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Tomographic velocity inversion for ADCIGs in areas with a rugged surface 被引量:2
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作者 张凯 李振春 +2 位作者 曾同生 秦宁 姚云霞 《Applied Geophysics》 SCIE CSCD 2012年第3期313-318,361,共7页
Pre-stack depth migration velocity analysis is one of the key techniques influencing image quality. As for areas with a rugged surface and complex subsurface, conventional prestack depth migration velocity analysis co... Pre-stack depth migration velocity analysis is one of the key techniques influencing image quality. As for areas with a rugged surface and complex subsurface, conventional prestack depth migration velocity analysis corrects the rugged surface to a known datum or designed surface velocity model on which to perform migration and update the velocity. We propose a rugged surface tomographic velocity inversion method based on angle-domain common image gathers by which the velocity field can be updated directly from the rugged surface without static correction for pre-stack data and improve inversion precision and efficiency. First, we introduce a method to acquire angle-domain common image gathers (ADCIGs) in rugged surface areas and then perform rugged surface tornographic velocity inversion. Tests with model and field data prove the method to be correct and effective. 展开更多
关键词 rugged surface angle-domain common image gathers tomographic inversion velocity modeling
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Two-dimensional frequency-domain acoustic fullwaveform inversion with rugged topography 被引量:1
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作者 张钱江 戴世坤 +3 位作者 陈龙伟 李昆 赵东东 黄兴兴 《Applied Geophysics》 SCIE CSCD 2015年第3期378-388,467,468,共13页
We studied finite-element-method-based two-dimensional frequency-domain acoustic FWI under rugged topography conditions. The exponential attenuation boundary condition suitable for rugged topography is proposed to sol... We studied finite-element-method-based two-dimensional frequency-domain acoustic FWI under rugged topography conditions. The exponential attenuation boundary condition suitable for rugged topography is proposed to solve the cutoff botmdary problem as well as to consider the requirement of using the same subdivision grid in joint multifrequency inversion. The proposed method introduces the attenuation factor, and by adjusting it, acoustic waves are sufficiently attenuated in the attenuation layer to minimize the cutoff boundary effect. Based on the law of exponential attenuation, expressions for computing the attenuation factor and the thickness of attenuation layers are derived for different frequencies. In multifrequency-domain FWI, the conjugate gradient method is used to solve equations in the Gauss-Newton algorithm and thus minimize the computation cost in calculating the Hessian matrix. In addition, the effect of initial model selection and frequency combination on FWI is analyzed. Examples using numerical simulations and FWI calculations are used to verify the efficiency of the proposed method. 展开更多
关键词 Full-waveform inversion rugged topography attenuation boundary condition finite element method
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Rugged Resonant Pole and Its Applications in Soft-Switching Converter
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作者 肖岚 严仰光 《Journal of Southeast University(English Edition)》 EI CAS 2002年第3期225-232,共8页
The soft switching operation principle and operation performance of rugged resonant pole (RRP) is given. The applications of RRP in soft switching DC DC converter and soft switching inverter are discussed in detail. R... The soft switching operation principle and operation performance of rugged resonant pole (RRP) is given. The applications of RRP in soft switching DC DC converter and soft switching inverter are discussed in detail. RRP can constitute buck boost soft switching DC DC converter and isolated soft switching DC DC converter with the automatic limitation performance of output power. Partial series resonant DC DC converter with RRP can realize the zero voltage/zero current switching of power devices. RR... 展开更多
关键词 rugged resonant pole soft switching DC DC converter INVERTER
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Plane-Wave Least-Squares Reverse Time Migration for Rugged Topography 被引量:7
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作者 Jianping Huang Chuang Li +1 位作者 Rongrong Wang Qingyang Li 《Journal of Earth Science》 SCIE CAS CSCD 2015年第4期471-480,共10页
We present a method based on least-squares reverse time migration with plane-wave encoding (P-LSRTM) for rugged topography. Instead of modifying the wave field before migration, we modify the plane-wave encoding fun... We present a method based on least-squares reverse time migration with plane-wave encoding (P-LSRTM) for rugged topography. Instead of modifying the wave field before migration, we modify the plane-wave encoding function and fill constant velocity to the area above rugged topography in the model so that P-LSRTM can be directly performed from rugged surface in the way same to shot domain reverse time migration. In order to improve efficiency and reduce I/O (input/output) cost, the dynamic en- coding strategy and hybrid encoding strategy are implemented. Numerical test on SEG rugged topography model show that P-LSRTM can suppress migration artifacts in the migration image, and compensate am- plitude in the middle-deep part efficiently. Without data correction, P-LSRTM can produce a satisfying image of near-surface if we could get an accurate near-surface velocity model. Moreover, the pre-stack P- LSRTM is more robust than conventional RTM in the presence of migration velocity errors. 展开更多
关键词 least-squares migration rugged topography plane-wave encoding dynamic encoding hybrid encoding.
