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Safe flight corridor constrained sequential convex programming for efficient trajectory generation of fixed-wing UAVs 被引量:2
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作者 Jing SUN Guangtong XU +2 位作者 Zhu WANG Teng LONG Jingliang SUN 《Chinese Journal of Aeronautics》 2025年第1期537-550,共14页
Generating dynamically feasible trajectory for fixed-wing Unmanned Aerial Vehicles(UAVs)in dense obstacle environments remains computationally intractable.This paper proposes a Safe Flight Corridor constrained Sequent... Generating dynamically feasible trajectory for fixed-wing Unmanned Aerial Vehicles(UAVs)in dense obstacle environments remains computationally intractable.This paper proposes a Safe Flight Corridor constrained Sequential Convex Programming(SFC-SCP)to improve the computation efficiency and reliability of trajectory generation.SFC-SCP combines the front-end convex polyhedron SFC construction and back-end SCP-based trajectory optimization.A Sparse A^(*)Search(SAS)driven SFC construction method is designed to efficiently generate polyhedron SFC according to the geometric relation among obstacles and collision-free waypoints.Via transforming the nonconvex obstacle-avoidance constraints to linear inequality constraints,SFC can mitigate infeasibility of trajectory planning and reduce computation complexity.Then,SCP casts the nonlinear trajectory optimization subject to SFC into convex programming subproblems to decrease the problem complexity.In addition,a convex optimizer based on interior point method is customized,where the search direction is calculated via successive elimination to further improve efficiency.Simulation experiments on dense obstacle scenarios show that SFC-SCP can generate dynamically feasible safe trajectory rapidly.Comparative studies with state-of-the-art SCP-based methods demonstrate the efficiency and reliability merits of SFC-SCP.Besides,the customized convex optimizer outperforms off-the-shelf optimizers in terms of computation time. 展开更多
关键词 Fixed-wing unmanned aerial vehicle Efficient trajectory planning safe flight corridor Sequential convex programming Customized convex optimizer
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Influence mechanism and calculation of the minimum safe thickness of waterproof rock mass in karst tunnels 被引量:1
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作者 AN Pengtao LI Maoxiang +1 位作者 ZHANG Wenjun LIU Xiong 《Journal of Mountain Science》 2025年第2期695-709,共15页
Due to the influence of karst cave development and route selection,the location relationship between concealed karst cave and tunnel is more random.In order to explore the influence rule of karst cave location on the ... Due to the influence of karst cave development and route selection,the location relationship between concealed karst cave and tunnel is more random.In order to explore the influence rule of karst cave location on the minimum safe thickness of water-proof rock mass,a simplified calculation model of water-proof rock mass thickness when the karst cave is located at any location around the tunnel is established,and the influence of multiple factors on the overall stability of water-proof rock mass is considered.Based on the cusp catastrophe theory,the analytical expressions for the safety thickness of waterproof rock mass are derived.Based on the finite difference principle,the analytical expressions of the safety thickness of water-proof rock mass are verified.In order to improve the application range of the analytical formula derived in this paper,the analytical formula is optimized based on the instability principle differences between the simplified calculation model and the elastic compressive bar.The research results show that the necessary condition solution is more applicable and much safer than the sufficient condition solution.Tectonic stress,rock beam length and karst cave water pressure are significantly positively correlated with the safe thickness of the waterproof rock mass.The calculated results of the semioptimized formula and the unoptimized formula are constant values,independent of the karst cave location.While the calculated results of the fully optimized formula are variable values,correlated with the karst cave location,the thickness of the waterproof rock mass gradually decreases as the karst cave location moves from the top of the tunnel to the bottom of the tunnel.The unoptimized formula does not consider the influence of the lateral force of the rock beam,and is not suitable for the working condition with large lateral force,the calculation results of the semi-optimized formula and the fully optimized formula are not very different and are biased to safety,so it can be given priority. 展开更多
关键词 Tunnel engineering Water inrush disaster safe thickness Waterproof rock mass Concealed karst cave
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Acetabular Component Positioning and Risk of Dislocation in Hip Arthroplasty: Is Lewinnek’s Safe Zone Truly Safe?
