal ...In clinical dermatology,approximately 15%of patients suffer from nail disorders.Different nail diseases may present with similar clinical manifestations.When clinical diagnosis based on symptoms,dermoscopy,and fungal tests is inconclusive,nail biopsy becomes the most critical diagnostic tool.Nail specimens are highly rigid,brittle,and adhere poorly to slide glass,making sectioning challenging and posing significant difficulties for pathology technicians.Limited literature exists on nail histology processing techniques.This paper reviews and consolidates the available literature on nail paraffin sectioning techniques,aiming to provide insights and methods for pathology technicians.展开更多
基金Project (9140C850205120C8501) supported by the Major Program of National Key Laboratory of Remanufacturing and the Army Foundation Project of China
文摘A required finite element method（FEM） model applicable for narrow gap CMT and CMT＋P MIX welding was established based on the interactions between arc,base metal and filler metal.A novel method of simplifying wire feeding pulses and heat input pulses was supposed under the conduction of equivalent input.The method together with composed double-ellipse heat sources was included in the model.The model was employed in the investigation of thermal cycling and the identification of the softened zone of AA7A52 base plates.Low-frequency behavior emerged in the form of low-cooling rate sects,which were not expected under experimental conditions.The softened zone including the quenched zone and averaging zone of the base plate was much wider internal the base plate than that close to the surfaces.The reliability of the predictions in thermal cycling was supported by infrared imaging test results of the thermal cycle process.
文摘Using the Gleeble 3500 thermal-mechanical system to simulate thermal cycles with different peak temperatures, the hardness and microstructure in the heat-affected zones of two kinds of 100 kg class hot-rolled extra-high-strength steel were compared. When the peak temperature of the thermal cycle was 800℃ ,incomplete transformation occurred during quenching in both steels, and massive martensite and bainite grains were formed. The hardness was determined by the composition and distribution of the microstructure. The concentration of massive martensite was low, and hence the hardness was low,in steel #1. Conversely,the massive martensite content in steel #2 was high and uniformly distributed,resulting in a high hardness. These findings can provide a reference for improving the mechanical properties in the softened zone.
文摘Mouthguard thickness is affected by the softened state of the sheet during thermoforming. The aim of this study is to establish an effective method for controlling the softened state of the sheet to prevent the mouthguard thickness from decreasing during mouthguard fabrication using a vacuum-forming machine. Mouthguards were thermoformed using an ethylene-vinyl acetate sheet (thickness: 4.0 mm) and a vacuum-forming machine. The working model was trimmed to the anterior height of 25 mm and the posterior height of 20 mm. The following two heating methods were compared: 1) the sheet was formed when it sagged 15 mm below the level of the sheet frame at the top of the post (condition T);and 2) the sheet frame was lowered to and heated at 50 mm below its usual height and the sheet was formed when it sagged 15 mm below the level of the sheet frame (condition L). For each heating method, the vacuum was applied immediately (T0, L0) or 5 s (T5, L5) after the sheet frame was lowered to the forming unit. The sheet surface temperature immediately before the vacuum was applied under each condition was measured. The differences in mouthguard thickness due to forming conditions were analyzed by one-way ANOVA and Bonferroni’s multiple comparison tests. The temperature difference between the center and the posterior depending on the condition decreased in the order T0 > T5 > L0 > L5, and that was 20<span style="white-space:nowrap;">°</span>C or higher for T0 and T5, and 10<span style="white-space:nowrap;">°</span>C or less for L0 and L5. At the incisal edge and the cusp, L0 and L5 were significantly thicker than T0. No significant differences were observed between conditions L0 and L5 at any measurement points. For the labial and buccal surfaces, significant differences in thicknesses among all conditions, except L0 and L5, were observed and were in the order T0 < T5 < L0 and L5. This study was suggested that the lowering the sheet frame and heating was more effective than adjusting the vacuum timing for uniform softening of the sheet.
