In this paper, based on the robust inverse scattering method, we construct two kinds of solutions to the focusing modified Korteweg–de Vries equation. One is the classical soliton solution under the zero background c...In this paper, based on the robust inverse scattering method, we construct two kinds of solutions to the focusing modified Korteweg–de Vries equation. One is the classical soliton solution under the zero background condition and the other one is given through the nonzero background.Especially, for the nonzero background case, we choose a special spectral parameter such that the nonzero background solution is changed into the rational travelling waves. Finally, we also give a simple analysis of the soliton as the time t is large, then we give the comparison between the exact solution and the asymptotic solution.展开更多
In-situ characterization of non-aqueous nano-dispersion systems（NANDS） by freeze-etching transmission electron microscope（FETEM） was reported.To improve just-for-once successive rate of specimen preparation and ge...In-situ characterization of non-aqueous nano-dispersion systems（NANDS） by freeze-etching transmission electron microscope（FETEM） was reported.To improve just-for-once successive rate of specimen preparation and get good characterization results,an improving specimen preparation method of freezing etching was developed.Size,distribution and morphology of NANDS were directly visualized.Some information of particle dispersion feature and particle density can also be obtained.Reproductivity of the FETEM characterization is excellent.Comparing with laser scattering method,which is liable to give positive error especially for small size particle anchoring disperser,FETEM characterization can give more accurate measurement of particle size.Moreover,FETEM can give dispersion feature of nanoparticle in non-aqueous medium.展开更多
The atmospheric scattering optical transfer function （OTF） is solved by applying the multi-coupled single scattering （MCSS） method to the three-dimensional radiative transfer equation （RTE） under the periodic gr...The atmospheric scattering optical transfer function （OTF） is solved by applying the multi-coupled single scattering （MCSS） method to the three-dimensional radiative transfer equation （RTE） under the periodic ground condition. This approach is a direct hit to the atmospheric scattering OTF using the same original context of modulation transfer function （MTF） measurement, i.e., images of sinusoidal grating at different spatial frequencies. Both the amplitude and phase shift of the OTF at various zenith and azimuth angles can be obtained at an arbitrary spatial frequency.展开更多
A Hauser-Ernst-type extended hyperbolic complex linear system given in our previous paper [Gao Y J 2004 Chin. Phys. 13 602] is slightly modified and used to develop a new inverse scattering method for the stationary a...A Hauser-Ernst-type extended hyperbolic complex linear system given in our previous paper [Gao Y J 2004 Chin. Phys. 13 602] is slightly modified and used to develop a new inverse scattering method for the stationary axisymmetric Einstein-Maxwell theory with multiple Abelian gauge fields. The reduction procedures in this inverse scattering method are found to be fairly simple, which makes the inverse scattering method be fine and effective in practical application. As an example, a concrete family of soliton solutions for the considered theory is obtained.展开更多
A new method of multi-coupled single scattering （MCSS） for solving a vector radiative transfer equation is de- veloped and made public on Internet. Recent solutions from Chandrasekhar＇s X-Y method is used to valida...A new method of multi-coupled single scattering （MCSS） for solving a vector radiative transfer equation is de- veloped and made public on Internet. Recent solutions from Chandrasekhar＇s X-Y method is used to validate the MCSS＇s result, which shows high precision. The MCSS method is theoretically simple and clear, so it can be easily and credibly extended to the simulation of aerosol/cloud atmosphere＇s radiative properties, which provides effective support for research into polarized remote sensing.展开更多
This study introduces a comprehensive theoretical framework for accurately calculating the electronic band-structure of strained long-wavelength InAs/GaSb type-Ⅱsuperlattices.Utilizing an eight-band k·p Hamilto⁃...This study introduces a comprehensive theoretical framework for accurately calculating the electronic band-structure of strained long-wavelength InAs/GaSb type-Ⅱsuperlattices.Utilizing an eight-band k·p Hamilto⁃nian in conjunction with a scattering matrix method,the model effectively incorporates quantum confinement,strain effects,and interface states.This robust and numerically stable approach achieves exceptional agreement with experimental data,offering a reliable tool for analyzing and engineering the band structure of complex multi⁃layer systems.展开更多