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作者 Oliver Damiani Meyer Luis Henrique Zambra Wink +3 位作者 Walter Brandt Iserhard Carlos Roberto Schwartsmann Anthony Kerbes Yépez Leandro de Freitas Spinelli 《Open Journal of Orthopedics》 2025年第2期47-53,共7页
Objective: The present research aims to determine if adherence to the Lewinnek safe zone, when exclusively considered, constitutes a pivotal element for ensuring stability in the context of total hip arthroplasty. Thi... Objective: The present research aims to determine if adherence to the Lewinnek safe zone, when exclusively considered, constitutes a pivotal element for ensuring stability in the context of total hip arthroplasty. This is done by examining the acetabular placement in instances of hip dislocation after total hip arthroplasty (THA). Methodology: The authors searched 2653 patient records from 2015 to 2022 looking for patients who had total hip arthroplasty at our facility. For the analysis, 23 patients were culled from 64 individuals who exhibited post-THA dislocations, employing a stringent exclusion criterion, and the resultant acetabular angulation and anteversion were quantified utilizing PEEKMED software (Peek Health S.A., Portugal) upon radiographic evidence. Results: Within the operational timeframe, from the cohort of 2653 subjects, 64 presented with at least a singular incident of displacement. Post-exclusion criterion enforcement, 23 patients were eligible for inclusion. Of these, 10 patients conformed to the safe zone demarcated by Lewinnek for both inclination and anteversion angles, while 13 exhibited deviations from the prescribed anteversion and/or inclination benchmarks. Conclusion: Analysis of the 23 patients reveals that 13 did not confirm to be in the safe zone parameters for anteversion and/or inclination, whereas 10 were within the safe zone as per Lewinnek’s guidelines. This investigative review, corroborated by extant literature, suggests that the isolated consideration of the Lewinnek safe zone does not suffice as a solitary protective factor. It further posits that additional variables are equally critical as acetabular positioning and mandate individual assessment. 展开更多
关键词 Acetabular Component Positioning DISLOCATION Hip Arthroplasty Lewinnek’s safe Zone
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A Low-Collision and Efficient Grasping Method for Manipulator Based on Safe Reinforcement Learning
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作者 Qinglei Zhang Bai Hu +2 位作者 Jiyun Qin Jianguo Duan Ying Zhou 《Computers, Materials & Continua》 2025年第4期1257-1273,共17页
Grasping is one of the most fundamental operations in modern robotics applications.While deep rein-forcement learning(DRL)has demonstrated strong potential in robotics,there is too much emphasis on maximizing the cumu... Grasping is one of the most fundamental operations in modern robotics applications.While deep rein-forcement learning(DRL)has demonstrated strong potential in robotics,there is too much emphasis on maximizing the cumulative reward in executing tasks,and the potential safety risks are often ignored.In this paper,an optimization method based on safe reinforcement learning(Safe RL)is proposed to address the robotic grasping problem under safety constraints.Specifically,considering the obstacle avoidance constraints of the system,the grasping problem of the manipulator is modeled as a Constrained Markov Decision Process(CMDP).The Lagrange multiplier and a dynamic weighted mechanism are introduced into the Proximal Policy Optimization(PPO)framework,leading to the development of the dynamic weighted Lagrange PPO(DWL-PPO)algorithm.The behavior of violating safety constraints is punished while the policy is optimized in this proposed method.In addition,the orientation control of the end-effector is included in the reward function,and a compound reward function adapted to changes in pose is designed.Ultimately,the efficacy and advantages of the suggested method are proved by extensive training and testing in the Pybullet simulator.The results of grasping experiments reveal that the recommended approach provides superior safety and efficiency compared with other advanced RL methods and achieves a good trade-off between model learning and risk aversion. 展开更多