基金Project supported by the National Natural Science Foundation of China(Nos.12172149,12172151,and 12202378)the MOE Key Laboratory of Fututer Intelligent Manufacturing Technologies for High-End Equipment of China(No.FIMFYUST-2025B07)+1 种基金the Guangzhou Municipal Bureau of Science and Technology of China(No.SL2023A04J01461)the Ministry of Science and Technology of China(No.G20221990122)。
文摘This study focuses on a new and high-efficiency approach in a unified sense of accurately simulating strength-degrading effects for geomaterials,including non-symmetric hardening-to-softening effects in tension and compression as well as non-symmetric tensile and compressive stiffness-degrading effects during unloading.It is intended to bypass both modeling and numerical complexities involved in existing approaches.To this goal,new elastoplastic equations are established with new numerical techniques.With a decoupling technique of treating tension-compression asymmetry,the foregoing complex effects are automatically incorporated as inherent response features of the new elastoplastic equations,thus bypassing usual modeling complexities.A new numerical technique of renormalizing piecewise spline functions is introduced to resolve the central yet tough issue of obtaining accurate and unified expressions for the tensile and compressive strength functions,thus bypassing usual numerical complexities and uncertainties in treating numerous unknown parameters and multiple ad hoc criteria.As such,the new approach is not only of wide applicability for various geomaterials but also of high computational efficiency with no more than three adjustable parameters.Toward validating the efficacy of the new approach,numerical examples for granite,salt rock,and sandstone-concrete combined body as well as plain concrete,high-performance concrete,and ultrahigh-performance concrete are presented by comparing model predictions with multiple data sets for strength-degrading effects in tension and compression.
基金supported by the Lendület/Momentum Programme of the Hungarian Academy of Sciencesthe National Research, Development, and Innovation Office, Hungary (Grant Nos. LP2024/21 and K146791)+2 种基金Bayers fellowship program MEDHA and Department of Botany, University of Calicutthe financial assistance provided in the form of Junior Research Fellowship from the University Grants Commission (UGC), Indiathe financial assistance provided by the Council for Scientific and Industrial Research(CSIR), India
文摘Ascorbate(Asc),commonly known as vitamin C,is a vital molecule for plant growth,development,and stress resilience.It is also known to play a crucial role in various physiological processes,including photosynthesis,cell division,and differentiation.This article thoroughly explores the processes governing the metabolism of Asc in plants and its roles in physiological functions.It lays down a robust theoretical groundwork for delving into Asc production,transportation,functions,and its potential applications in stress alleviation and horticulture.Furthermore,recent studies indicate that Asc plays a role in regulating fruit development and affecting postharvest storage characteristics,thereby influencing fruit ripening and resilience to stress.Hence,there is a growing importance in studying the synthesis and utilization of Asc in plants.Although the critical role of Asc in controlling plant redox signals has been extensively studied,the precise mechanisms by which it manages cellular redox homeostasis to maintain the equilibrium between reactive oxygen scavenging and cell redox signaling remain elusive.This gap in knowledge presents fresh opportunities to explore how the production of Asc in plants is regulated and how plants react to environmental stressors.Furthermore,this article delves into the potential for a comprehensive investigation into the essential function of Asc in fruits,the development of Asc-rich fruits,and the enhancement of postharvest storage properties.
基金supported by grants from the China Postdoctoral Science Foundation(2023M742867)the High-level Innovation and Entrepreneurship Talents Program of QinChuangYuan,Shaanxi Province,China(QCYRCXM-2022-234)the National Key R&D Program of China(2019YFD1000203)。
文摘Softening of fleshy fruits during ripening and postharvest is a programmed physiological process that substantially impacts fruit quality and shelf life.However,the molecular mechanism underlying peach softening remains largely unknown.Lateral organ boundary(LOB)domain(LBD)proteins are pivotal regulators of plant growth and development.To date,certain LOB/LBD transcription factors are seemingly implicated in fruit softening.In this study,we identified 42 LOB/LBD genes in the peach genome.Expression analysis showed a significant upregulation of PpLOB1 transcripts toward peach fruit ripening.PpLOB1 was classified into Class II subgroup,and showed high sequence similarity to several softening-related LOB/LBD transcription factors.Transient transformation assays showed that PpLOB1 positively modulates peach softening.Further experiments demonstrated that PpLOB1 directly targets and activates the promoters of pectate lyase 1(PpPL1)and PpPL15,thereby contributing to the regulation of fruit softening.Additionally,PpNAP4 up-regulates PpLOB1 expression by binding to its promoter.Meanwhile,our findings revealed that PpNAP4 and PpNAP6 cooperatively modulate the expression of Pp LOB1.Taken together,our findings revealed a novel regulatory module involving PpNAP4 and PpLOB1 that modulates peach fruit softening.