A semi-analytical/numerical model based on the multiple scattering （MS） method has been established for analyzing the effect of acoustic performance on main energy attenua- tion mechanism in viscoelastic coating con...A semi-analytical/numerical model based on the multiple scattering （MS） method has been established for analyzing the effect of acoustic performance on main energy attenua- tion mechanism in viscoelastic coating containing axisymmetric cavities. The basic functions of stress and displacement of the axisymmetric cavity surface are derived in the system of spheri- cal coordinates. The transition matrix between the incident wave and the scattering wave are obtained by the numerical integral of the basic functions of the cavity surface. The reflection, transmission and absorption performance of viscoelastic materials containing periodic cavities are calculated using the MS method and the wave propagating theory of the multi-layered medium. The results indicate that low frequency energy is mainly attenuated through cavity resonance. The resonant properties are found to be very sensitive to the boundary conditions. The coupling of the double-cavity is capable of extending the absorption to even lower fre- quencies. The absorption performance of the viscoelastic coating in the high frequency range is independent of the backing material. Its energy attenuation depends mainly on acoustic properties of cavity scattering and mode conversion.展开更多
Using the integral representation of the Jost solution,we deduce some conditions as the kernel functionN(x,y,t)if the Jost solution satisfies the two Lax equations.Then we verify the multi-soliton solution of NLS equa...Using the integral representation of the Jost solution,we deduce some conditions as the kernel functionN(x,y,t)if the Jost solution satisfies the two Lax equations.Then we verify the multi-soliton solution of NLS equationwith non-vanishing boundary conditions if we prove that these conditions can be demonstrated by the GLM equation,which determines the kernel function N(x,y,t)in according to the inverse scattering method.展开更多
The evolution of solitons in Bose-Einstein condensates （BECs） with time-dependent atomic scattering length in an expulsive parabolic potential is studied. Based on the extended hyperbolic function method, we success...The evolution of solitons in Bose-Einstein condensates （BECs） with time-dependent atomic scattering length in an expulsive parabolic potential is studied. Based on the extended hyperbolic function method, we successfully obtain the bright and dark soliton solutions. In addition, some new soliton solutions in this model are found. The results in this paper include some in the literature （Phys. Rev. Lett. 94（2005）050402 and Chin. Phys. Lett. 22（2005） 1855）.展开更多
An analytical technique, referred to as the scattering matrix method （SMM）, is developed to analyse the scattering of a planar wave from a conductolution for the nonuniform fering cylinder coated with nonuniform mag...An analytical technique, referred to as the scattering matrix method （SMM）, is developed to analyse the scattering of a planar wave from a conductolution for the nonuniform fering cylinder coated with nonuniform magnetized ferrite. The SMM srite coating can be reduced to the expressions for the scattering and penetrated coefficients in four particular cases： nonuniform magnetized ferrite cylinder, uniform magnetized ferrite-coated conducting cylinder, uniform ferrite cylinder as well as homogeneous dielectric-coated conducting cylinder. The resonant condition for the nonuniform ferrite coating is obtained. The distinctive differences in scattering between the nonuniform ferrite coating and the nonuniform dielectric coating are demonstrated. The effects of applied magnetic fields and wave frequencies on the scattering characteristics for two types of the linear profiles are revealed.展开更多
The multiple scattering cluster (MSC) method has been employed to perform a theoretical analysis on carbon is near edge X-ray absorption fine structure of the deuteron acetylene (C2 D2) adsorbed on Si(111)7× 7 at...The multiple scattering cluster (MSC) method has been employed to perform a theoretical analysis on carbon is near edge X-ray absorption fine structure of the deuteron acetylene (C2 D2) adsorbed on Si(111)7× 7 at room temperature. From the MSC study. it is confirmed that the (22D2 molecule is bonded to a pair of adjacent Si adatom and Si restatom with C-Si bond length about 0.18nm. The carbon-deuteron bond is bent away front the surface and the CCD bond angle is about 120°. The molecule plane tilt slightly away from the surface normal. Compared with C2D2 in gas phase, the C-C bond and C-D bond are elongated by about 0.03nm and 0.02nm respectively when acetylene was adsorbed on the subtrate. Keyowrds: adsorption of deuteron acetylene on Si(111)7×7. near edge X- ray absorption fine structure. multiple scattering cluster method展开更多