关键词 safe reinforcement learning(safe RL) manipulator grasping obstacle avoidance constraints lagrange multiplier dynamic weighted
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Urban flourish or peril:Navigating the safe and just space through the lens of ecosystem services in China’s urbanization
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作者 Qin Zhou Changgao Cheng +9 位作者 Zhou Fang Shi Xue Qiuya Zhao Zhongde Huang Jie Wang Wei Jin Chenjun Zhang Yang Bai Ni Geng Hengquan Zhang 《Geography and Sustainability》 2025年第5期152-164,共13页
Urbanization develops with the goal of establishing improved and more sustainable habitats for residents.Environmental and social performance must be simultaneously monitored to ascertain whether regions are progressi... Urbanization develops with the goal of establishing improved and more sustainable habitats for residents.Environmental and social performance must be simultaneously monitored to ascertain whether regions are progressing towards or deviating from the safe and just space(SJS)in urbanization.Despite relevant studies,the absence of indicators that bridge ecological preservation and human well-beings renders dual monitoring challenging.This study bridged the gap by exploring the interactions between urbanization,ecosystem services(ESs),and basic water,energy,and food(WEF)needs within the SJS framework across China and its provinces.By quantifying the minimum and actual demands for freshwater withdrawal,carbon emissions,phosphorus emissions,and land use,as well as the supply of ESs into unified biophysical indicators,we found that:(1)China can meet the basic WEF needs for all from 2000 to 2020,but only water and land provisioning ESs can operate within the SJS.Carbon emissions surpassed the sequestration capacity in 2010,while phosphorus purification ES has consistently been unsafe.(2)The SJS performance in terms of ecological and social fulfilment exhibited scale differences and undergone changes with urbanization.Overall,no province in China can consistently operate within all SJSs.(3)In the process of urbanization,improvements in ecological protection and production practices in most provinces expanded the size of SJS,but the continuous increase in total demand failed to steer regions toward safer spaces.Our framework emphasized the common but differentiated pathways that regions at varying stages of urbanization navigate to achieve safety and justice.It also provides an applicable solution for regions aiming to pursue urban growth while maintaining ecological conservation and social justice,ultimately achieving sustainable development. 展开更多
关键词 URBANIZATION safe andjust space Ecosystem services Water-energy-food Sustainability assessment
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Risk factors for safe injection practice performance among nurses in general hospitals
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作者 Hyeon Jin Jang Soonyoung Shon +1 位作者 Inah Kim Mi-So Shim 《Frontiers of Nursing》 2025年第4期537-546,共10页