基金supported by the National Natural Science Foundation of China through grant numbers 12002245 and 12172263the Science and Technology Research Program of Chongqing Municipal Education Commission through grant number KJQN202300742+1 种基金the National Natural Science Foundation of ChongqingMunicipality through grant number CSTB2025NSCQ-GPX0841Chongqing Jiaotong University through grant number F1220038.
文摘Granular materials exhibit complex macroscopic mechanical behaviors closely related to their microscalemicrostructural features.Traditional macroscopic phenomenological elasto-plastic models,however,usually have complex formulations and lack explicit relations to these microstructural features.To avoid these limitations,this study proposes a micromechanics-based softening hyperelastic model for granular materials,integrating softening hyperelasticity withmicrostructural insights to capture strain softening,critical state,and strain localization behaviors.The model has two key advantages:(1)a clear conceptualization,straightforward formulation,and ease of numerical implementation(via Abaqus UMAT subroutine in this study);(2)explicit incorporation of micro-scale features(e.g.,contact stiffness,particle size,porosity)to reveal their influences on macroscopic responses.An isotropic directional distribution density of contacts and three specific microstructures are considered,and their softening hyperelastic constitutive modulus tensors are explicitly derived.By introducing a softening factor and critical failure energy density,the model can describe geomaterial behaviors,simulating residual strength,X-shaped shear bands,and strain localization evolution.Numerical validations in comparison with themacro-scale hyperelastic model,Abaqus Drucker-Prager model,and the experiment confirm its accuracy.Parametric studies reveal critical dependencies:a normal to tangential contact stiffness ratio of 2-8(depending on stiffness magnitude),an internal length of 2-4 mm to ensure shear band formation,and a critical failure energy density(≤10 kJ/m^(3))to trigger strain softening and localization.Influences of the specific microstructures on strain localization and softening are investigated.The model also shows mesh independence due to the introduction of an internal length.The model’s applicability is further demonstrated by slope stability analysis,capturing slip surface evolution,and load-displacement characteristics.This study develops a robust microstructure-aware hyperelastic framework to describe the mechanical behaviors of granular materials,providing multiscale insights for geotechnical engineering applications.
基金funded by the National Natural Science Foundation of China(Grant No.52471032).
文摘In this study,a 1400 MPa-grade ultra-high-strength steel thin-plate butt-welded joint was selected as the research object,and the joint was fabricated using the metal inert gas(MIG)welding process with ER307Si filler wire.Residual stress distributions were measured via the hole-drilling method,while micro-hardness was assessed using a micro-hardness tester.Simultaneously,both transverse shrinkage and angular distortion of the welded joint were experimentally determined.According to the hardness distribution of the joint,a thermalmetallurgical-mechanical finite element model was developed based on SYSWELD software platform.This model incorporates solid-state phase transformations(SSPT)and softening effect in the HAZ,as well as strain hardening and annealing behaviors in the weld metal.The temperature field,residual stress distribution,and welding deformation of single-pass butt-welded joint were simulated by the developed computational method.The simulation results were validated against experimental measurements,confirming the accuracy and reliability of the proposed computational approach.Furthermore,based on the numerical results,the influence mechanisms of SSPT and material softening on residual stress and deformation were analyzed.The findings indicate that SSPT exhibits considerable influences on the magnitude and distribution of welding residual stress.It reduces the peak longitudinal residual stress from 1620 MPa to 1350 MPa and increases the peak transverse residual stress from 350 MPa to 402 MPa.The results also manifest that the softening effect further reduces the peak longitudinal residual stress by 300 MPa,while exhibits minor effect on transverse residual stress.However,the results show that neither the SSPT nor the softening effect presents obvious influence on welding deformation.
基金funded by the Open Research Fund Programof State Key Laboratory of Hydroscience and Engineering(Project No.sklhse-2023-D-04)the National Natural Science Foundation of China(Project No.51979144).