The nested Bethe ansatz (BA) method is applied to find the eigenvalues and the eigenvectors of the transfer matrix for spin-ladder model with open boundary conditions. Based on the reflection equation, we find the gen...The nested Bethe ansatz (BA) method is applied to find the eigenvalues and the eigenvectors of the transfer matrix for spin-ladder model with open boundary conditions. Based on the reflection equation, we find the general diagonal solution, which determines the generalboundary interaction in the Hamiltonian. We introduce the spin-ladder model with open boundary conditions. By finding the solution K± of the reflection equation which determines the nontrivial boundary terms in the Hamiltonian, we diagonalize the transfer matrix of the spin-ladder model with open boundary conditions in the framework of nested BA.展开更多
The surface in R3 associated with the Tzitzeica equation ＆ considered. By curvature coordinate transformation and surface imbedding, the Gauss-Codazzi equation is presented. Resorting to the solutions of the Gauss-Co...The surface in R3 associated with the Tzitzeica equation ＆ considered. By curvature coordinate transformation and surface imbedding, the Gauss-Codazzi equation is presented. Resorting to the solutions of the Gauss-Codazzi equation, the solution of the Tzitzeica equation ＆ obtained under a restrictive condition.展开更多
In this note, it is shown that the revision of the Kaup-Newell＇s works on 1ST for DNLS equation is only available in the ease of solving the bright one-soliton solution to the equation. An example is taken to illustr...In this note, it is shown that the revision of the Kaup-Newell＇s works on 1ST for DNLS equation is only available in the ease of solving the bright one-soliton solution to the equation. An example is taken to illustrate our point of view.展开更多
Based on the multiple scattering method,this paper investigates a benchmark problem of the propagation of liquid surface waves over finite graphene (or honeycomb) structured arrays of cylinders.Comparing the graphene ...Based on the multiple scattering method,this paper investigates a benchmark problem of the propagation of liquid surface waves over finite graphene (or honeycomb) structured arrays of cylinders.Comparing the graphene structured array with the square structured and with triangle structured arrays,it finds that the finite graphene structure can produce more complete band gaps than the other finite structures,and the finite graphene structure has less localized ability than the other finite structures.展开更多
The flow field in a typical inward-turning inlet was visualized using the Planar Laser Scattering(PLS)method in a shock tunnel with a nominal Mach number of 6.The opaque inlet,which is truncated at a series of section...The flow field in a typical inward-turning inlet was visualized using the Planar Laser Scattering(PLS)method in a shock tunnel with a nominal Mach number of 6.The opaque inlet,which is truncated at a series of sections,and the following transparent isolator,are combined to enable the optical access at different streamwise locations.The sequential PLS images provide a tomography-like flow visualization,which confirm the existence of streamwise Counter-rotating Vortex Pairs(CVPs)in both external and internal flow field of the inlet.Generation mechanisms of these CVPs are unraveled with the help of a numerical simulation,among which the cowl notch plays an important role in the generation of surface trailing CVPs along the centerline of the cowl.Moreover,the cowl shock sweeps the internal boundary layer towards the body side,which ultimately accumulates low-momentum flow on the body side in forms of a large CVP propagating downstream through the isolator.The CVPs formed in the shape-transition are responsible for the nonuniform flow field of the inward-turning inlet.This study indicates that the V-shaped cowl notch affects the downstream flow significantly and,therefore,should be examined thoroughly in practical applications.展开更多
The microstructure and misorientation of ultrathin hot strip were analyzed by CSP technology using electron back scattered diffraction (EBSD) method and Autoforge finite element program. The experimental results showe...The microstructure and misorientation of ultrathin hot strip were analyzed by CSP technology using electron back scattered diffraction (EBSD) method and Autoforge finite element program. The experimental results showed that the finishing hot rolling microstructures were the mixture of recrystallized and deformed austenite. After phase transformation, ferrite grains embody substructures and dislocations, leading to the high strength and relatively low elongation rate of the ultrathin hot strip. The FEM simulation of strain mode and distribution in deformation area has been fulfilled. The simulation results are in good agreement with the theoretical analysis and experimental results.展开更多