Objective:Nurses must follow safe injection practices to prevent healthcare-associated infections(HAIs).This study aimed to identify the risk factors for safe injection practice among nurses in general hospitals.Metho... Objective:Nurses must follow safe injection practices to prevent healthcare-associated infections(HAIs).This study aimed to identify the risk factors for safe injection practice among nurses in general hospitals.Methods:This cross-sectional study included 215 nurses employed in Korean general hospitals.Data were collected from September 22 to October 9,2023.Multiple linear regression analysis was performed using SPSS Statistics 27.0.Results:The regression analysis revealed that a higher level of patient safety priority in the patient safety culture perception,increased knowledge of safe injection practices,and fewer working hours per week were associated with improved performance of safe injection practices among general hospital nurses.Conclusions:To enhance the performance of general hospital nurses in safe injection practice,it is necessary to establish a patient safety culture so that nurses recognize patient safety as a top priority.Additionally,an effective educational program is needed to increase the practical knowledge of safe injection practices,along with a supportive working environment that ensures appropriate working hours to prevent patient safety incidents. 展开更多
关键词 infection control NURSE patient safety safe injection practice work environment
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Comparative Study on the Safe-Haven Asset Characteristics of Bitcoin and Gold
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作者 GUO Zuoqi 《Journal of Modern Accounting and Auditing》 2025年第4期287-291,共5页
With the increasingly turbulent political situation and the outbreak of public health events without warning,it will not only affect people’s physical health,but also affect the global financial market,causing the ma... With the increasingly turbulent political situation and the outbreak of public health events without warning,it will not only affect people’s physical health,but also affect the global financial market,causing the market to fall into a huge crisis,thus leading to a continued decline in the worldwide economy.During periods of financial market turmoil,many investors fall into panic and urgently need a“haven”to protect their assets.With the rise of the digital economy,gold no longer seems to be the only safe-haven option.Bitcoin has gradually entered the investors’field of vision.Some investors believe that Bitcoin can become an emerging safe-haven asset that is as important as or surpasses gold.Based on an analysis of the safe-haven properties of Bitcoin and gold during major political and historical events and public health events,this article will clarify which of the two is more suitable as a reliable contemporary safe-haven asset and provide advice to investors. 展开更多
关键词 Bitcoin GOLD safe haven
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Application Value of Bundle Management in Safe Nursing Care for Patients with Autoimmune Encephalitis
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作者 Ying Cui 《Journal of Clinical and Nursing Research》 2025年第4期149-154,共6页
Objective:To explore the application effect of bundle management in the safe nursing of patients with autoimmune encephalitis.Methods:Seventy-five patients with autoimmune encephalitis who met the inclusion criteria i... Objective:To explore the application effect of bundle management in the safe nursing of patients with autoimmune encephalitis.Methods:Seventy-five patients with autoimmune encephalitis who met the inclusion criteria in our hospital from January 2024 to June 2024 were randomly divided into two groups:an observation group of 39 patients and a control group of 36 patients.The control group received routine nursing care,while the observation group implemented a bundle management strategy based on routine nursing care.Safety nursing outcomes,clinical symptom improvement time,hospital stay,and neurologic function recovery were observed in both groups.Results:The incidence of adverse events in the observation group was 12.82%,significantly