文摘Characterization of mechanical alterations of shale constituent phases is critical for an in-depth understanding of the underlying mechanisms of shale softening.In this study,a hydro-thermal reaction system is set up to mimic the interactions between shale and water-based fluids under the subsurface environment in shale formations.Using a coupled analysis of grid nanoindentation and in situ mineralogical identification,mechanical alterations of shale constituent mineral phases are revealed.Mechanical degradation of carbonate and clay phases is 10 times greater than quartz,pyrite and organic phases.The KCl additive greatly mitigates mechanical degradation of the clay phase.The high temperature and pressure results in a mechanical degradation of carbonate minerals as much as three times of that occurs at room temperature and atmospheric pressure.Multiscale mechanical models,which are established based on Mori-Tanaka(MT)and self-consistent(SC)schemes,predict more accurate elastic softening of shale composite than the microindentation experiments,due to the microcracks generated in the experiments.Based on the calculation of the multiscale mechanical model,under the subsurface environment of shale formations(e.g.80℃ and 8 MPa),the carbonate dissolution leads to a reduction in Young's modulus of shale composite by about 30%,while the degradation of clay minerals only causes a reduction by up to 9%.
基金support from the National Natural Science Foundation of China(Grant Nos.52104207 and 52374214)the Shandong Provincial Youth Innovation Team Development Program for Higher Education Institutions(Grant No.2023KJ305).
文摘In the field of rock engineering,the influence of water is a dynamic process that exhibits varying effects over time and across different locations.To further understand how water influences the mechanical properties and acoustic emission(AE)behavior of rocks,this study conducted uniaxial compression experiments on sandstones with varying degrees of wetting under both natural conditions and water-chemical environments.In addition,the study combined AE equipment with digital image correlation(DIC)to monitor the entire failure process.Using the sliding window algorithm,the variation in the variance of AE characteristic parameters during the process of sandstone loading to failure is analyzed from the perspective of critical slowing down.This analysis enables the effective identification of the early warning signal before failure.The experimental findings suggest that an increase in wetting height results in a gradual decrease in peak stress,accompanied by a concomitant increase in the percentage of shear cracks.The characteristic parameters,including energy,amplitude,and ringing count,all exhibit critical slowing phenomena.The waveform of AE characteristic parameters of the same sample is similar,and the mutation time of the precursor signal is roughly the same.All signals appear in the irreversible plastic deformation stage of microcrack initiation.The integration of critical slowing down theory and the b-value early warning method facilitates a more comprehensive evaluation of the stability of rock mass,thereby significantly enhancing the efficiency and safety of disaster prevention measures.
基金supported by the National Natural Science Foundation of China(Grant No.52174371)the National Key Research and Development Program of China(Grant No.2021YFB3501003)the Shaanxi Provincial Science and Technology Department Enterprise Joint Fund(Grant No.2021JLM-33).
文摘Single-pass and double-pass high-temperature deformation experiments were conducted on 40Cr10Si2Mo steel using a Gleeble-3500 thermal simulator.The static recrystallization(SRX)behavior and recrystallization mechanisms of 40Cr10Si2Mo steel were investigated under deformation temperatures of 900-1100℃,deformation strains of 10%,20%,and 30%,and inter-pass times of 1-120 s.A static recrystallization fraction model was developed.The results showed that the SRX volume fraction increased with higher deformation temperature,larger deformation amount,and longer inter-pass time,with the deformation temperature having the most significant effect on SRX.During the deformation process,different process parameters led to different internal deformation mechanisms of the material.Static recovery and continuous static recrystallization(CSRX)dominated deformation at lower temperatures through progressive lattice rotation.In comparison,at higher temperatures,the deformation mechanism was dominated by CSRX and discontinuous static recrystallization(DSRX).The nucleation mechanisms of the SRX process were grain boundary bulging nucleation and subgrain merging nucleation,with grain boundary bulging present under all conditions.Subgrain merging nucleation could provide an additional nucleation mode at lower deformation temperatures or lower deformation amounts.Based on the traditional Avarmi equation,a modified model coefficient was used to establish the SRX kinetic model for 40Cr10Si2Mo steel.The linear correlation coefficient R^(2) between the predicted and experimental static recrystallization volume fraction was 0.96702,indicating high prediction accuracy.