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Distributed modeling of direct solar radiation on rugged terrain of the Yellow River Basin 被引量:4
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作者 ZENG Yan QIU Xinfa +1 位作者 LIU Changming JIANG Aijun 《Journal of Geographical Sciences》 SCIE CSCD 2005年第4期439-447,共9页
Due to the influences of local topographical factors and terrain inter-shielding, calculation of direct solar radiation (DSR) quantity of rugged terrain is very complex. Based on digital elevation model (DEM) data... Due to the influences of local topographical factors and terrain inter-shielding, calculation of direct solar radiation (DSR) quantity of rugged terrain is very complex. Based on digital elevation model (DEM) data and meteorological observations, a distributed model for calculating DSR over rugged terrain is developed. This model gives an all-sided consideration on factors influencing th a resolution of 1 km × 1 km for thDSR. Using the developed model, normals of annual DSR quantity wie Yellow River Basin was generated, with DEM data as the general characterization of terrain. Characteristics of DSR quantity influenced by geographic and topographic factors over rugged terrain were analyzed thoroughly. Results suggest that: influenced by local topographic factors, i.e. azimuth, slope and so on, and annual DSR quantity over mountainous area has a clear spatial difference; annual DSR quantity of sunny slope (or southern slope) of mountains is obviously larger than that of shady slope (or northern slope). The calculated DSR quantity of the Yellow River Basin is provided in the same way as other kinds of spatial information and can be employed as basic geographic data for relevant studies as well. 展开更多
关键词 direct solar radiation (DSR) rugged terrain digital elevation model (DEM) distributed model Yellow River Basin
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Distributed Modeling of Extraterrestrial Solar Radiation Over the Rugged Terrains of Pakistan 被引量:3
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作者 Romana AMBREEN QIU Xinfa Iftikhar AHMAD 《Journal of Mountain Science》 SCIE CSCD 2011年第3期427-436,共10页
In Pakistan,the solar analogue has been addressed but its surface geographical parameterization has given least attention.Inappropriate density of stations and their spatial coverage particularly in difficult peripher... In Pakistan,the solar analogue has been addressed but its surface geographical parameterization has given least attention.Inappropriate density of stations and their spatial coverage particularly in difficult peripheral national territories,little or no solar radiation data,non-satisfactory sunshine hours data,and low quality of ground observed cloud cover data create a