lower than the 33.33%in the control group,with a statistically significant difference(P<0.05).There was no statistically significant difference in restraint usage and ICU transfer rates between the two groups(P>0.05).The clinical symptom improvement time,hospital stay,and neurologic function recovery in the observation group were significantly better than those in the control group,with a statistically significant difference(P<0.05).Conclusion:Through the bundle management model,effective connections can be ensured in various aspects of treatment and rehabilitation for patients with autoimmune encephalitis,providing patients with comprehensive and multi-level nursing services and improving their overall satisfaction and treatment effectiveness. 展开更多
关键词 Bundle management Autoimmune Encephalitis safe nursing Clinical effect
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An Active Safe Semi-Supervised Fuzzy Clustering with Pairwise Constraints Based on Cluster Boundary
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作者 Duong Tien Dung Ha Hai Nam +1 位作者 Nguyen Long Giang Luong Thi Hong Lan 《Computers, Materials & Continua》 2025年第12期5625-5642,共18页
Semi-supervised clustering techniques attempt to improve clustering accuracy by utilizing a limited number of labeled data for guidance.This method effectively integrates prior knowledge using pre-labeled data.While s... Semi-supervised clustering techniques attempt to improve clustering accuracy by utilizing a limited number of labeled data for guidance.This method effectively integrates prior knowledge using pre-labeled data.While semi-supervised fuzzy clustering(SSFC)methods leverage limited labeled data to enhance accuracy,they remain highly susceptible to inappropriate or mislabeled prior knowledge,especially in noisy or overlapping datasets where cluster boundaries are ambiguous.To enhance the effectiveness of clustering algorithms,it is essential to leverage labeled data while ensuring the safety of the previous knowledge.Existing solutions,such as the Trusted Safe Semi-Supervised Fuzzy Clustering Method(TS3FCM),struggle with random centroid initialization,fixed neighbor radius formulas,and handling outliers or noise at cluster overlaps.A new framework called Active Safe Semi-Supervised Fuzzy Clustering with Pairwise Constraints Based on Cluster Boundary(AS3FCPC)is proposed in this paper to deal with these problems.It does this by combining pairwise constraints and active learning.AS3FCPC uses active learning to query only the most informative data instances close to the cluster boundaries.It also uses pairwise constraints to enforce the cluster structure,which makes the system more accurate and robust.Extensive test results on diverse datasets,including challenging noisy and overlapping scenarios,demonstrate that AS3FCPC consistently achieves superior performance compared to state-of-the-art methods like TS3FCM and other baselines,especially when the data is noisy and overlaps.This significant improvement underscores AS3FCPC’s potential for reliable and accurate semisupervised fuzzy clustering in complex,real-world applications,particularly by effectively managing mislabeled data and ambiguous cluster boundaries. 展开更多
关键词 Active learning safe semi-supervised fuzzy clustering confidence weight boundary identification pairwise constraints
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Historical Safe Haven in Shanghai
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作者 LU JIAJUN 《China Today》 2025年第9期36-41,共6页
IN the Shanghai Jewish Refugees Museum,a beautiful handbag is waiting for its owner in a display cabinet.The handbag belongs to a Jewish couple.When they sought refuge in Shanghai during World War II,they pawned the h... IN the Shanghai Jewish Refugees Museum,a beautiful handbag is waiting for its owner in a display cabinet.The handbag belongs to a Jewish couple.When they sought refuge in Shanghai during World War II,they pawned the handbag to Jin Wenzhen’s grandfather in exchange for their child’s medical expenses.He lent the couple the cash equivalent of one month’s revenue from his rice shop,but then never saw them again. 展开更多
