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Modern research on the Meridian tropism theory of traditional Chinese medicine processing with auxiliary materials–taking the theory of“Salt-processing enhancing drug into kidney meridian”as an example
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作者 Yu-Ting Zhang Meng-Ting Wang +7 位作者 Zhi-Tong Yang Zi-Lu Liu Xue Zhang De-Ling Wu Chuan-Shan Jin Shan-Shan Li Tu-Lin Lu Xiao-Li Wang 《Integrative Medicine Discovery》 2024年第33期1-19,共19页
The theory of“Salt-processing enhancing drug into kidney meridian”was firstly put forward by Chen Jiamu,a medical doctor of Xin’an,in“Enlightening Primer of Materia Medica”.This theory integrates the theory of th... The theory of“Salt-processing enhancing drug into kidney meridian”was firstly put forward by Chen Jiamu,a medical doctor of Xin’an,in“Enlightening Primer of Materia Medica”.This theory integrates the theory of the five elements of Chinese medicine that the five flavors enter into the five viscera,and forms the theory of the role of the auxiliary materials of Chinese medicine concoctions.This theory is an important guiding significance for the clinical use of raw and cooked Chinese medicine tablets.At present,there are more studies on the theory of“Salt-processing enhancing drug into kidney meridian”in the literature,mainly focusing on the chemical composition,efficacy changes and the concoction mechanism of salt products of traditional Chinese medicines before and after salt preparation.There are relatively few review papers on the theory of“Salt-processing enhancing drug into kidney meridian”from the perspectives of auxiliary salt and attribution of meridians.In this paper,through reviewing relevant ancient books and literature,and on the basis of the previous review articles,this paper centers on the auxiliary salt,and conducts in-depth excavation and elaboration in terms of its sources,types,and the historical evolution of the salt production method.From the perspective of categorization,focusing on the core theory of“Kidney stores essence,governing reproduction,bone and generating marrow,water and brain”,we summarize the changes in efficacy before and after the salt preparation of kidney tonic traditional Chinese medicines,the changes in external and internal constituents as well as the scientific connotation of the concocting mechanism behind the effect-constituent changes.The scientific connotation of the concoction theory of“Salt-processing enhancing drug into kidney meridian”was initially elucidated,providing a new reference model for the study of the theory of Chinese medicine concoction attribution. 展开更多
关键词 salt-processing enhancing drug into kidney meridian history of salt processed effect change compositional change salt-processing mechanism
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Cathodic reduction process of Al-Cu-Y alloy in fluoride-oxide eutectic system via molten salt electrolysis 被引量:6
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作者 Xu Wang Chunfa Liao +1 位作者 Yunfen Jiao Hao Tang 《Journal of Rare Earths》 SCIE EI CAS CSCD 2018年第3期324-330,共7页
Al-Cu-Y alloys were prepared by molten salt electrolysis in fluoride-oxide system composed of electrolyte(Na3 AlF6-AlF3-LiF-MgF2) and oxide(Al2 O3-CuO-Y2 O3). Cathodic reduction process of Al2 O3,CuO and Y2 O3 wer... Al-Cu-Y alloys were prepared by molten salt electrolysis in fluoride-oxide system composed of electrolyte(Na3 AlF6-AlF3-LiF-MgF2) and oxide(Al2 O3-CuO-Y2 O3). Cathodic reduction process of Al2 O3,CuO and Y2 O3 were analyzed by cyclic voltammetry and chronoamperometry. Components and phase composition of alloy samples prepared by potentiostatic electrolysis were characterized by scanning electron microscopy and energy dispersive spectroscopy. The results show that the Al-Cu-Y alloy can be prepared in the AIF3-NaF-5 wt%LiF-5 wt%MgF2(NaF/AlF3 = 2.2, molecular ratio) eutectic system with mixed oxide(Al2 O3-CuO-Y2 O3) through 2 h at the conditions of a temperature of 1208 K, cell voltage3.0 V, cathode current density 0.7 A/cm^2. Al(Ⅲ) and Cu(Ⅱ) ions can be reduced to zero valence Al(0) and Cu(0) directly on carbonaceous electrode surface by instantaneous nucleation, respectively, the reduction process is controlled by diffusion. The reduction potential of Y(Ⅲ) ions is close to the active ions of fluoride melts, but strengthened phase AI3 Y can be formed through electrochemical reduction and alloyed process with active Al(Ⅲ) and Cu(Ⅱ) ions, meanwhile, the Al2 Cu and Al3 Y phases are distributed at the grain boundary of Al matrix. 展开更多