The analysis of sucrose esters with long acyl chain by improved high performance liquid chromatographic method with evaporative light scattering detection （HPLC-ELSD） and electrospray ionization mass spectrum （ESI...The analysis of sucrose esters with long acyl chain by improved high performance liquid chromatographic method with evaporative light scattering detection （HPLC-ELSD） and electrospray ionization mass spectrum （ESI-MS） is investigated. The improved HPLC-ELSD method for the separation and quantitation of commercial and synthesized sucrose esters is described. Samples are analyzed by means of a reversed-phase （RP） HPLC using a Hypersil C8 column （250 mm× 4.6 mm, 5 μm particle size） with methanol-tetrahydrofuran （vo）ume ratio of 90 ： 10） and water under gradientcondition as the mobile phase, in which the flow rate is 1.0 ml·min^-1 and the column temperature is set at 40℃. This procedure provides a complete separation and determination ot monoester, diester, triester and higher esters with different acyl chain lengths in each fraction by a single run, in combination with the ESI-MS technology. With this method, it is possible to determine the approximate compositions of monoto polyesters in one analysis and quantitate pure positional isomers precisely using an external standard method. It is found that the method of ESI-MS coupling with HPLC system for the analysis of sucrose esters is straight forward, rapid and inexpensive, and can be readily applied in synthesis, purification and structure studies.展开更多
The rational design of the sample cell may improve the sensitivity of surface-enhanced Raman scattering （SERS） detection in a high degree. Finite difference time domain （FDTD） simulations of the configuration of A...The rational design of the sample cell may improve the sensitivity of surface-enhanced Raman scattering （SERS） detection in a high degree. Finite difference time domain （FDTD） simulations of the configuration of Ag film-Ag particles illuminated by plane wave and evanescent wave are performed to provide physical insight for design of the sample cell. Numerical solutions indicate that the sample cell can provide more ＂hot spots＂ and the massive field intensity enhancement occurs in these ＂hot spots＂. More information on the nanometer character of the sample can be got because of gradient-field Raman （GFR） of evanescent wave. OCIS codes： 290.5860, 240.0310, 240.6680, 999.9999 （surface-enhanced Raman scattering）.展开更多
基金supported by the Natural Science Foundation of Shandong Province(Grant No.ZR2019QD018)National Natural Science Foundation of China(Grant Nos.11975143,12105161,61602188)+1 种基金CAS Key Laboratory of Science and Technology on Operational Oceanography(Grant No.OOST2021-05)Scientific Research Foundation of Shandong University of Science and Technology for Recruited Talents(Grant Nos.2017RCJJ068,2017RCJJ069)。
文摘In this paper, based on the robust inverse scattering method, we construct two kinds of solutions to the focusing modified Korteweg–de Vries equation. One is the classical soliton solution under the zero background condition and the other one is given through the nonzero background.Especially, for the nonzero background case, we choose a special spectral parameter such that the nonzero background solution is changed into the rational travelling waves. Finally, we also give a simple analysis of the soliton as the time t is large, then we give the comparison between the exact solution and the asymptotic solution.
基金Funded by National Natural Science Foundation of China(No.50572121) Key Pre-research Foundation of Weapon and Equipment(No. 9140A27010206JB35)
文摘In-situ characterization of non-aqueous nano-dispersion systems（NANDS） by freeze-etching transmission electron microscope（FETEM） was reported.To improve just-for-once successive rate of specimen preparation and get good characterization results,an improving specimen preparation method of freezing etching was developed.Size,distribution and morphology of NANDS were directly visualized.Some information of particle dispersion feature and particle density can also be obtained.Reproductivity of the FETEM characterization is excellent.Comparing with laser scattering method,which is liable to give positive error especially for small size particle anchoring disperser,FETEM characterization can give more accurate measurement of particle size.Moreover,FETEM can give dispersion feature of nanoparticle in non-aqueous medium.