关键词 rice shop Jewish refugees SHANGHAI historical safe haven pawned handbag medical expenses World War II
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Navigating the safe and just operating space for urban systems:A cross-scale landscape approach
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作者 Hongyan Bian Jianguo Wu +4 位作者 Runxi Jia Linyong Wang Zihan Zhu Mengyu Wei Jie Gao 《Geography and Sustainability》 2025年第6期129-145,共17页
Safe and just operating spaces(SJOS)are influenced by complex cross-scale interactions and cascading effects spanning global,regional,and local landscape scales.However,existing SJOS research has often focused on sing... Safe and just operating spaces(SJOS)are influenced by complex cross-scale interactions and cascading effects spanning global,regional,and local landscape scales.However,existing SJOS research has often focused on single-scale assessments,overlooking the impacts of multiscale interactions and within-region heterogeneity on urban SJOS.To address this gap,we developed a cross-scale framework for assessing urban SJOS,explicitly incorporating top-down influences from upper-level constraints and bottom-up effects from lower-level heterogeneity.This approach was applied to China's five major metropolises to examine the states and cross-scale dynamics influencing urban SJOS between 1990 and 2020.Our findings reveal that the SJOS of China's metropolises were primarily influenced by factors at national and local landscape scales,with weaker influences from the global and continental scales.A persistent trade-off between social justice and environmental safety was identified across spatiotemporal scales.For instance,Chongqing in southwestern China lagged behind the eastern four metropolises in social performance but exhibited stronger environmental safety due to its extensive natural landscapes,which mitigated the anthropogenic impacts of urban centers.Regional issues,such as the overshoot of PM_(2.5)and ecological footprints(EF),were primarily driven by the bottom-up accumulation of localized pressures,while the overshoot of CO_(2)was attributed to national policy constraints and the universal exceedance of safe thresholds across scales.Addressing urban sustainability requires avoiding adverse cascading effects from other levels by emphasizing landscape heterogeneity within metropolises and fostering coordinated collaboration across scales,particularly at the regional landscape and national levels. 展开更多
关键词 safe and just operating space Cross-scale interaction Landscape approach Metropolises
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Bye microplastics! Ocean-safe straws that break down naturally
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作者 Zhao Xinhua 《China Textile》 2025年第3期26-27,共2页
Against the backdrop of the global push for environmental protection and the reduction of plastic pollution,the research and development of alternatives to daily disposable plastic products such as straws have become ... Against the backdrop of the global push for environmental protection and the reduction of plastic pollution,the research and development of alternatives to daily disposable plastic products such as straws have become a hot topic in the environmental protection field.Traditional plastic straws are difficult to degrade,imposing a severe burden on the environment.Meanwhile,existing alternatives like paper straws and PLA(polylactic acid)straws also have numerous drawbacks. 展开更多