基金supported by the National Natural Science Foundation of China(21875210)the National Key Research and Development Program of China(2016YFC1102203)+3 种基金the Natural Key Research and Development Project of Zhejiang Province(2018C03015)Zhejiang Provincial Ten Thousand Talents Program(2018R52001)the Fundamental Research Funds for the Central Universities(2020FZZX003-01-03)the Higher Education Discipline Innovation Project(111 Project)(B16042)。
文摘It has long been hypothesized that an increase in the extracellular matrix(ECM)stiffness mechanoactivates malignant phenotypes of breast tumor cells by regulating an array of processes underlying cancer biology.Although the contribution of substrate stiffening to drive malignant phenotype traits and other biological functions of a tumor is increasingly understood,the functional role of substrate softening on breast cancer cellular responses has rarely been investigated.Herein,we employed matrix metalloproteinase(MMP)-sensitive film to perform assays to explore the consequences of lowering stiffness on the biological behaviors of breast cancer cell MDA-MB-231.We demonstrated that cells underwent dramatic changes in migration,cellular conjunction,and expression of malignance-associated proteins and genes when the substrate stiffness decreased.Based on RNA sequencing and analysis,we found that hub genes including TP53,CCND1,MYC,CTNNB1,and YAP were validated to play central parts in regulating stiffness-dependent cellular manner change.Moreover,through visualization of differentially expressed genes(DEGs),cells on dynamically softened substrate appeared less influenced by transfer to tissue culture polystyrene(TCPS).These results suggest substrates with decreasing stiffness could normalize breast tumor malignant phenotype and help cells store the mechanical memory of the consequential weaker malignance.
基金supported by the National Science and Technology Council of Taiwan(NSTC 111-2622-E-150-002).
文摘This study examined the feasibility of utilizing high-pressure processing(HPP)with enzymatic impregnation to soften vegetables.Freeze-thaw(FT)processing was used as a positive control to compare the hardness,physicochemical characteristics,and cell microstructure of vegetables.Carrot and broccoli samples were subjected to 200 MPa pressure for 15 min and then impregnated using a Viscozyme L enzyme solution.Compared with the hardness of fresh samples,the hardness of the carrot and broccoli samples that underwent HPP and enzymatic impregnation decreased by 84.6%and 95.5%,respectively,and the hardness of the carrot and broccoli samples that underwent FT processed decreased by 73.6%and 91.3%,respectively.In particular,HPP with enzymatic impregnation reduced the content of insoluble dietary fibers(18%),increased the content of soluble dietary fibers(3%),and considerably increased the concentration of carotene(1.9 times)and isothiocyanate(4.5 times)in carrots and broccoli,respectively.Scanning electron microscopy reveals that HPP physically damaged the intercellular compartments of the vegetables,thereby increasing the impregnation of enzymes.In addition,the level of HPP and the holding time increased,and the amount of vegetable residue and the degree of moisture retention substantially decreased,indicating a negative correlation between damage and hardness.Moreover,HPP pretreatment require a short processing time then FT,which promoted the penetration of enzymes and the internal microstructural biodegradation of vegetables,and it also helped these vegetables release more soluble nutrients.Overall,HPP can be used with enzymatic impregnation to obtain texture-modified vegetables for older consumers with mastication difficulties.
基金supported by the Natural Science Foundation of Heilongjiang Province(No.JQ2022E004).
文摘In this paper,the work hardening and softening behavior of AZ31 magnesium alloy sheets by hard plate accumulative roll bonding(HP-ARB)process in a specific temperature range was studied for the first time,and the cyclic stress relaxation test,EBSD,TEM and other characterization methods were used.When the rolling temperature is 350℃,the grain size of magnesium sheets is refined to 4.32(±0.36)μm on average,and it shows an excellent combination of strength and plasticity.The tensile strength reaches 307(±8.52)MPa and the elongation is 12.73(±0.84)%.At this time,the curve of work hardening rate decreases smoothly and the degree of hardening is the lowest,and the amplitude of stress drop △σ_(p) in work softening test is the smallest with the increase of cycle times,which shows that the well coordination between work hardening and softening behavior has been achieved.Research has found that the combined effect of grain boundary strengthening and fine grain strengthening enhances the yield and tensile strength of magnesium sheets after three passes HP-ARB process at 350℃.This is attributed to the high degree of dislocation slip opening in the pyramidal surfaceand<c+a>,which not only coordinates the c-axis strain of the entire grain,but also promotes the slip transfer of dislocations in the fine-grained region,significantly improving the elongation of the sheets.This study provides a new idea for the forming and manufacturing of high performance magnesium alloy sheets.