situation in which the spatial modeling of Extraterrestrial Solar Radiation(ESR) and its ground parameterization got sufficient scope.The Digital Elevation Model (DEM) input into Geographic Information System (GIS) is a compatible tool to demonstrate the spatial distribution of ESR over the rugged terrains of the study domain.For the first time,distributed modeling of ESR is done over the rugged terrains of Pakistan,based on DEM and ArcGIS..Results clearly depict that the complex landforms profoundly disrupt the zonal distribution of ESR in Pakistan.The screening impact of topography is higher on spatial distribution of ESR in winter and considerably low in summer.The combined effect of topography and latitude is obvious.Hence,the model was further testified by plotting Rb (ratio of ESR quantity over rugged terrain against plane surface) against azimuth at different latitudes with different angled slopes.The results clearly support the strong screening effect of rugged terrain through out the country especially in Himalayas,Karakoram and Hindukush (HKH),western border mountains and Balochistan Plateau.This model can be instrumental as baseline geospatial information for scientific investigations in Pakistan,where substantial fraction of national population is living in mountainous regions. 展开更多
关键词 Pakistan distributed modeling ESR DEM GIS rugged terrain
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Application of Gaussian beam pre-stack depth migration in rugged seabed
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作者 HAN Fuxing YI Xin +3 位作者 SUN Zhangqing HU Jia XU Baoyin XU Hai 《Global Geology》 2021年第2期119-128,共10页
Strong fluctuation of seabed,abrupt variation in depth and dip of seabed bring seismic imaging problems,such as irregular reflection waves,obvious multiple waves,serious lateral wave development,poor imaging on base s... Strong fluctuation of seabed,abrupt variation in depth and dip of seabed bring seismic imaging problems,such as irregular reflection waves,obvious multiple waves,serious lateral wave development,poor imaging on base surface and depression structure,low signal-to-noise ratio of middle and deep layers.In this paper,Gaussian beam migration imaging method is used to analyze the imaging effect of rugged seabed in deep water area,and the ray tracing method of wavefront construction method is used to analyze the kinematic characteristics of seismic waves.By improving the design of seismic data acquisition and observation system,imaging quality of fine structures is improved. 展开更多
关键词 Gaussian beam migration wavefront construction method Gaussian beam pre-stack depth rugged seabed
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户外爱好者挚爱 Lacia Rugged XL移动硬盘