关键词 Fluoride-oxide eutectic Al-Cu-Y alloy Molten salt electrolysis Cyclic voltammetry Electrode process Rare earths
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Mechanism of Salt Migration Driven by Tectonic Processes:Insights from Physical and Numerical Modeling 被引量:2
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作者 YIN Hongwei ZHENG Mianping +2 位作者 ZHANG Zhen WU Zhenyun WANG Xingyuan 《Acta Geologica Sinica(English Edition)》 SCIE CAS CSCD 2014年第S1期273-274,共2页
1 Introduction Physical and numerical models are constructed to investigate the evolution and mechanism of salt migration driven by tectonic processes.In recent years,we have designed and ran series of models to simul... 1 Introduction Physical and numerical models are constructed to investigate the evolution and mechanism of salt migration driven by tectonic processes.In recent years,we have designed and ran series of models to simulate salt 展开更多
关键词 In Mechanism of salt Migration Driven by Tectonic processes
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Salts as Indicators for the Interior Processes of Solid Planets
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作者 KONG Weigang ZHENG Mianping KONG Fanjing 《Acta Geologica Sinica(English Edition)》 SCIE CAS CSCD 2014年第S1期422-423,共2页
1 Introduction It has been noticed that salts link the Earth’s spheres(Zheng,2007),and rich information must have been recorded by salts on the geological processes they involved in.Salts have been found on Mars,Euro... 1 Introduction It has been noticed that salts link the Earth’s spheres(Zheng,2007),and rich information must have been recorded by salts on the geological processes they involved in.Salts have been found on Mars,Europa,Enceladus,and salts might be common on planets(Zheng et al.,2013).Thus salts can be potential indicators for studying the geological history of planets.From the beginning of the 21st century,much new 展开更多
关键词 salts as Indicators for the Interior processes of Solid Planets
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The Surface Morphologies and Spectroscopy Analysis of VC Coatings on the Substrate of Cr12MoV Prepared by TD Process after Salt Spray 被引量:2
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作者 孔德军 《Journal of Wuhan University of Technology(Materials Science)》 SCIE EI CAS 2012年第4期628-633,共6页
The normal temperature corrosion of VC coating on the substrate of Cr12MoV prepared by TD process was tested in 5% NaCl aqueous solution, its surface morphologies and corrosion components after salt spray were observe... The normal temperature corrosion of VC coating on the substrate of Cr12MoV prepared by TD process was tested in 5% NaCl aqueous solution, its surface morphologies and corrosion components after salt spray were observed with SEM and EDS, respectively, and the effects of salt spray on micro-structures of VC coating were analyzed. Moreover, the invalidation mechanism of VC coating after salt spray and its effect on substrate material were discussed. The experimental results shown that the uniformity and integrity of VC coating surface are destroyed by salt spray for 120 h, a large number of the pits are produced on the coating surface, and the coating falls off, which speeds corrosion breakage of its substrate; the oxidated film on its surface becomes rougher, broken and discontinuous, and falls off easily, which reduce the ability of resistance salt spray; the failure modes of VC coating after salt spray are expressed with falling off of oxidated film, stress concentration and pore effect and so on, the corrosion breakage of oxidated film is the corrosion result of deoxidization corrosion from oxygen and HCl produced by NaCl and vapor. 展开更多