基金supported by the Main Direction Program of Knowledge Innovation of Chinese Academy of Sciences(Grant No.KGFZD-125-13-006)
文摘The atmospheric scattering optical transfer function （OTF） is solved by applying the multi-coupled single scattering （MCSS） method to the three-dimensional radiative transfer equation （RTE） under the periodic ground condition. This approach is a direct hit to the atmospheric scattering OTF using the same original context of modulation transfer function （MTF） measurement, i.e., images of sinusoidal grating at different spatial frequencies. Both the amplitude and phase shift of the OTF at various zenith and azimuth angles can be obtained at an arbitrary spatial frequency.
基金Project supported by the National Natural Science Foundation of China (Grant No 10475036)
文摘A Hauser-Ernst-type extended hyperbolic complex linear system given in our previous paper [Gao Y J 2004 Chin. Phys. 13 602] is slightly modified and used to develop a new inverse scattering method for the stationary axisymmetric Einstein-Maxwell theory with multiple Abelian gauge fields. The reduction procedures in this inverse scattering method are found to be fairly simple, which makes the inverse scattering method be fine and effective in practical application. As an example, a concrete family of soliton solutions for the considered theory is obtained.
基金Project supported by the Science Foundation of the Airborne Remote Sensing System,Large Research Infrastructure of the Chinese Academy of Sciences
文摘A new method of multi-coupled single scattering （MCSS） for solving a vector radiative transfer equation is de- veloped and made public on Internet. Recent solutions from Chandrasekhar＇s X-Y method is used to validate the MCSS＇s result, which shows high precision. The MCSS method is theoretically simple and clear, so it can be easily and credibly extended to the simulation of aerosol/cloud atmosphere＇s radiative properties, which provides effective support for research into polarized remote sensing.
文摘This study introduces a comprehensive theoretical framework for accurately calculating the electronic band-structure of strained long-wavelength InAs/GaSb type-Ⅱsuperlattices.Utilizing an eight-band k·p Hamilto⁃nian in conjunction with a scattering matrix method,the model effectively incorporates quantum confinement,strain effects,and interface states.This robust and numerically stable approach achieves exceptional agreement with experimental data,offering a reliable tool for analyzing and engineering the band structure of complex multi⁃layer systems.
基金supported by the National Nature Science Foundation of China(11104310)the 973 National key Basic Research Program of China(2013CB632900)the 863 National High Technology Program of China(2011AA11A103)
文摘A semi-analytical/numerical model based on the multiple scattering （MS） method has been established for analyzing the effect of acoustic performance on main energy attenua- tion mechanism in viscoelastic coating containing axisymmetric cavities. The basic functions of stress and displacement of the axisymmetric cavity surface are derived in the system of spheri- cal coordinates. The transition matrix between the incident wave and the scattering wave are obtained by the numerical integral of the basic functions of the cavity surface. The reflection, transmission and absorption performance of viscoelastic materials containing periodic cavities are calculated using the MS method and the wave propagating theory of the multi-layered medium. The results indicate that low frequency energy is mainly attenuated through cavity resonance. The resonant properties are found to be very sensitive to the boundary conditions. The coupling of the double-cavity is capable of extending the absorption to even lower fre- quencies. The absorption performance of the viscoelastic coating in the high frequency range is independent of the backing material. Its energy attenuation depends mainly on acoustic properties of cavity scattering and mode conversion.
基金the Huazhong University of Science and Technology under Grant No.0101011110National Natural Science Foundation of China under Grant No.10375041
文摘Using the integral representation of the Jost solution,we deduce some conditions as the kernel functionN(x,y,t)if the Jost solution satisfies the two Lax equations.Then we verify the multi-soliton solution of NLS equationwith non-vanishing boundary conditions if we prove that these conditions can be demonstrated by the GLM equation,which determines the kernel function N(x,y,t)in according to the inverse scattering method.
