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Tomographic velocity inversion for ADCIGs in areas with a rugged surface 被引量:2
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作者 张凯 李振春 +2 位作者 曾同生 秦宁 姚云霞 《Applied Geophysics》 SCIE CSCD 2012年第3期313-318,361,共7页
Pre-stack depth migration velocity analysis is one of the key techniques influencing image quality. As for areas with a rugged surface and complex subsurface, conventional prestack depth migration velocity analysis co... Pre-stack depth migration velocity analysis is one of the key techniques influencing image quality. As for areas with a rugged surface and complex subsurface, conventional prestack depth migration velocity analysis corrects the rugged surface to a known datum or designed surface velocity model on which to perform migration and update the velocity. We propose a rugged surface tomographic velocity inversion method based on angle-domain common image gathers by which the velocity field can be updated directly from the rugged surface without static correction for pre-stack data and improve inversion precision and efficiency. First, we introduce a method to acquire angle-domain common image gathers (ADCIGs) in rugged surface areas and then perform rugged surface tornographic velocity inversion. Tests with model and field data prove the method to be correct and effective. 展开更多
关键词 rugged surface angle-domain common image gathers tomographic inversion velocity modeling
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应用RUGⅢ对脑梗塞康复病例试行分类的研究 被引量:7
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作者 姚瑾 刘松筠 +2 位作者 党雅君 刘桂芬 王万斌 《中国康复理论与实践》 CSCD 1996年第4期171-175,共5页
采用RUGⅢ这一新的慢性病例分类模式,对我院75例脑梗塞康复患者试行分类,结果表明,RUGⅢ能比较客观地反映康复医疗的全面成本,可表明费用支付的合理性。同时,探讨了RUGⅢ对疗养、家庭病床、临终护理等机构的费用管理的... 采用RUGⅢ这一新的慢性病例分类模式,对我院75例脑梗塞康复患者试行分类,结果表明,RUGⅢ能比较客观地反映康复医疗的全面成本,可表明费用支付的合理性。同时,探讨了RUGⅢ对疗养、家庭病床、临终护理等机构的费用管理的意义。 展开更多
关键词 脑梗塞 康复 rug 病例分类
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Two-dimensional frequency-domain acoustic fullwaveform inversion with rugged topography 被引量:1
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作者 张钱江 戴世坤 +3 位作者 陈龙伟 李昆 赵东东 黄兴兴 《Applied Geophysics》 SCIE CSCD 2015年第3期378-388,467,468,共13页
We studied finite-element-method-based two-dimensional frequency-domain acoustic FWI under rugged topography conditions. The exponential attenuation boundary condition suitable for rugged topography is proposed to sol... We studied finite-element-method-based two-dimensional frequency-domain acoustic FWI under rugged topography conditions. The exponential attenuation boundary condition suitable for rugged topography is proposed to solve the cutoff botmdary problem as well as to consider the requirement of using the same subdivision grid in joint multifrequency inversion. The proposed method introduces the attenuation factor, and by adjusting it, acoustic waves are sufficiently attenuated in the attenuation layer to minimize the cutoff boundary effect. Based on the law of exponential attenuation, expressions for computing the attenuation factor and the thickness of attenuation layers are derived for different frequencies. In multifrequency-domain FWI, the conjugate gradient method is used to solve equations in the Gauss-Newton algorithm and thus minimize the computation cost in calculating the Hessian matrix. In addition, the effect of initial model selection and frequency combination on FWI is analyzed. Examples using numerical simulations and FWI calculations are used to verify the efficiency of the proposed method. 展开更多
关键词 Full-waveform inversion rugged topography attenuation boundary condition finite element method
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Rugged Resonant Pole and Its Applications in Soft-Switching Converter
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作者 肖岚 严仰光 《Journal of Southeast University(English Edition)》 EI CAS 2002年第3期225-232,共8页