关键词 salt spray surface morphology spectroscopy analysis VC coating TD process
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Application of Salt Whey from Egyptian Ras Cheese in Processed Cheese Making
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作者 Sameh Awad Nour Elhoda Ahmed Morsi El Soda 《Food and Nutrition Sciences》 2013年第9期79-86,共8页
The objective of this study was to evaluate characteristics of processed cheese made from salt Ras cheese whey and young Cheddar containing exopolysaccharide producing cultures (EPS) as compared with those in cheese m... The objective of this study was to evaluate characteristics of processed cheese made from salt Ras cheese whey and young Cheddar containing exopolysaccharide producing cultures (EPS) as compared with those in cheese made from EPS-negative cheeses. Processed cheeses were manufactured using young (1 day) or 1-month-old EPS-positive or EPSnegative Cheddar cheese and replacing the added water by Ras cheese whey or ultrafiltrated (UF) whey. Moisture and fat of processed cheese were standardized to 54% and 23%, respectively. Exopolysaccharide-positive processed cheese was softer, less chewy and gummy than the EPS-negative cheeses. The hardness and chewiness were lower in processed cheeses made from 1-month-old Cheddar than in the corresponding cheeses made from 1-day-old Cheddar cheese. Sensory scores for texture of EPS positive processed cheeses were higher than those of the EPS-negative cheeses. Generally, processed cheese made from replacing all added water with whey received higher scores in flavor and overall than did the corresponding cheeses made without whey. The obtained results are showing promise for application of salt whey in processed cheese making. 展开更多
关键词 processed CHEESE EXOPOLYSACCHARIDE Producing CULTURES salt WHEY UF WHEY
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盐制炮制对地黄凉血止血功效的增效作用探索
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作者 张月月 龙冰玉 +5 位作者 王君明 何庆文 巫晓慧 宋玲玲 纪丽婕 张天柱 《中华中医药学刊》 北大核心 2026年第1期77-81,共5页
目的探索盐制炮制对地黄凉血止血功效的增效作用。方法在制备盐制地黄炮制品基础上,参考文献方法以干姜水煎液15 g·kg^(-1)联合5%乙醇复制小鼠血热出血模型,通过对小鼠一般体征、肛温、饮水量、出血时间、血浆凝血酶时间(TT)、凝... 目的探索盐制炮制对地黄凉血止血功效的增效作用。方法在制备盐制地黄炮制品基础上,参考文献方法以干姜水煎液15 g·kg^(-1)联合5%乙醇复制小鼠血热出血模型,通过对小鼠一般体征、肛温、饮水量、出血时间、血浆凝血酶时间(TT)、凝血酶原时间(PT)、活化部分凝血活酶时间(APTT)、纤维蛋白原含量(FIB)以及对能够反映温度趋向性的热区停留比例等指标的检测分析,并通过对凉血止血功效的主成分分析和功效主成分分别与主要质控成分梓醇和地黄苷D的含量以及反映寒热药性的温度趋向性指标的灰色关联分析,综合评价盐制炮制对地黄凉血止血功效的增效作用。结果模型引起了小鼠在热区停留比例显著降低、饮水量增加以及肛温、出血时间、PT、APTT、TT、FIB、Na^(+)-K^(+)-ATP、Ca^(2+)-Mg^(2+)-ATP均显著延长或升高(P<0.05或P<0.01);地黄生品及其盐制品低、高剂量(3、6 g·kg^(-1))对上述模型引起的指标异常均具有改善作用,且高剂量的改善作用优于低剂量(P<0.05或P<0.01);地黄盐制品对上述指标的改善作用优于同剂量下的地黄生品(P<0.05或P<0.01)。主要质控成分梓醇和地黄苷D对凉血止血功效成分(PCA)-灰色关联(GCA)分析的灰色关联系数分别为0.818和0.676,以及对寒热药性指标的灰色关联系数分别为0.801和0.572。结论盐制炮制对地黄凉血止血功效具有增效作用,在一定程度上该炮制增效作用可能与盐制增强地黄的寒性药性、梓醇和地黄苷D含量有关,其中地黄苷D含量贡献最大。 展开更多
关键词 盐制地黄 凉血止血功效 炮制增效 寒性药性 主成分-灰色关联分析
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20 Years Advances in Preparation of Potassium Salts from Potassic Rocks:A Review 被引量:6
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作者 MA Hongwen YANG Jing +6 位作者 SU Shuangqing LIU Meitang ZHENG Hong WANG Yingbin QI Hongbin ZHANG Pan YAO Wengui 《Acta Geologica Sinica(English Edition)》 SCIE CAS CSCD 2015年第6期2058-2071,共14页
Long-term research on key techniques of clean utilization of potassic rocks from over twenty localities has been performed to settle the shortage of soluble potassium resources in China. The results show that K-feldsp... Long-term research on key techniques of clean utilization of potassic rocks from over twenty localities has been performed to settle the shortage of soluble potassium resources in China. The results show that K-feldspar as the principal mineral enriched in potassium could be decomposed in the media of Ca(OH)_2, NaOH, KOH-H_2O solution via hydrothermal treatment, into tobermorite, hydroxylcancrinite, and kalsilite respectively. By further processing, these compounds are feasible for