文摘Large interfacial strains in particles are crucial for promoting bonding in cold spraying(CS),initiated either by adiabatic shear instability(ASI)due to softening prevailing over strain hardening or by hydrostatic plasticity,which is claimed to promote bonding even without ASI.A thorough microstructural analysis is vital to fully understand the bonding mechanisms at play during microparticle impacts and throughout the CS process.In this study,the HEA CoCrFeMnNi,known for its relatively high strain hardening and resistance to softening,was selected to investigate the microstructure characteristics and bonding mech-anisms in CS.This study used characterization techniques covering a range of length scales,including electron channeling contrast imaging(ECCI),electron backscatter diffraction(EBSD),and high-resolution transmission microscopy(HR-TEM),to explore the microstructure characteristics of bonding and overall structure development of CoCrFeMnNi microparticles after impact in CS.HR-TEM lamellae were prepared using focused ion beam milling.Additionally,the effects of deformation field variables on microstructure development were determined through finite element modeling(FEM)of microparticle impacts.The ECCI,EBSD,and HR-TEM analyses revealed an interplay between dislocation-driven processes and twinning,leading to the development of four distinct deformation microstructures.Significant grain refinement occurs at the interface through continuous dynamic recrystallization(CDRX)due to high strain and temperature rise from adiabatic deformation,signs of softening,and ASI.Near the interface,a necklace-like structure of refined grains forms around grain boundaries,along with elongated grains,resulting from the coexistence of dynamic recovery and discontinuous dynamic recrystallization(DDRX)due to lower temperature rise and strain.Towards the particle or substrate interior,concurrent twinning and dislocation-mediated mechanisms refine the structure,forming straight,curved,and intersected twins.At the top of the particles,only deformed grains with a low dislocation density are observed.Our results showed that DRX induces microstructure softening in highly strained interface areas,facilitating atomic bonding in CoCrFeMnNi.HR-TEM investigation confirms the formation of atomic bonds between particles and substrate,with a gradual change in crystal lattice orientation from the particle to the substrate and the occurrence of some misfit dislocations and vacancies at the interface.Finally,the findings of this research suggest that softening and ASI,even in materials resistant to softening,are required to establish bonding in CS.
基金supported by the“National Natural Science Foundation of China”(Grants.52271109 and 52001223)Support from the“National Key Research and Development Program for Young Scientists”(Grant.2021YFB3703300)+1 种基金the Major Special Plan for Science and Technology in Shanxi Province(202201050201012)the Special Fund Project for Guiding Local Science and Technology Development by the Central Government(Grant.YDZJSX2021B019)。
文摘To obtain the Ti_(p)with different aspect ratios,the Ti_(p)/Mg-5Zn-0.3Ca composite prepared by semi-solid stir casting was subjected to extrusion at 220℃,180℃,and 140℃,respectively.Then,the effect of the Ti_(p)’s aspect ratio on the microstructure,mechanical properties,work hardening and softening behaviors of Ti_(p)/Mg-5Zn-0.3Ca composites was investigated.The results indicated that the Ti_(p)could be elongated obviously after low-temperature extrusion,and the aspect ratio of which would reach to 13.7:1 as the extrusion temperature deceased to 140℃.Then the“Ti/Mg”layer-like structure was formed in the Ti_(p)/Mg-5Zn-0.3Ca composite.Accompanied with the elongation of Ti_(p),the dynamic recrystallized grains and dynamic precipitates were both refined significantly,however,the dynamic recrystallization rate changed a little.The elongated Ti_(p)endowed the Ti_(p)/Mg-5Zn-0.3Ca composites with better matching of strength and toughness without the sacrifice of elongation and bending strain.Both the work hardening rate and softening rate of Ti_(p)/Mg-5Zn-0.3Ca composites increased with the increasing aspect ratio of Ti_(p).The formation of“Ti/Mg”layer-like structure contributed to the redistribution of strain from large aggregations to a network-like distribution,which effectively suppresses the initiation and propagation of micro-cracks,thus enhancing the plasticity of the Ti_(p)/Mg-5Zn-0.3Ca composites.
基金the financial support received from the UK Engineering and Physical Sciences Research Council(EPSRC)through project grants EP/W010089/1 and EP/T005254/1.