基金Project supported by the National Natural Science Foundation of China （Grant Nos 1057508 and 10302018）, the Natural Science Foundation of Zhejiang Province, China （Grant No Y605056）.
文摘The evolution of solitons in Bose-Einstein condensates （BECs） with time-dependent atomic scattering length in an expulsive parabolic potential is studied. Based on the extended hyperbolic function method, we successfully obtain the bright and dark soliton solutions. In addition, some new soliton solutions in this model are found. The results in this paper include some in the literature （Phys. Rev. Lett. 94（2005）050402 and Chin. Phys. Lett. 22（2005） 1855）.
文摘An analytical technique, referred to as the scattering matrix method （SMM）, is developed to analyse the scattering of a planar wave from a conductolution for the nonuniform fering cylinder coated with nonuniform magnetized ferrite. The SMM srite coating can be reduced to the expressions for the scattering and penetrated coefficients in four particular cases： nonuniform magnetized ferrite cylinder, uniform magnetized ferrite-coated conducting cylinder, uniform ferrite cylinder as well as homogeneous dielectric-coated conducting cylinder. The resonant condition for the nonuniform ferrite coating is obtained. The distinctive differences in scattering between the nonuniform ferrite coating and the nonuniform dielectric coating are demonstrated. The effects of applied magnetic fields and wave frequencies on the scattering characteristics for two types of the linear profiles are revealed.
基金The authors acknowledge the financial support of the National Natural Science Foun-dation of China (Grant No.19974036)
文摘The multiple scattering cluster (MSC) method has been employed to perform a theoretical analysis on carbon is near edge X-ray absorption fine structure of the deuteron acetylene (C2 D2) adsorbed on Si(111)7× 7 at room temperature. From the MSC study. it is confirmed that the (22D2 molecule is bonded to a pair of adjacent Si adatom and Si restatom with C-Si bond length about 0.18nm. The carbon-deuteron bond is bent away front the surface and the CCD bond angle is about 120°. The molecule plane tilt slightly away from the surface normal. Compared with C2D2 in gas phase, the C-C bond and C-D bond are elongated by about 0.03nm and 0.02nm respectively when acetylene was adsorbed on the subtrate. Keyowrds: adsorption of deuteron acetylene on Si(111)7×7. near edge X- ray absorption fine structure. multiple scattering cluster method
文摘The nested Bethe ansatz (BA) method is applied to find the eigenvalues and the eigenvectors of the transfer matrix for spin-ladder model with open boundary conditions. Based on the reflection equation, we find the general diagonal solution, which determines the generalboundary interaction in the Hamiltonian. We introduce the spin-ladder model with open boundary conditions. By finding the solution K± of the reflection equation which determines the nontrivial boundary terms in the Hamiltonian, we diagonalize the transfer matrix of the spin-ladder model with open boundary conditions in the framework of nested BA.
基金Supported by the National Natural Science Foundation of China under Grant No 10471132, and the Special Foundation for the Major State Basic Research Project ＇Nonlinear Science＇ in China.
文摘The surface in R3 associated with the Tzitzeica equation ＆ considered. By curvature coordinate transformation and surface imbedding, the Gauss-Codazzi equation is presented. Resorting to the solutions of the Gauss-Codazzi equation, the solution of the Tzitzeica equation ＆ obtained under a restrictive condition.
基金the Postdoctoral Fund of Huazhong University of Science and Technology under Grant No.0128011006
文摘In this note, it is shown that the revision of the Kaup-Newell＇s works on 1ST for DNLS equation is only available in the ease of solving the bright one-soliton solution to the equation. An example is taken to illustrate our point of view.
基金supported by the National Natural Science Foundation of China (10932010 and 11072220)the Young Foundation of Zhejiang Normal University (KJ20100001)
文摘Based on the multiple scattering method,this paper investigates a benchmark problem of the propagation of liquid surface waves over finite graphene (or honeycomb) structured arrays of cylinders.Comparing the graphene structured array with the square structured and with triangle structured arrays,it finds that the finite graphene structure can produce more complete band gaps than the other finite structures,and the finite graphene structure has less localized ability than the other finite structures.