being as slow-release carrier of potassium nitrate, extracting alumina, and preparing farm-oriented fertilizers of potassium sulphate and nitrate. Correspondingly, the filtrate is KOH,(Na, K)_2SiO_3, and K_2SiO_3 solution, from which potassium carbonate, sulphate, nitrate, and phosphate could be easily fabricated. As NaO H and KOH are recycled in the processing chains by causticizing sodium and/or potassium metasilicate solutions, the hydrothermal alkaline techniques as developed in this research have several advantages as lower consumption of disposable mineral resources and energy, maximized utilization of potassic mineral resources, as well as clean productions etc. Based on the approaches presented in this paper, the technical system of efficiently utilizing insoluble potassium resources has been established. The hydrothermal alkaline methods are feasible to be industrialized on a large scale, thus resulting in decreasing imports of potash fertilizers, improving the pattern of potassium fertilizer consumption, and enhancing the supplying guarantee of potassium resource in China. 展开更多
关键词 K-FELDSPAR potassium salt alkaline digestion green processing sustainable development
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G-protein β subunit AGB1 positively regulates salt stress tolerance in Arabidopsis 被引量:2
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作者 MA Ya-nan CHEN Ming +8 位作者 XU Dong-bei FANG Guang-ning WANG Er-hui GAO Shi-qing XU Zhao-shi LI Lian-cheng ZHANG Xiao-hong MIN Dong-hong MA You-zhi 《Journal of Integrative Agriculture》 SCIE CAS CSCD 2015年第2期314-325,共12页
The heterotrimeric GTP-binding proteins(G-proteins) in eukaryotes consisted of α, β and γ subunits and are important in molecular signaling by interacting with G-protein-coupled receptors(GPCR), on which to tra... The heterotrimeric GTP-binding proteins(G-proteins) in eukaryotes consisted of α, β and γ subunits and are important in molecular signaling by interacting with G-protein-coupled receptors(GPCR), on which to transduce signaling into the cytoplast through appropriate downstream effectors. However, downstream effectors regulated by the G-proteins in plants are currently not well defined. In this study, the transcripts of AGB1, a G protein β subunit gene in Arabidopsis were found to be down-regulated by cold and heat, but up-regulated by high salt stress treatment. AGB1 mutant(agb1-2) was more sensitive to high salt stress than wild-type(WT). Compared with WT, the cotyledon greening rates, fresh weight, root length, seedling germination rates and survival rates decreased more rapidly in agb1-2 along with increasing concentrations of Na Cl in normal(MS) medium. Physiological characteristic analysis showed that compared to WT, the contents of chlorophyll, relative proline accumulation and peroxidase(POD) were reduced, whereas the malonaldehyde(MDA) content and concentration ratio of Na+/K+ were increased in agb1-2 under salt stress condition. Further studies on the expression of several stress inducible genes associated with above physiological processes were investigated, and the results revealed that the expressions of genes related to proline biosynthesis, oxidative stress response, Na+ homeostasis, stress- and ABAresponses were lower in agb1-2 than in WT, suggesting that those genes are possible downstream genes of AGB1 and that their changed expression plays an important role in determining phenotypic and physiologic traits in agb1-2. Taken together, these findings indicate that AGB1 positively regulates salt tolerance in Arabidopsis through its modulation of genes transcription related to proline biosynthesis, oxidative stress, ion homeostasis, stress- and ABA-responses. 展开更多
关键词 ARABIDOPSIS heterotrimeric G-protein β subunit physiological processes salt stress tolerance
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Preparation and Magnetic Property of La_(0.7)Sr_(0.3)MnO_3 Nanorod by Combination Sol-Gel with Molten Salt 被引量:1