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《数码》 2009年第5期34-34,共1页
不管做什么都讲究专业.哪怕是移动硬盘这样的小东西。对于户外爱好者和探险家来说.拥有一款可以和JEEP媲美的移动硬盘同样重要。它必须拥有结实的外表.舒适的使用环境,超强的速度体验.能够克服任何恶劣的环境,它就是来自法国莱希L... 不管做什么都讲究专业.哪怕是移动硬盘这样的小东西。对于户外爱好者和探险家来说.拥有一款可以和JEEP媲美的移动硬盘同样重要。它必须拥有结实的外表.舒适的使用环境,超强的速度体验.能够克服任何恶劣的环境,它就是来自法国莱希Lacie的移动硬盘Rugged XL——探路者。 展开更多
关键词 移动硬盘 使用环境 Lacia rugged XL
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QuEChERS-液相色谱串联高分辨质谱法检测果蔬中34种农药残留 被引量:1
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作者 罗景阳 周长民 +5 位作者 刘鑫 袁帅 李巧莲 李娇 张承昕 王岩松 《食品研究与开发》 2025年第13期165-176,共12页
采用QuEChERS(quick,easy,cheap,effective,rugged and safe)-液相色谱串联高分辨质谱法建立蔬菜水果样品中34种农药残留的检测方法,并建立数据库。样品提取条件为4 g无水硫酸镁、1.5 g无水乙酸钠、1 g氯化钠和10 mL乙腈(1%乙酸),净化... 采用QuEChERS(quick,easy,cheap,effective,rugged and safe)-液相色谱串联高分辨质谱法建立蔬菜水果样品中34种农药残留的检测方法,并建立数据库。样品提取条件为4 g无水硫酸镁、1.5 g无水乙酸钠、1 g氯化钠和10 mL乙腈(1%乙酸),净化剂条件为10 mg石墨化碳黑、500 mg乙二胺-N-丙基硅烷化硅胶、600 mg MgSO_(4)和200 mg C_(18),在乙腈-水流动相条件下,选择C_(18)色谱柱进行目标物分离,采用一级全扫描-触发二级全扫描模式进行检测,检测结果通过保留时间、一级精确分子质量和二级碎片进行定性,通过一级精确分子质量对样品进行定量,以韭菜、菠菜、茄子、葡萄、桃和香蕉为代表样品,采用基质匹配标准曲线法进行定量。结果表明,各农药在相应线性范围内呈现良好的线性关系,R2均大于0.99,检出限为1~5μg/kg,定量限为2~10μg/kg,回收率为70.06%~119.79%,精密度为0.23%~13.77%。该方法具有简便快速、准确度高、灵敏度好的特点,适用于蔬菜水果中34种农药的检测。 展开更多
关键词 农药残留 高分辨质谱 QuEChERS(quick EASY cheap effective rugged and safe) 水果 蔬菜
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代理模型辅助的复杂地形风电场微观选址多目标优化设计
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作者 刘佳惠 王聪 +3 位作者 张宏立 马萍 李新凯 董颖超 《上海交通大学学报》 北大核心 2025年第9期1315-1326,共12页
为解决复杂地形下风电场微观选址优化难度大、耗时长的问题,提出一种基于代理模型辅助的复杂地形风电场微观选址多目标优化方法.首先,考虑复杂地形起伏大的地理特征,计算崎岖度指数,将地面平整度进行数值量化,并对崎岖度过大的点进行约... 为解决复杂地形下风电场微观选址优化难度大、耗时长的问题,提出一种基于代理模型辅助的复杂地形风电场微观选址多目标优化方法.首先,考虑复杂地形起伏大的地理特征,计算崎岖度指数,将地面平整度进行数值量化,并对崎岖度过大的点进行约束处理;其次,建立三维多风向下尾流叠加计算发电量的数学模型,构建三维地形集电线路拓扑优化代理模型,检验代理模型的预测精度,表明可替代集电线路拓扑优化的大量计算,有效提高计算效率,然后采用多目标离散状态转移算法,获得复杂地形微观选址多目标优化设计的Pareto前沿;最后,以中国新疆某实际复杂地形风电场为例,实现复杂地形风电场多目标微观选址,并将该算法与单目标优化结果进行比较.仿真结果表明,在考虑复杂地形因素特点的情况下,代理模型辅助的多目标离散状态转移算法能在优化年发电量的前提下减少总电缆铺设长度,降低工程建设投资,为工程实际提供更多布局方案. 展开更多
关键词 风电场 微观选址 复杂地形 多目标优化算法 崎岖度指数 代理模型
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Distributed modeling of monthly air temperatures over the rugged terrain of the Yellow River Basin 被引量:12
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作者 ZENG Yan QIU XinFa +2 位作者 HE YongJian SHI GuoPing LIU ChangMing 《Science China Earth Sciences》 SCIE EI CAS 2009年第5期694-707,共14页
Our analyses of the monthly mean air temperature of meteorological stations show that altitude, global solar radiation and surface effective radiation have a significant impact on air temperature. We set up a physical... Our analyses of the monthly mean air temperature of meteorological stations show that altitude, global solar radiation and surface effective radiation have a significant impact on air temperature. We set up a