The soft switching operation principle and operation performance of rugged resonant pole (RRP) is given. The applications of RRP in soft switching DC DC converter and soft switching inverter are discussed in detail. R... The soft switching operation principle and operation performance of rugged resonant pole (RRP) is given. The applications of RRP in soft switching DC DC converter and soft switching inverter are discussed in detail. RRP can constitute buck boost soft switching DC DC converter and isolated soft switching DC DC converter with the automatic limitation performance of output power. Partial series resonant DC DC converter with RRP can realize the zero voltage/zero current switching of power devices. RR... 展开更多
关键词 rugged resonant pole soft switching DC DC converter INVERTER
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Plane-Wave Least-Squares Reverse Time Migration for Rugged Topography 被引量:7
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作者 Jianping Huang Chuang Li +1 位作者 Rongrong Wang Qingyang Li 《Journal of Earth Science》 SCIE CAS CSCD 2015年第4期471-480,共10页
We present a method based on least-squares reverse time migration with plane-wave encoding (P-LSRTM) for rugged topography. Instead of modifying the wave field before migration, we modify the plane-wave encoding fun... We present a method based on least-squares reverse time migration with plane-wave encoding (P-LSRTM) for rugged topography. Instead of modifying the wave field before migration, we modify the plane-wave encoding function and fill constant velocity to the area above rugged topography in the model so that P-LSRTM can be directly performed from rugged surface in the way same to shot domain reverse time migration. In order to improve efficiency and reduce I/O (input/output) cost, the dynamic en- coding strategy and hybrid encoding strategy are implemented. Numerical test on SEG rugged topography model show that P-LSRTM can suppress migration artifacts in the migration image, and compensate am- plitude in the middle-deep part efficiently. Without data correction, P-LSRTM can produce a satisfying image of near-surface if we could get an accurate near-surface velocity model. Moreover, the pre-stack P- LSRTM is more robust than conventional RTM in the presence of migration velocity errors. 展开更多
关键词 least-squares migration rugged topography plane-wave encoding dynamic encoding hybrid encoding.
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Distributed modeling of direct solar radiation on rugged terrain of the Yellow River Basin 被引量:4
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作者 ZENG Yan QIU Xinfa +1 位作者 LIU Changming JIANG Aijun 《Journal of Geographical Sciences》 SCIE CSCD 2005年第4期439-447,共9页
Due to the influences of local topographical factors and terrain inter-shielding, calculation of direct solar radiation (DSR) quantity of rugged terrain is very complex. Based on digital elevation model (DEM) data... Due to the influences of local topographical factors and terrain inter-shielding, calculation of direct solar radiation (DSR) quantity of rugged terrain is very complex. Based on digital elevation model (DEM) data and meteorological observations, a distributed model for calculating DSR over rugged terrain is developed. This model gives an all-sided consideration on factors influencing th a resolution of 1 km × 1 km for thDSR. Using the developed model, normals of annual DSR quantity wie Yellow River Basin was generated, with DEM data as the general characterization of terrain. Characteristics of DSR quantity influenced by geographic and topographic factors over rugged terrain were analyzed thoroughly. Results suggest that: influenced by local topographic factors, i.e. azimuth, slope and so on, and annual DSR quantity over mountainous area has a clear spatial difference; annual DSR quantity of sunny slope (or southern slope) of mountains is obviously larger than that of shady slope (or northern slope). The calculated DSR quantity of the Yellow River Basin is provided in the same way as other kinds of spatial information and can be employed as basic geographic data for relevant studies as well. 展开更多