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作者 QI Shu-yan FENG Jing XU Xiao-dong WANG Jing-ping HOU Xiang-yu ZHANG Mi-lin 《Chemical Research in Chinese Universities》 SCIE CAS CSCD 2008年第6期672-674,共3页
La0.7Sr0.3MnO3(LSMO) nanorods were synthesized by a method combining sol-gel with molten salts at 950 ℃ for 10 h, which employed KCl+NaCl(mass ratio 4:1) as eutectic molten salts. The morphologies and magnetic ... La0.7Sr0.3MnO3(LSMO) nanorods were synthesized by a method combining sol-gel with molten salts at 950 ℃ for 10 h, which employed KCl+NaCl(mass ratio 4:1) as eutectic molten salts. The morphologies and magnetic properties of the resulting LSMO nanorods were investigated by X-ray diffraction(XRD), scanning electron microscopy(SEM), transmission electron microscopy(TEM), and vibrating sample magnetometer(VSM) measurements. It was found that the obtained perovskite manganite LSMO was a uniform nanorod with a diameter of about 50 nm and a length of longer than 500 rim. The Curie temperature(To) of the LSMO nanorod used here was 262 K, much lower than that of bulky single crystal LSMO(360 K). The low Curie temperature might be a result of the great disorder near the grain boundary, which could be observed clearly from the TEM picture. 展开更多
关键词 Molten salt synthesis Sol-gel processes PEROVSKITE Nanostructured materials
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Electrolysis of Magnesia from Bischofite in Qinghai Salt Lakes 被引量:1
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作者 Huimin Lu1, Lanlan Yu1, Pei Liang2, Yitian Liang2 1)Department of Nonferrous Metallurgy, University of Science and Technology Beijing, Beijing 100083, China 2) Laboratory of Nonferrous Metallurgy, Qinghai University. Xining 810016, China 《Rare Metals》 SCIE EI CAS CSCD 2001年第4期209-212,共4页
A new technique of magnesia electrolysis from bischofite in Qinghai salt lakes was investigated experimentally. Magnesia was prepared by ammonia processing. On an electrolysis cell of about 100 A capacity at 700degree... A new technique of magnesia electrolysis from bischofite in Qinghai salt lakes was investigated experimentally. Magnesia was prepared by ammonia processing. On an electrolysis cell of about 100 A capacity at 700degreesC, magnesium metal was obtained with a current efficiency of 90.23% and a specific energy consumption of 11.5 kW(.)h. The new technique has the advantages of energy saving, high current efficiency and environmental amity. 展开更多
关键词 BISCHOFITE ammonia processing MAGNESIA molten salt electrolysis
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Iodine Content of Processed Foods and Condiments Sampled in China, 2017-2019
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作者 Zhu Wang Jun Wang +5 位作者 Weisheng Xu Jing Xu Xiuwei Li Jia Zhao Guodong Wang Xiaoguang Yang 《Food and Nutrition Sciences》 2021年第12期1217-1231,共15页
<span style="font-family:;" "=""><strong>Introduction</strong><strong>:</strong></span><span style="font-family:;" "=""> Faci... <span style="font-family:;" "=""><strong>Introduction</strong><strong>:</strong></span><span style="font-family:;" "=""> Facing the challenge of increasing consumption of processed foods in China, along with the demand for salt reduction, and dynamic adjustment of universal salt iodization (USI) policy, it is necessary to timely evaluate the distribution of iodine content in processed foods and condiments, so as to provide more accurate data for population dietary iodine intake assessment. <b>Methods:</b> From markets in 6 cities and e-commerce platforms, cereal, tuber, le</span><span style="font-family:;" "="">gume, meat, fish, egg, and dairy products, and condiments, consumed by volunteers who attended in iodine intake investigation, and top selling products in particular with well-noted brands were preferentially sampled during 2017 t<span>o 2019. After being mixed and homogenized, each sample was detected by ICP-MS method. The range and medium of iodine content in each type of product were given. <b>Results:</b> After merging samples with close value in the same style of the same brand, and screening out samples with no added salt or low sodium content (≤120 