关键词 traditional plastic straws paper straws ocean safe straws plastic pollution alternatives disposable plastics microplastics natural breakdown environmental protection
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Identification of Visibility Level for Enhanced Road Safety under Different Visibility Conditions:A Hierarchical Clustering-Based Learning Model
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作者 Asmat Ullah Yar Muhammad +4 位作者 Bakht Zada Korhan Cengiz Nikola Ivkovic Mario Konecki Abid Yahya 《Computers, Materials & Continua》 2025年第11期3767-3786,共20页
Low visibility conditions,particularly those caused by fog,significantly affect road safety and reduce drivers’ability to see ahead clearly.The conventional approaches used to address this problem primarily rely on i... Low visibility conditions,particularly those caused by fog,significantly affect road safety and reduce drivers’ability to see ahead clearly.The conventional approaches used to address this problem primarily rely on instrument-based and fixed-threshold-based theoretical frameworks,which face challenges in adaptability and demonstrate lower performance under varying environmental conditions.To overcome these challenges,we propose a real-time visibility estimation model that leverages roadside CCTV cameras to monitor and identify visibility levels under different weather conditions.The proposedmethod begins by identifying specific regions of interest(ROI)in the CCTVimages and focuses on extracting specific features such as the number of lines and contours detected within these regions.These features are then provided as an input to the proposed hierarchical clusteringmodel,which classifies them into different visibility levels without the need for predefined rules and threshold values.In the proposed approach,we used two different distance similaritymetrics,namely dynamic time warping(DTW)and Euclidean distance,alongside the proposed hierarchical clustering model and noted its performance in terms of numerous evaluation measures.The proposed model achieved an average accuracy of 97.81%,precision of 91.31%,recall of 91.25%,and F1-score of 91.27% using theDTWdistancemetric.We also conducted experiments for other deep learning(DL)-based models used in the literature and compared their performances with the proposed model.The experimental results demonstrate that the proposedmodel ismore adaptable and consistent compared to themethods used in the literature.The proposedmethod provides drivers real-time and accurate visibility information and enhances road safety during low visibility conditions. 展开更多
关键词 CCTV images road safety and security visibility level estimation hierarchical clustering learning feature extraction safe and secure transportation
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Safe and healthy working environment for occupational health:advancing evidence-informed policy-making
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作者 Min Zhang 《Global Health Journal》 2025年第2期63-64,F0002,共3页
With the civilization and modernization of human society,occupational health has emerged as a fundamental goal of social justice,as highlighted in the United Nations'Sustainable Development Goals(SDGs)since 2016.S... With the civilization and modernization of human society,occupational health has emerged as a fundamental goal of social justice,as highlighted in the United Nations'Sustainable Development Goals(SDGs)since 2016.Specifically,"SDG Goal 1:No Poverty","SDG 3:Good Health and Well-being",and"SDG 8:Decent Work and Economic Growth",are interconnected with other SDGs to support the pursuit of occupational health. 展开更多
关键词 modernization CIVILIZATION safe working environment development goals sdgs social justice occupational health evidence informed policy making healthy working environment
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气煤交叉开采三维可视化及风险预警研究