关键词 direct solar radiation (DSR) rugged terrain digital elevation model (DEM) distributed model Yellow River Basin
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Distributed Modeling of Extraterrestrial Solar Radiation Over the Rugged Terrains of Pakistan 被引量:3
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作者 Romana AMBREEN QIU Xinfa Iftikhar AHMAD 《Journal of Mountain Science》 SCIE CSCD 2011年第3期427-436,共10页
In Pakistan,the solar analogue has been addressed but its surface geographical parameterization has given least attention.Inappropriate density of stations and their spatial coverage particularly in difficult peripher... In Pakistan,the solar analogue has been addressed but its surface geographical parameterization has given least attention.Inappropriate density of stations and their spatial coverage particularly in difficult peripheral national territories,little or no solar radiation data,non-satisfactory sunshine hours data,and low quality of ground observed cloud cover data create a situation in which the spatial modeling of Extraterrestrial Solar Radiation(ESR) and its ground parameterization got sufficient scope.The Digital Elevation Model (DEM) input into Geographic Information System (GIS) is a compatible tool to demonstrate the spatial distribution of ESR over the rugged terrains of the study domain.For the first time,distributed modeling of ESR is done over the rugged terrains of Pakistan,based on DEM and ArcGIS..Results clearly depict that the complex landforms profoundly disrupt the zonal distribution of ESR in Pakistan.The screening impact of topography is higher on spatial distribution of ESR in winter and considerably low in summer.The combined effect of topography and latitude is obvious.Hence,the model was further testified by plotting Rb (ratio of ESR quantity over rugged terrain against plane surface) against azimuth at different latitudes with different angled slopes.The results clearly support the strong screening effect of rugged terrain through out the country especially in Himalayas,Karakoram and Hindukush (HKH),western border mountains and Balochistan Plateau.This model can be instrumental as baseline geospatial information for scientific investigations in Pakistan,where substantial fraction of national population is living in mountainous regions. 展开更多
关键词 Pakistan distributed modeling ESR DEM GIS rugged terrain
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RUGⅢ:一种新的支付医疗费用的慢性病例分类模式 被引量:2
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作者 张宝库 侯延武 +3 位作者 王桂玲 栾淑珍 赵瑞 卢国华 《中国卫生事业管理》 1994年第10期528-531,共4页
RUGⅢ:一种新的支付医疗费用的慢性病例分类模式中国医院管理杂志社(150036)张宝库,侯延武,王桂玲黑龙江省医院栾淑珍中国卫生信息报社赵瑞兴隆林业局第二职工医院卢国华在医疗保险和社会福利制度中,设计能合理补偿供给... RUGⅢ:一种新的支付医疗费用的慢性病例分类模式中国医院管理杂志社(150036)张宝库,侯延武,王桂玲黑龙江省医院栾淑珍中国卫生信息报社赵瑞兴隆林业局第二职工医院卢国华在医疗保险和社会福利制度中,设计能合理补偿供给医疗服务所需成本的医疗费用支付方式... 展开更多
关键词 医院改革 医疗制度 医疗费用 rug
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Core-Germplasm Construction of <i>Rosa rugosa</i>Collections by CDDP Molecular Markers 被引量:2
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作者 Liyuan Jiang Dekui Zang 《Open Journal of Applied Sciences》 2017年第11期635-645,共11页
A method for constructing core-germplasm of Rosa rugosa in China based on molecular marker data was probed and the optimum core germplasm was established. Studies were initiated to analyze the genetic diversity of 120... A method for constructing core-germplasm of Rosa rugosa in China based on molecular marker data was probed and the optimum core germplasm was established. Studies were initiated to analyze the genetic diversity of 120 rugged roses from 6 different Chinese source populations based on CDDP marker, and a preliminary construction of the core collection was established using stepwise UPGMA clustering sampling method. The 26 core collection resources of R. rugosa collections in China have 20% germplasm samples of initial collection, the retention ratio of polymorphic loci, effective number of alleles (Ne), Nei’s genetic diversity (H) and Shannon information index (I) were respectively 97.52%, 104.16%, 108.38% and 106.18%. The results of t-test showed that no significant difference was found in genetic diversity indexes between the core collection and the original collection. These results also demonstrated that the core collection could stand for original collection excellently. The results show that CDDP molecular technology can be successfully applied to the construction of core germplasm resources of rugged roses. 展开更多