mg/100g), total 725 data were sub-grouped and analyzed. In comparison with the 95<sup>th</sup> percentile of the iodine distribution in relative nature source, assessed by our previous study, nearly 77% of products made from grains, potatoes, beans, nuts, livestock and poultry meat were presumed to be processed with iodized salt. In somewhat, related with sodium value marked on food labeling, the median iodine ranged from 1.1 mg/100g to 149 mg/100g. The variation of iodine in egg, milk and fish made products, and seaweed or with seaweed products was greatly affected by the background of ingredients, the median content most floated between 12.8 mg/100g and 86.8 mg/100g, even up to 1800 mg/100g in seasoned seaweed. Based on the frequency of iodine digital and the ratio of iodine to sodium, it was speculated that nearly 90% of soy sauce and 73.5% of other seasonings like vinegar, sauce, paste, etc., were not added iodized salt, with overall median iodine 4.0 mg/100g an</span><span>d 12 mg/100g respectively. <b>Conclusion:</b> Using iodized salt in processed foo</span><span>ds is an approach of USI police. Affected by the nature backgrounds of ingredients composed, the amount of salt used, and the regulated fortification level, iodine content in each kind of product varied largely. It’s important to establish a monitoring system in processed foods, as well as fortification salt, to control the b</span>enefit and risk of iodine health.</span> 展开更多
关键词 Iodine Content Universal salt Iodization processed Food Edible salt DATABASE
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Hydrochemical Dynamic Characteristics and Evolution of Underground Brine in the Mahai Salt Lake of the Qaidam Basin Qinghai-Tibet Plateau 被引量:5
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作者 HU Shuya ZHAO Quansheng +2 位作者 WANG Guangcai ZHANG Jianwei FENG Juan 《Acta Geologica Sinica(English Edition)》 CAS CSCD 2018年第5期1981-1990,共10页
The mineral rock salts present in the Mahai Salt Lake of the Qaidam basin exhibit high solubilities in water. In addition, the multicomponent underground brine exhibits a high salinity and is easily precipitated. In t... The mineral rock salts present in the Mahai Salt Lake of the Qaidam basin exhibit high solubilities in water. In addition, the multicomponent underground brine exhibits a high salinity and is easily precipitated. In the natural state, brine transport in the brine layer is extremely slow, and the brine is in a relatively stable chemical equilibrium state with the rock salt media. However, during mining, both the seepage and the chemical fields fluctuate significantly, thereby disrupting the equilibrium and leading to variations in the chemical composition and dynamic characteristics of the brine. Therefore, we selected underground brine from the Mahai Salt Lake, collecting a total of 183 brine samples over three stages of mining(i.e., the early stage of underground brine extraction, the initial stage of mining, and the later stage of mining). Using a range of analytical techniques, the chemical dynamics of the underground brine water and its evolution were systematically studied. We found that evaporation and enrichment were the main mechanisms of underground brine evolution in the Mahai Salt Lake, with cation exchange and mineral dissolution/precipitation being key factors in determining the dynamic characteristics and evolution of the brine. 展开更多
关键词 Hydrochemical dynamics evolution exploitation process underground brine Mahai salt Lake Qinghai-Tibet Plateau
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Nano Si preparation by constant cell voltage electrolysis of FFC-Cambridge Process in molten CaCl_2 被引量:2
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作者 Ji Zhao Shengmei Lu +1 位作者 Linyan Hu Can Li 《Journal of Energy Chemistry》 SCIE EI CAS CSCD 2013年第6期819-825,共7页