文摘With the generation of both localised thermal and vibration in incremental sheet forming(ISF)by novel tool designs,rotational vibration assisted ISF(RV-ISF)can achieve significant force reduction and material softening.However,the combined thermal and vibration softening in RV-ISF is unclear.By evaluating the similarities and differences of friction stir ISF(FS-ISF)and RV-ISF,this study develops a novel approach to decouple and quantify the thermal and vibration softening effects in RV-ISF of AZ31B-H24,providing new insights into underlying thermal and vibration softening mechanism.Experimental results reveal that in RV-ISF of AZ31B-H24 the thermal softening due to frictional heating dominates with 45∼65%of softening,while the vibration effect only contributes up to 15%of softening,from the conventional ISF,depending on the tool designs and tool rotational speed.The double-offset tool(T2)produces greater vibration softening than the three-groove tool(T3)owing to the higher vibration amplitude of the T2 tool.An increase in tool rotational speed primarily enhances thermal softening with only marginal changes to the vibration effect.Microstructural analysis suggests that with average grain size of 0.94μm at the top layer,RV-ISF with T3 and 3000 rpm is more effective for microstructure refinement than that by FS-ISF,especially on the tool-sheet contact surface,which confirms the occurrence of surface shearing.This refinement is a result of the reduced recrystallisation degree,71.8%at the top bottom layer.Compared with FS-ISF,RV-ISF can lead to not only higher geometrically necessary dislocation density,but also higher fraction of low-angle grain boundaries,indicating that softening mechanism due to localised vibration effect is resulted from the enhanced rearrangement and annihilation of dislocations.These findings contribute to new understanding of the thermal and vibration softening effects in RV-ISF of AZ31B-H24 and offer a theoretical foundation for the tool design and process optimisation.
基金supported by the National Natural Science Foundation of China(Nos.12172014,U224126412332001)。
文摘In order to obtain a lower frequency band gap,this paper proposes a novel locally resonant meta-beam incorporating a softening nonlinear factor.An improved camroller structure is designed in this meta-beam to achieve the softening nonlinear stiffness of the local oscillators.Firstly,based on Hamilton's principle and the Galerkin method,the control equations for the coupled system are established.The theoretical band gap boundary is then derived with the modal analysis method.The theoretical results reveal that the band gap of the meta-beam shifts towards lower frequencies due to the presence of a softening nonlinear factor,distinguishing it from both linear metamaterials and those with hardening nonlinear characteristics.Then,the vibration attenuation characteristics of a finite size meta-beam are investigated through numerical calculation,and are verified by the theoretical results.Furthermore,parameter studies indicate that the reasonable design of the local oscillator parameters based on lightweight principles helps to achieve further broadband and efficient vibration reduction in the low-frequency region.Finally,a prototype of the meta-beam is fabricated and assembled,and the formations of the low-frequency band gap and the amplitude-induced band gap phenomenon are verified through experiments.
文摘Rubbery waste at the end of the cycle often constitutes a threat for the environment because of their encumbrance and low biodeterioration.The purpose of the research presented is to develop the rubber fine powder as a pavement.It is interested primarily in the behavior of two types of bitumen 40/50 modified by the addition of two varieties of rubber fine powders of different grading,resulting from the crushing of the rubbery products intended for the clothes industry of soles of shoes.The objective of the experimentation is to study the influence of the added polymer on the physical properties of the ordinary road bitumen with the incorporation of the fine powder.The experimental approach is carried out using the two tests of characterization of the bitumen i.e.the softening point test and the penetration test which remain the most used to define and classify the road bitumen.It will be noted however,that the experimental investigation which is based on several tests according to the type and the content of fine powders,leads on a whole of interesting correlations.
文摘In clinical dermatology,approximately 15%of patients suffer from nail disorders.Different nail diseases may present with similar clinical manifestations.When clinical diagnosis based on symptoms,dermoscopy,and fungal tests is inconclusive,nail biopsy becomes the most critical diagnostic tool.Nail specimens are highly rigid,brittle,and adhere poorly to slide glass,making sectioning challenging and posing significant difficulties for pathology technicians.Limited literature exists on nail histology processing techniques.This paper reviews and consolidates the available literature on nail paraffin sectioning techniques,aiming to provide insights and methods for pathology technicians.