关键词 rugged Rose in China CDDP Markers Genetic Diversity CORE Collection
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Application of Gaussian beam pre-stack depth migration in rugged seabed
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作者 HAN Fuxing YI Xin +3 位作者 SUN Zhangqing HU Jia XU Baoyin XU Hai 《Global Geology》 2021年第2期119-128,共10页
Strong fluctuation of seabed,abrupt variation in depth and dip of seabed bring seismic imaging problems,such as irregular reflection waves,obvious multiple waves,serious lateral wave development,poor imaging on base s... Strong fluctuation of seabed,abrupt variation in depth and dip of seabed bring seismic imaging problems,such as irregular reflection waves,obvious multiple waves,serious lateral wave development,poor imaging on base surface and depression structure,low signal-to-noise ratio of middle and deep layers.In this paper,Gaussian beam migration imaging method is used to analyze the imaging effect of rugged seabed in deep water area,and the ray tracing method of wavefront construction method is used to analyze the kinematic characteristics of seismic waves.By improving the design of seismic data acquisition and observation system,imaging quality of fine structures is improved. 展开更多
关键词 Gaussian beam migration wavefront construction method Gaussian beam pre-stack depth rugged seabed
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户外爱好者挚爱 Lacia Rugged XL移动硬盘
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《数码》 2009年第5期34-34,共1页
不管做什么都讲究专业.哪怕是移动硬盘这样的小东西。对于户外爱好者和探险家来说.拥有一款可以和JEEP媲美的移动硬盘同样重要。它必须拥有结实的外表.舒适的使用环境,超强的速度体验.能够克服任何恶劣的环境,它就是来自法国莱希L... 不管做什么都讲究专业.哪怕是移动硬盘这样的小东西。对于户外爱好者和探险家来说.拥有一款可以和JEEP媲美的移动硬盘同样重要。它必须拥有结实的外表.舒适的使用环境,超强的速度体验.能够克服任何恶劣的环境,它就是来自法国莱希Lacie的移动硬盘Rugged XL——探路者。 展开更多
关键词 移动硬盘 使用环境 Lacia rugged XL
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Stanton Rug公司推出家用系列地毯
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《纺织装饰科技》 2003年第4期27-27,共1页
在今年7月13日至16日的亚特兰大国际区域地毯展上,Stanton Rug公司介绍了一种配套家用系列区域地毯,它是长方形,阔幅的地毯,图案设计是新颖的。据国家地毯销售经理Mike Shupp讲:'我们的配套地毯产品的推出是非常成功的,它将满足各... 在今年7月13日至16日的亚特兰大国际区域地毯展上,Stanton Rug公司介绍了一种配套家用系列区域地毯,它是长方形,阔幅的地毯,图案设计是新颖的。据国家地毯销售经理Mike Shupp讲:'我们的配套地毯产品的推出是非常成功的,它将满足各种不同的需要'。 Stanton公司新设计地毯Royal Sovereign系列中包括下列几个名称的地毯: Anastasia:是100%新西兰羊毛地毯,有两种色彩:深暗蓝色及紫红色,地毯的尺寸有:5′×8′,8′×10′,10′×13′及2′6″×8′的长形地毯。 Catherine:是100%新西兰羊毛。 展开更多
关键词 Stanton rug公司 家用系列地毯 产品设计 Anastasia Catherine 产品规格
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丘陵山地甘蔗分步式机收质量及其经济效益分析 被引量:1
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作者 艾静 李宝 +7 位作者 王禹童 易湘艳 刀静梅 赵勇 李红军 杨绍聪 邓军 张跃彬 《热带作物学报》 北大核心 2026年第1期134-144,共11页
针对我国丘陵蔗区因地形破碎与窄行密植导致甘蔗收获机械化受限的产业瓶颈,本研究旨在系统解析分步式机收模式对生产效率、原料质量及蔗农收益的影响,以明确其在丘陵蔗区的应用潜力与推广策略。以云南耿马蔗区为研究区域,基于2023/2024... 针对我国丘陵蔗区因地形破碎与窄行密植导致甘蔗收获机械化受限的产业瓶颈,本研究旨在系统解析分步式机收模式对生产效率、原料质量及蔗农收益的影响,以明确其在丘陵蔗区的应用潜力与推广策略。以云南耿马蔗区为研究区域,基于2023/2024、2024/2025榨季云南耿马蔗区实例,采用多源数据融合分析(自然生长含杂质溯源试验,分步式机收含杂质溯源、成本监测),系统比较“联合机收”“传统人工”“委托加工”和“毛蔗交售”4种收获模式的经济效益。采用方差分析等统计方法,解析甘蔗生育进程与主栽品种对原料含杂率的影响机制。结果表明:经济效益上,与“传统人工”模式(蔗农净收益318.00元/t)相比,分步式机收的“委托加工”模式使蔗农净收益提升至365.00元/t,增幅达14.80%,且收获成本降低42.06%,该收益接近“联合机收”模式,且有效规避了后者对宿根蔗蔸的损伤。原料质量控制上,品种遗传差异对含杂率无显著影响,而收获时间是主导因素。随着收获期从12月推至次年4月,人工砍收下的甘蔗净蔗得率从75.76%显著提升至84.90%;而分步式机收的含杂率也从6.42%显著降至4.52%,选择在1月份之后甘蔗充分成熟的窗口期作业,可有效控制原料杂质。本研究还发现,糖厂的商业扣杂标准与田间实测含杂率存在“评价错位”,表现出显著的品种间差异,可能影响新技术的公平推广。分步式机收是适应我国丘陵山地特点,兼顾经济效益与生态可持续性的优选收获模式,其推广策略应优先聚焦于建立基于生育进程的作业时间表,而非为现有品种开发差异化的收获系统。该模式为丘陵蔗区机械化提供可量化、可推广的解决方案,对增强我国糖业竞争力与保障糖业安全具有重要实践价值和战略意义。 展开更多