physically-based empirical model for monthly air temperature simulation. Combined the proposed model with the distributed modeling results of global solar radiation and routine meteorological observation data, we also developed a method for the distributed simulation of monthly air temperatures over rugged terrain. Spatial distribution maps are generated at a resolution of 1 km×1 km for the monthly mean, the monthly mean maximum and the monthly mean minimum air temperatures for the Yellow River Basin. Analysis shows that the simulation results reflect to a considerable extent the macro and local distribution characteristics of air temperature. Cross-validation shows that the proposed model displays good stability with mean absolute bias errors of 0.19°C–0.35°C. Tests carried out on local meteorological station data and case year data show that the model has good spatial and temporal simulation capacity. The proposed model solely uses routine meteorological data and can be applied easily to other regions. 展开更多
关键词 YELLOW RIVER BASIN MONTHLY mean air temperature rugged TERRAIN DISTRIBUTED modeling
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Modeling the land surface reflectance for optical remote sensing data in rugged terrain 被引量:12
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作者 WEN JianGuang LIU QinHuo +2 位作者 XIAO Qing LIU Qiang LI XiaoWen 《Science China Earth Sciences》 SCIE EI CAS 2008年第8期1169-1178,共10页
A model for topographic correction and land surface reflectance estimation for optical remote sensing data in rugged terrian is presented.Considering a directional-directional reflectance that is used for direct solar... A model for topographic correction and land surface reflectance estimation for optical remote sensing data in rugged terrian is presented.Considering a directional-directional reflectance that is used for direct solar irradiance correction and a hemispheric-directional reflectance that is used for atmospheric diffuse irradiance and terrain background reflected irradiance correction respectively,the directional reflectance-based model for topographic effects removing and land surface reflectance calculation is developed by deducing the directional reflectance with topographic effects and using a radiative transfer model.A canopy reflectance simulated by GOMS model and Landsat/TM raw data covering Jiangxi rugged area were taken to validate the performance of the model presented in the paper.The validation results show that the model presented here has a remarkable ability to correct topography and estimate land surface reflectance and also provides a technique method for sequently quantitative remote sensing application in terrain area. 展开更多