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作者 王文 周青山 +4 位作者 芦晓伟 郭润生 曹海波 张通 《河南理工大学学报(自然科学版)》 北大核心 2026年第1期86-94,共9页
目的为实时预警叠置区域内煤气开采潜在的风险,保障煤气交叉开采安全。以鄂尔多斯盆地内大牛地气田与呼吉尔特矿区某煤矿为工程背景,研究采动影响下天然气井受力变形特征与易破坏位置。方法建立天然气井安全避让距离控制预测方法,采用3d... 目的为实时预警叠置区域内煤气开采潜在的风险,保障煤气交叉开采安全。以鄂尔多斯盆地内大牛地气田与呼吉尔特矿区某煤矿为工程背景,研究采动影响下天然气井受力变形特征与易破坏位置。方法建立天然气井安全避让距离控制预测方法,采用3ds Max数字建模、Unity3D引擎和C#语言结合,开发煤气模型三维联动显示、交叉区域风险预警的三维可视化与风险预警平台,并开发六大功能模块。结果结果表明:以数字模型和场景搭建为基础,实现基于虚实映射的三维模型可视化,为预警平台设计开发奠定坚实基础;结合现场监测数据,提取分析采动影响下覆岩移动地表沉降对上覆油气管道变形影响,构建区域内地表下沉等值线分区的三维可视化;基于天然气井安全避让距离控制预测方法,实现天然气井与采煤工作面间的可视化实时风险预警;基于GNSS监测技术建立地表沉降监测、管道变形监测和天然气井安全避让距离监测相结合的综合风险预测预警平台。结论基于可视化平台实现气煤叠置区三维显示、数据监测和实时风险预警,可为气煤叠置区煤气协调开采提供参考,为煤气叠置区灾害防控提供依据。 展开更多
关键词 三维可视化 煤气协调开采 UNITY3D 安全避让距离 实时预警
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SAFE与SDE法对金华火腿皮下脂肪气味活性物质研究 被引量:28
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作者 刘笑生 刘建斌 +3 位作者 刘梦雅 何聪聪 杨政茂 宋焕禄 《食品科学技术学报》 CAS 2014年第1期40-46,共7页
通过溶剂辅助风味蒸发系统(SAFE)和同时蒸馏提取技术(SDE)与气相色谱-嗅闻仪-质谱联机法(GC-O-MS)结合,对已发酵18个月的金华火腿皮下脂肪气味化合物进行定性定量分析和感官评价.SAFE和SDE法分别检测并嗅闻到40种和22种气味活性化合物,... 通过溶剂辅助风味蒸发系统(SAFE)和同时蒸馏提取技术(SDE)与气相色谱-嗅闻仪-质谱联机法(GC-O-MS)结合,对已发酵18个月的金华火腿皮下脂肪气味化合物进行定性定量分析和感官评价.SAFE和SDE法分别检测并嗅闻到40种和22种气味活性化合物,对脂肪气味贡献度较大的10种关键性化合物分别是:己醛、庚醛、二异丙基二硫醚、辛醛、反-2-辛烯醛、3-甲基丁酸、反,反-2,4-癸二烯醛、γ-癸内酯、γ-十一内酯和苯乙酸. 展开更多
关键词 safe SDE 金华火腿皮下脂肪 气味活性物质
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SPME和SAFE结合GC-O-MS分析鲜榨西瓜汁挥发性香气成分 被引量:39
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作者 何聪聪 刘梦雅 +3 位作者 刘建彬 刘笑生 刘野 宋焕禄 《食品工业科技》 CAS CSCD 北大核心 2014年第2期49-53,58,共6页
为比较不同萃取方式对西瓜汁风味的萃取效果,本研究采用固相微萃取(SPME)和溶剂辅助风味蒸发(SAFE)两种方法结合GC-O-MS对无籽西瓜中的挥发性香气成分进行分析。共鉴定出46种化合物,这些化合物主要包括醛类8种,烯醛类9种,醇类12种,酮类6... 为比较不同萃取方式对西瓜汁风味的萃取效果,本研究采用固相微萃取(SPME)和溶剂辅助风味蒸发(SAFE)两种方法结合GC-O-MS对无籽西瓜中的挥发性香气成分进行分析。共鉴定出46种化合物,这些化合物主要包括醛类8种,烯醛类9种,醇类12种,酮类6种,呋喃2种,内酯1种,酯类2种。无籽西瓜中重要的挥发性香气成分有己醛(青草香)、6-甲基-5-庚烯-2-酮(柠檬味、苹果味)、反-6-壬烯醛(甜瓜味)、反-2-壬烯醛(甜瓜味、清香)、反,顺-2,6壬二烯醛(黄瓜味)、顺-3-壬烯-1-醇(清香、动物脂味)、反,顺-3,6-壬二烯-1-醇(黄瓜味)。SPME和SAFE对西瓜汁中关键香气成分均具有良好的萃取效果,但SPME萃取得到的化合物种类更多。 展开更多
关键词 溶剂辅助风味蒸发 固相微萃取 西瓜 香气成分
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SAFE-GC-MS分析酸牛奶挥发性成分 被引量:34
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作者 刘南南 郑福平 +6 位作者 张玉玉 范婷婷 黄明泉 陈海涛 刘玉平 谢建春 孙宝国 《食品科学》 EI CAS CSCD 北大核心 2014年第22期150-153,共4页
采用溶剂辅助风味蒸发法萃取原味酸牛奶挥发性成分,利用气相色谱-质谱联用法结合保留指数、标准品对照对挥发性成分进行定性分析,采用面积归一化法加邻二氯苯作内标定量,共鉴定出挥发性成分52种,其中酸12种、醛2种、酮5种、醇2种、酯3... 采用溶剂辅助风味蒸发法萃取原味酸牛奶挥发性成分,利用气相色谱-质谱联用法结合保留指数、标准品对照对挥发性成分进行定性分析,采用面积归一化法加邻二氯苯作内标定量,共鉴定出挥发性成分52种,其中酸12种、醛2种、酮5种、醇2种、酯3种、内酯2种、烯烃4种、烷烃17种、其他5种。其中,对酸牛奶风味影响较大的可能有乙酸、丁酸、己酸、辛酸、癸酸、9-癸稀酸、乙偶姻、2-壬酮、2-十一酮、壬醛、香兰素、3-甲基-2-丁烯-1-醇、十六硫醇、丁位癸内酯、丁位十二内酯等。 展开更多
关键词 酸牛奶 溶剂辅助风味蒸发 气相色谱-质谱联用 挥发性成分 保留指数 标准品
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基于Fe-safe螺杆泵定子橡胶疲劳裂纹形成寿命预测 被引量:13
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作者 祖海英 耿春丽 +1 位作者 李大奇 宋玉杰 《机械强度》 CAS CSCD 北大核心 2018年第1期195-199,共5页
采油用螺杆泵橡胶定子为研究对象,通过对定子橡胶材料的进行伸张疲劳试验,建立定子橡胶的S-N曲线;对螺杆泵进行力学特性分析,确定在靠近高压腔室螺旋密封带上螺杆泵最易发生疲劳失效;利用Fe-safe对螺杆泵定子橡胶进行疲劳裂纹形成寿命... 采油用螺杆泵橡胶定子为研究对象,通过对定子橡胶材料的进行伸张疲劳试验,建立定子橡胶的S-N曲线;对螺杆泵进行力学特性分析,确定在靠近高压腔室螺旋密封带上螺杆泵最易发生疲劳失效;利用Fe-safe对螺杆泵定子橡胶进行疲劳裂纹形成寿命进行预测研究,确定螺杆泵定子橡胶各段模型的最小疲劳裂纹形成寿命和安全系数和随腔室压力的关系,即随腔室压力升高而下降,并拟合得到橡胶定子疲劳裂纹形成寿命与腔室压力的关系式。 展开更多
关键词 螺杆泵 定子橡胶 裂纹形成寿命 S-N曲线 Fe-safe分析
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SDE与SAFE分析全脂巴氏乳挥发性成分 被引量:8
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作者 艾娜丝 张晓梅 +3 位作者 仝令君 王静 孙宝国 郑福平 《食品研究与开发》 CAS 北大核心 2016年第10期109-112,5,共4页
采用同时蒸馏萃取与溶剂辅助风味蒸发法萃取分析巴氏全脂乳的挥发性成分,用气相色谱-质谱联用(GC-MS)对挥发性成分进行了分析。结果表明同时蒸馏萃取法以二氯甲烷为萃取溶剂时鉴定出8种成分,以乙醚为萃取溶剂时鉴定出6种成分;溶剂辅助... 采用同时蒸馏萃取与溶剂辅助风味蒸发法萃取分析巴氏全脂乳的挥发性成分,用气相色谱-质谱联用(GC-MS)对挥发性成分进行了分析。结果表明同时蒸馏萃取法以二氯甲烷为萃取溶剂时鉴定出8种成分,以乙醚为萃取溶剂时鉴定出6种成分;溶剂辅助风味蒸发法鉴定出8种,两种方法共计鉴定出14种挥发性成分,其中酸类8种、醛类1种、醇类2种、酯类2种、其它类1种,其中含量较大的有己酸、辛酸、癸酸、月桂酸、肉豆蔻酸等。 展开更多
关键词 巴氏全脂乳 同时蒸馏萃取 溶剂辅助风味蒸发 气质联用 挥发性成分
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