Using FFC-Cambridge Process to prepare Si from SiO2 is a promising method to prepare nanostructured and highly pure silicon for solar cells.However,the method still has many problems unsolved and the controlling effec... Using FFC-Cambridge Process to prepare Si from SiO2 is a promising method to prepare nanostructured and highly pure silicon for solar cells.However,the method still has many problems unsolved and the controlling effect of the cell voltage on silicon product is not clear.Here we report in this article that nano cluster-like silicon product with purity of 99.95%has been prepared by complete conversion of raw material SiO2,quartz glass plate,using constant cell voltage electrolysis FFC-Cambridge Process.By analysis of XRD,EDS,TEM,HRTEM and ICP-AES as well as the discussion from the thermodynamics calculation,the morphology and components of the product based on the change of cell voltage are clarified.It is clear that pure silicon could be prepared at the cell voltage of 1.7 2.1 V in this reaction system.The silicon material have cluster-like structure which are made of silicon nanoparticles in 20 100 nm size.Interestingly,the cluster-like nano structure of the silicon can be tuned by the used cell voltage.The purity,yield and the energy cost of silicon product prepared at the optimized cell voltage are discussed.The purity of the silicon product could be further improved,hence this method is promising for the preparation of solar grade silicon in future. 展开更多
关键词 silicon nanostructures molten salt electrochemistry solar grade Si FFC-Cambridge process
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盐湖碳酸锂沉锂母液制备磷酸锂工艺研究 被引量:1
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作者 王怀有 余国云 +3 位作者 权朝明 张佳 唐发满 王敏 《材料导报》 北大核心 2025年第S1期115-122,共8页
随着近年来新能源技术的蓬勃发展,全球对锂产品的需求急剧增加。盐湖碳酸锂沉锂母液是重要的可高效回收锂资源之一。然而,现有的盐湖碳酸锂沉锂母液多闲置未利用。本工作针对碳酸锂沉锂母液中锂资源赋存特点,开发了碳酸锂沉锂母液制备... 随着近年来新能源技术的蓬勃发展,全球对锂产品的需求急剧增加。盐湖碳酸锂沉锂母液是重要的可高效回收锂资源之一。然而,现有的盐湖碳酸锂沉锂母液多闲置未利用。本工作针对碳酸锂沉锂母液中锂资源赋存特点,开发了碳酸锂沉锂母液制备磷酸锂的新工艺。首先采用Minitab19软件设计实验(DOE)方法预测了反应温度、搅拌速度、给料速度和磷盐过量系数等因素对锂收率的影响。残差“四合一”分析表明实验数据满足正态性、残差和为零以及残差随机波动的假设条件,在最优条件下,锂收率预测值(89.49%)与实验值(89.67%)的误差仅为0.2%,验证了预测的有效性和准确性,其中反应温度和磷盐过量系数是主要影响因素,但以磷酸钠为原料制备的磷酸锂纯度为88.57%。进一步对比研究了以磷酸、磷酸和磷酸钠及盐酸和磷酸钠复合磷源对锂收率和产品纯度的影响,结果表明,以磷酸为磷源可将产品纯度提高至97.65%,但锂收率降低至74.26%;以磷酸和磷酸钠为复合磷源时产品纯度为92.3%,锂收率为71.66%;以盐酸和磷酸钠为原料时产品纯度为98.07%,锂收率为80.31%。最后,引入聚乙二醇作为分散剂,改善了磷酸锂结晶过程中的团聚现象,进一步提高了产品纯度(99.78%),并显著降低了主要杂质离子含量,最终确定以盐酸+磷酸为原料的两步法制备电池级磷酸锂工艺为最优工艺。 展开更多
关键词 磷酸锂 结晶过程控制 盐湖碳酸锂沉锂母液 工艺优化
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超滤膜技术对盐湖卤水的预处理工艺 被引量:1
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作者 李燕 王敏 +1 位作者 杨红军 赵有璟 《水处理技术》 北大核心 2025年第9期60-66,共7页
利用超滤膜分离技术对盐湖卤水进行预处理,考察了不同操作参数及超滤预处理工艺对盐湖卤水中硅及有机污染物截留效果的影响。结果表明,盐湖卤水含盐量为20 g/L、进料温度为20℃时,Titan-NF膜的预处理效果较优;含盐量为100 g/L、进料温度... 利用超滤膜分离技术对盐湖卤水进行预处理,考察了不同操作参数及超滤预处理工艺对盐湖卤水中硅及有机污染物截留效果的影响。结果表明,盐湖卤水含盐量为20 g/L、进料温度为20℃时,Titan-NF膜的预处理效果较优;含盐量为100 g/L、进料温度为20℃、回收率为62%时,有利于BFUF300中空纤维超滤膜的预处理效果。Titan-NF膜和BFUF300中空纤维超滤膜对盐湖卤水的预处理效果均优于多介质过滤器和传统超滤膜的预处理方式,能够为盐湖卤水锂资源的绿色高效利用提供支持。 展开更多
关键词 超滤 盐湖卤水 预处理 过程控制
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DILECTRIC AND THERMAL PROPERTIES OF PEO DOPED WITH CADIMIUM CHLORIDE SALT
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作者 Jibril Al-Hawarin Ayman S.Ayesh Rami A.Abdel-Rahem 《Chinese Journal of Polymer Science》 SCIE CAS CSCD 2012年第2期143-151,共9页
The main aim of this research is to investigate the effect of salt concentration on the dielectric properties (AC (CrAC), permittivity (d), dielectric loss (d'), and dielectric relaxation process) and melting... The main aim of this research is to investigate the effect of salt concentration on the dielectric properties (AC (CrAC), permittivity (d), dielectric loss (d'), and dielectric relaxation process) and melting behavior of polyethylene oxide (PEO)/CdC12 complexes. The dielectric study was carried out over a frequency range 10-335 kHz and a temperature range 25--45~C. The AC conductivity, permittivity and dielectric loss of the PEO/CdC12 complexes increase with increasing salt concentration and temperature. Also, it was found that the addition of CdC12 salt to PEO host reduced the melting temperature of PEO host. Dielectric results reveal that the relaxation process of these complexes is due to viscoelastic relaxation or non-Debye relaxation at room temperature. Additionally, it was found that relaxation behavior remained viscoelastic at different temperatures and salt concentrations. 展开更多