关键词 bidirectional reflectance topographic/atmospheric correction SKY DIFFUSE IRRADIANCE ADJACENT terrain-reflected IRRADIANCE rugged area
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An RF LDMOS with excellent efficiency and ruggedness based on a modified CMOS process 被引量:2
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作者 余庭 罗玲 《Journal of Semiconductors》 EI CAS CSCD 2013年第9期63-66,共4页
Two types of RF LDMOS devices, specified for application in the driver stage and output stage of a power amplifier, are designed based on a modified CMOS process. By optimizing the layout and process, the output capac... Two types of RF LDMOS devices, specified for application in the driver stage and output stage of a power amplifier, are designed based on a modified CMOS process. By optimizing the layout and process, the output capacitance per unit of gate width is as low as 225 fF/mm. The driver stage and output stage devices achieve an output power of 44 W with a PAE of 82% and 230 W with a PAE of 72.3%, respectively (P3aB compression) at 1 GHz. Both devices are capable of withstanding extremely severe ruggedness tests without any performance degradation. These tests are 3-5 dB overdrive, 10:1 voltage standing wave ratio mismatch load through all phase angles, and 40% drain overvoltage elevation at a working point of P3aB. 展开更多
关键词 PAE ruggedNESS RF LDMOS CMOS output power
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VPX总线解析与接口设计
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作者 郭建平 欧阳迪 +1 位作者 樊凯 刘泽源 《机电产品开发与创新》 2025年第6期5-8,共4页
VPX总线作为ANSI/VITA标准体系之一的新一代计算机模块化互连标准,以其高带宽、高速率、高可靠性和稳定性、灵活的扩展性和模块化设计,涵盖了RapidIO、PCIe、以太网、光纤通信等多种常见的高速通信总线,受到各界的广泛好评,特别是在工... VPX总线作为ANSI/VITA标准体系之一的新一代计算机模块化互连标准,以其高带宽、高速率、高可靠性和稳定性、灵活的扩展性和模块化设计,涵盖了RapidIO、PCIe、以太网、光纤通信等多种常见的高速通信总线,受到各界的广泛好评,特别是在工业、军事、航空航天和其他高可靠性的电子系统中,VPX总线成为了高速信号处理、高速数据传输与交换、加固型产品设计等应用不可或缺的技术手段,基于VPX总线开展的各类产品研制技术,也必将是引领未来高性能、高速数据通信领域的最前沿技术。 展开更多
关键词 VPX总线 ANSI/VITA 高速通信 模块化设计 加固型产品
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某电厂老旧冷却塔结构检测鉴定研究 被引量:2
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作者 汪潇 张晓 时兴 《江苏建材》 2024年第2期5-7,共3页
一座大型老旧电厂的冷却塔出现了混凝土剥落和钢筋腐蚀的现象。利用大型3D激光雷达对塔架进行倾斜状态监测,对其混凝土强度、缺陷及循环水中的氯离子浓度等指标进行测试,并对其损伤机理进行了研究,获得了详尽的现场检测结果。通过综合评... 一座大型老旧电厂的冷却塔出现了混凝土剥落和钢筋腐蚀的现象。利用大型3D激光雷达对塔架进行倾斜状态监测,对其混凝土强度、缺陷及循环水中的氯离子浓度等指标进行测试,并对其损伤机理进行了研究,获得了详尽的现场检测结果。通过综合评估,为炼钢厂冷却塔结构提供了科学的鉴定结论,为后续维护与改造提供了重要参考。 展开更多
关键词 冷却塔 检测鉴定 倾斜检测 加固设计
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基于改进离散状态转移算法的复杂地形崎岖度约束风电场微观选址优化
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作者 刘佳惠 王聪 +2 位作者 张宏立 马萍 李新凯 《可再生能源》 CAS CSCD 北大核心 2024年第12期1618-1626,共9页