基金supported by the National Natural Science Foundation of China(Nos.11772325,11872356 and 11621202)。
文摘The flow field in a typical inward-turning inlet was visualized using the Planar Laser Scattering(PLS)method in a shock tunnel with a nominal Mach number of 6.The opaque inlet,which is truncated at a series of sections,and the following transparent isolator,are combined to enable the optical access at different streamwise locations.The sequential PLS images provide a tomography-like flow visualization,which confirm the existence of streamwise Counter-rotating Vortex Pairs(CVPs)in both external and internal flow field of the inlet.Generation mechanisms of these CVPs are unraveled with the help of a numerical simulation,among which the cowl notch plays an important role in the generation of surface trailing CVPs along the centerline of the cowl.Moreover,the cowl shock sweeps the internal boundary layer towards the body side,which ultimately accumulates low-momentum flow on the body side in forms of a large CVP propagating downstream through the isolator.The CVPs formed in the shape-transition are responsible for the nonuniform flow field of the inward-turning inlet.This study indicates that the V-shaped cowl notch affects the downstream flow significantly and,therefore,should be examined thoroughly in practical applications.
基金This research is supported by the State Foundation for Key Projects, Fundamental Research on New Generation of Steels (No.G1998061500)
文摘The microstructure and misorientation of ultrathin hot strip were analyzed by CSP technology using electron back scattered diffraction (EBSD) method and Autoforge finite element program. The experimental results showed that the finishing hot rolling microstructures were the mixture of recrystallized and deformed austenite. After phase transformation, ferrite grains embody substructures and dislocations, leading to the high strength and relatively low elongation rate of the ultrathin hot strip. The FEM simulation of strain mode and distribution in deformation area has been fulfilled. The simulation results are in good agreement with the theoretical analysis and experimental results.
基金Supported by the National Natural Science Foundation of China （20906052）, the Science Foundation of Nantong City Municipality （K2007011, K2008023）, the Science Foundation of Nantong University （08R08） and the University Science Research Project of Jiangsu Province （09KJB530008）.
文摘The analysis of sucrose esters with long acyl chain by improved high performance liquid chromatographic method with evaporative light scattering detection （HPLC-ELSD） and electrospray ionization mass spectrum （ESI-MS） is investigated. The improved HPLC-ELSD method for the separation and quantitation of commercial and synthesized sucrose esters is described. Samples are analyzed by means of a reversed-phase （RP） HPLC using a Hypersil C8 column （250 mm× 4.6 mm, 5 μm particle size） with methanol-tetrahydrofuran （vo）ume ratio of 90 ： 10） and water under gradientcondition as the mobile phase, in which the flow rate is 1.0 ml·min^-1 and the column temperature is set at 40℃. This procedure provides a complete separation and determination ot monoester, diester, triester and higher esters with different acyl chain lengths in each fraction by a single run, in combination with the ESI-MS technology. With this method, it is possible to determine the approximate compositions of monoto polyesters in one analysis and quantitate pure positional isomers precisely using an external standard method. It is found that the method of ESI-MS coupling with HPLC system for the analysis of sucrose esters is straight forward, rapid and inexpensive, and can be readily applied in synthesis, purification and structure studies.
文摘The rational design of the sample cell may improve the sensitivity of surface-enhanced Raman scattering （SERS） detection in a high degree. Finite difference time domain （FDTD） simulations of the configuration of Ag film-Ag particles illuminated by plane wave and evanescent wave are performed to provide physical insight for design of the sample cell. Numerical solutions indicate that the sample cell can provide more ＂hot spots＂ and the massive field intensity enhancement occurs in these ＂hot spots＂. More information on the nanometer character of the sample can be got because of gradient-field Raman （GFR） of evanescent wave. OCIS codes： 290.5860, 240.0310, 240.6680, 999.9999 （surface-enhanced Raman scattering）.