关键词 Polyethylene oxide CdC12 salt Dielectric properties Dielectric relaxation Relaxation process Thermalproperties.
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Two-stage treatment process of pickling wastewater in the cold-rolling production of stainless steel 被引量:3
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作者 SHI Lei CHEN Ronghuan WANG Ruyi 《Baosteel Technical Research》 CAS 2010年第2期16-22,共7页
Based on the characteristics of pickling wastewater in the cold-rolling production of stainless steel, a new processing route, featuring source sludge reduction, wastewater two-stage treatment, heavy metal-contained s... Based on the characteristics of pickling wastewater in the cold-rolling production of stainless steel, a new processing route, featuring source sludge reduction, wastewater two-stage treatment, heavy metal-contained sludge and calcium salt sludge separating recovery, was proposed. As shown by the research results, after the two-stage process treatment, the effluent water can steadily reach the emission standards, the sludge yield can be decreased by more than 8% ; within the heavy metal-contained sludge, the recovery rates of Fc,Cr and Ni can either reach or surpass 95% ,and the total content ofF and S can drop to around 3%. Therefore,the sludge in the front part can be used as ferric dust. In the calcium salt sludge ,the recovery rate of F can either reach or surpass 85% ,and the total contents of Fe,Cr and Ni can fall below 0.5%. So the sludge in the rear part can be used as fluorgypsum or fluorite. Meanwhile,the results of the analysis on heavy metals leaching toxicity and morphologic distribution indicate that the two kinds of sectionalized sludge are not classified as hazardous wastes, which have a stable behavior and better utilization values compared with the former mixed- sludge. 展开更多
关键词 cold-rolled pickling wastewater two-stage process heavy metal-contained sludge calcium salt sludge
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响应面法优选盐制山茱萸炮制工艺
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作者 王璐 李玉星 +5 位作者 黄莉 龙群赓 朱茜茜 黄雍 肖望重 戴冰 《中南药学》 2025年第9期2502-2508,共7页
目的优选盐制山茱萸的炮制工艺。方法采用响应面法,以食盐浓度、食盐用量、闷润时间、蒸制时间为考察因素,并以盐制山茱萸中马钱苷、莫诺苷、獐芽菜苷、没食子酸及5-羟甲基糠醛(5-HMF)5个成分的含量为评价指标,采用层次分析(AHP)-熵权... 目的优选盐制山茱萸的炮制工艺。方法采用响应面法,以食盐浓度、食盐用量、闷润时间、蒸制时间为考察因素,并以盐制山茱萸中马钱苷、莫诺苷、獐芽菜苷、没食子酸及5-羟甲基糠醛(5-HMF)5个成分的含量为评价指标,采用层次分析(AHP)-熵权法组合赋权确定各评价指标的权重系数并计算综合评分,优选盐制山茱萸最佳炮制工艺。结果盐制山茱萸最佳炮制工艺为:食盐浓度13.8%,食盐用量2.2%,闷润时间185 min,蒸制时间368 min;其中蒸制时间、食盐用量对其炮制工艺有显著影响。结论优选出的盐制山茱萸最佳炮制工艺稳定可行,可为提升盐制品质量及临床疗效提供一定的试验依据。 展开更多
关键词 山茱萸 盐制 层次分析-熵权法 Box-Behnken响应面法 高效液相色谱法
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黄芪不同炮制品中氨基酸组成及营养价值评价
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作者 高伟城 王小平 +1 位作者 李鑫如 陈荣珠 《山西中医药大学学报》 2025年第8期848-854,共7页
目的:对盐炙、盐煮、盐炒、盐麸炒等盐制黄芪样品及蜜炙黄芪样品、黄芪生品中的氨基酸进行含量测定及营养价值分析,以期为盐制黄芪的质量标准完善及临床应用提供理论参考依据。方法:采用异硫氰酸苯酯柱前衍生高效液相色谱法(PITC-HPLC)... 目的:对盐炙、盐煮、盐炒、盐麸炒等盐制黄芪样品及蜜炙黄芪样品、黄芪生品中的氨基酸进行含量测定及营养价值分析,以期为盐制黄芪的质量标准完善及临床应用提供理论参考依据。方法:采用异硫氰酸苯酯柱前衍生高效液相色谱法(PITC-HPLC)测定黄芪不同炮制品中氨基酸的含量,以必需氨基酸(EAA)、药用氨基酸(MAA)及甜味氨基酸(SAA)在总氨基酸(TAA)中的百分含量为变量进行聚类分析,根据氨基酸比值系数法(RCAA)对黄芪不同炮制品进行营养价值分析。结果:不同炮制方法的盐制黄芪中天门冬氨酸、谷氨酸、丝氨酸、甘氨酸、组氨酸、精氨酸、苏氨酸、丙氨酸、脯氨酸、酪氨酸、缬氨酸、甲硫氨酸、胱氨酸、异亮氨酸、亮氨酸、苯丙氨酸、赖氨酸等17种氨基酸的含量范围分别为7.553~12.769 mg/g,4.948~7.500 mg/g,1.982~2.913 mg/g,2.083~3.107 mg/g,2.928~3.697 mg/g,4.261~6.181 mg/g,1.563~2.702 mg/g,2.024~2.904 mg/g,4.850~6.964 mg/g,2.258~3.665 mg/g,1.419~1.930 mg/g,3.338~4.692 mg/g,1.043~1.275 mg/g,2.273~3.309 mg/g,3.013~4.360 mg/g,2.598~3.401 mg/g及3.195~4.442 mg/g。黄芪不同炮制品聚类为生品黄芪、蜜炙黄芪及盐制黄芪3类。EAA百分含量(EAA/TAA)及EAA与非必需氨基酸比值(EAA/NEAA),生品黄芪为31.921%、46.889%,蜜炙黄芪为35.433%、54.897%,盐制黄芪为32.096~33.897%、47.268~51.279%。生品黄芪、蜜炙黄芪及盐制黄芪的氨基酸比值系数分值(SRC)分别为77.696、90.735、90.202~96.684。黄芪不同炮制品的EAA含量高于世界卫生组织(WHO)及联合国粮农组织(FAO)提出的成人需求值。结论:所建方法可用于盐制黄芪的氨基酸含量测定,盐煮法有利于黄芪氨基酸的提取,生品黄芪经盐制及蜜炙后,可提高其营养价值。 展开更多
关键词 盐制黄芪 蜜炙黄芪 氨基酸 柱前衍生 营养价值
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