为解决复杂地形下风电场微观选址问题,文章提出了一种基于改进离散状态转移算法(RC-DSTA)的优化策略。首先,为解决地面平整度对风机安置的影响,引入崎岖度指数(TRI)将地面平整度进行数值量化,并对崎岖度过大的点进行约束处理;然后,提出... 为解决复杂地形下风电场微观选址问题,文章提出了一种基于改进离散状态转移算法(RC-DSTA)的优化策略。首先,为解决地面平整度对风机安置的影响,引入崎岖度指数(TRI)将地面平整度进行数值量化,并对崎岖度过大的点进行约束处理;然后,提出一种基于离散状态转移算法(DSTA)的多风向下三维尾流叠加计算发电量的风机布局优化方法,并对离散状态转移算法进行改进,减少适应度值的计算时间,以缩短复杂计算优化问题的计算时长,提高计算效率;最后,以新疆某实际复杂地形风电场为例,在同一地形条件和目标函数背景下,将该算法与遗传算法(GA)和工程设计的微观选址结果进行比较。结果表明,在考虑地形因素特点的情况下,提供合理的风机布局方案,RC-DSTA比其他两种方法更有效。 展开更多
关键词 风电场 微观选址 复杂地形 离散状态转移算法 崎岖度指数
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某国产化加固计算机主板抗振性分析与改进
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作者 李风新 徐立颖 任志超 《电子机械工程》 2024年第2期19-24,共6页
文中针对某国产化加固计算机在振动试验后主板板载内存产生应力损伤的问题,应用仿真软件对机箱结构和主板安装结构进行了应变、应力分析,得出了机箱和主板在随机振动和冲击激励下的响应数值。针对主板的应变、应力分析结果,提出了理论... 文中针对某国产化加固计算机在振动试验后主板板载内存产生应力损伤的问题,应用仿真软件对机箱结构和主板安装结构进行了应变、应力分析,得出了机箱和主板在随机振动和冲击激励下的响应数值。针对主板的应变、应力分析结果,提出了理论校核方法。通过对比分析机箱和主板安装结构在不同约束条件下的仿真结果,根据仿真数值与理论限制之间的校核结论,结合主板安装结构形式,给出了针对性的改进措施。试验验证表明,改进后的结构形式对主板的刚性固定效果较好,解决了设备主板在振动试验后出现应力损伤的问题,提高了主板的抗振性能,可为类似设备的主板安装结构设计提供参考。 展开更多
关键词 加固计算机 主板 振动 仿真分析 应力
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加固计算机振动仿真及其电路板抗振设计 被引量:1
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作者 黄义科 周代强 黄平刚 《电子机械工程》 2024年第2期25-29,共5页
文中针对某型加固计算机在振动试验中出现硬盘无法读取的问题,通过有限元软件对其进行模态、谐响应分析后,结合实测数据,将故障原因定位为主板刚度不足引发共振进而导致硬盘无法读取。结构整改后,主板不再发生共振,样机试验过程中故障... 文中针对某型加固计算机在振动试验中出现硬盘无法读取的问题,通过有限元软件对其进行模态、谐响应分析后,结合实测数据,将故障原因定位为主板刚度不足引发共振进而导致硬盘无法读取。结构整改后,主板不再发生共振,样机试验过程中故障不再出现,测试点的加速度明显减小。进一步探讨加固计算机电路板抗振设计方法。通过厚度、紧固螺钉间距近似计算电路板固有频率,得到了几组可广泛适用于加固计算机电路板厚度、紧固螺钉间距的设计值。 展开更多
关键词 加固计算机 有限元仿真 振动 螺钉间距 固有频率
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一种加固型超融合服务器的模块化高密度设计
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作者 陈爱波 何春林 +1 位作者 张新健 高葛 《工业控制计算机》 2024年第8期138-139,142,共3页
设计一种加固型服务器,采用计算、存储、网络、管理为一体的融合架构,作为野战应用信息处理系统的核心服务设备。服务器结构采用模块化、少线缆设计,主要由机箱模块、计算存储模块、管理交换模块、IO接口模块及电源模块等部件组成,各电... 设计一种加固型服务器,采用计算、存储、网络、管理为一体的融合架构,作为野战应用信息处理系统的核心服务设备。服务器结构采用模块化、少线缆设计,主要由机箱模块、计算存储模块、管理交换模块、IO接口模块及电源模块等部件组成,各电气模块相互独立可拔插,提升系统可靠性、维修性。为尽可能提高空间利用率,对计算存储模块的结构设计以及各电气模块在机箱内的布局设计,均做到极致紧凑,使加固服务器计算密度达到领先的0.337颗CPU/dm3。 展开更多
关键词 加固型服务器 超融合 模块化 可拔插 高计算密度
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QuEChERS-UPLC-MS/MS检测畜禽组织中金刚烷胺残留 被引量:6
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作者 李彦 关丽丽 +6 位作者 牟妍 孙磊丽 梁君妮 沙美兰 邹文晓 孙爱丽 曹鹏 《食品研究与开发》 CAS 北大核心 2013年第23期37-40,共4页
建立一种QuEChERS-超高效液相色谱-串联质谱(QuEChERS-UPLC-MS/MS)检测畜禽组织中金刚烷胺残留的方法。样品用1%乙酸乙腈溶液超声提取,提取液加入C18和PSA填料进行基质分散固相净化,浓缩后经Proshell120 EC-C18柱分离,用电喷雾离子源正... 建立一种QuEChERS-超高效液相色谱-串联质谱(QuEChERS-UPLC-MS/MS)检测畜禽组织中金刚烷胺残留的方法。样品用1%乙酸乙腈溶液超声提取,提取液加入C18和PSA填料进行基质分散固相净化,浓缩后经Proshell120 EC-C18柱分离,用电喷雾离子源正离子多反应监测(MRM)模式进行检测。在0.2μg/L^100.0μg/L线性范围内具有较好的线性关系,相关系数大于0.997。该方法检出限(LOD)为0.6μg/kg,定量限(LOQ)为2.0μg/kg,回收率为70.5%~100.1%,相对标准偏差(RSD)小于10%。该方法简便快速、准确度好,适用于畜禽组织中金刚烷胺药物残留的检测。 展开更多
关键词 Quick Easy Cheap rugged Safe(QuEChERS) 超高效液相色谱串联质谱 金刚烷胺 畜禽组织 Quick Easy Cheap rugged Safe (QuEChERS)
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