关键词 甘蔗 丘陵山区 分步式机收 经济效益 商业品种
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Distributed modeling of monthly air temperatures over the rugged terrain of the Yellow River Basin 被引量:12
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作者 ZENG Yan QIU XinFa +2 位作者 HE YongJian SHI GuoPing LIU ChangMing 《Science China Earth Sciences》 SCIE EI CAS 2009年第5期694-707,共14页
Our analyses of the monthly mean air temperature of meteorological stations show that altitude, global solar radiation and surface effective radiation have a significant impact on air temperature. We set up a physical... Our analyses of the monthly mean air temperature of meteorological stations show that altitude, global solar radiation and surface effective radiation have a significant impact on air temperature. We set up a physically-based empirical model for monthly air temperature simulation. Combined the proposed model with the distributed modeling results of global solar radiation and routine meteorological observation data, we also developed a method for the distributed simulation of monthly air temperatures over rugged terrain. Spatial distribution maps are generated at a resolution of 1 km×1 km for the monthly mean, the monthly mean maximum and the monthly mean minimum air temperatures for the Yellow River Basin. Analysis shows that the simulation results reflect to a considerable extent the macro and local distribution characteristics of air temperature. Cross-validation shows that the proposed model displays good stability with mean absolute bias errors of 0.19°C–0.35°C. Tests carried out on local meteorological station data and case year data show that the model has good spatial and temporal simulation capacity. The proposed model solely uses routine meteorological data and can be applied easily to other regions. 展开更多
关键词 YELLOW RIVER BASIN MONTHLY mean air temperature rugged TERRAIN DISTRIBUTED modeling
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Modeling the land surface reflectance for optical remote sensing data in rugged terrain 被引量:12
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作者 WEN JianGuang LIU QinHuo +2 位作者 XIAO Qing LIU Qiang LI XiaoWen 《Science China Earth Sciences》 SCIE EI CAS 2008年第8期1169-1178,共10页
A model for topographic correction and land surface reflectance estimation for optical remote sensing data in rugged terrian is presented.Considering a directional-directional reflectance that is used for direct solar... A model for topographic correction and land surface reflectance estimation for optical remote sensing data in rugged terrian is presented.Considering a directional-directional reflectance that is used for direct solar irradiance correction and a hemispheric-directional reflectance that is used for atmospheric diffuse irradiance and terrain background reflected irradiance correction respectively,the directional reflectance-based model for topographic effects removing and land surface reflectance calculation is developed by deducing the directional reflectance with topographic effects and using a radiative transfer model.A canopy reflectance simulated by GOMS model and Landsat/TM raw data covering Jiangxi rugged area were taken to validate the performance of the model presented in the paper.The validation results show that the model presented here has a remarkable ability to correct topography and estimate land surface reflectance and also provides a technique method for sequently quantitative remote sensing application in terrain area. 展开更多
关键词 bidirectional reflectance topographic/atmospheric correction SKY DIFFUSE IRRADIANCE ADJACENT terrain-reflected IRRADIANCE rugged area
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关于定制加固电源的数字化检验方法探讨
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作者 杨航 施声腾 《船电技术》 2026年第2期85-88,共4页
为解决定制加固电源因型号多、接口复杂所导致的检验效率低、准确性问题,本文提出并实现了一套手工检验与数字化检验工装相结合的数字化军检方案。该方案的核心是设计两类专用工装:其一为以MCU为控制核心的固定式检测设备,集成RS422、CA... 为解决定制加固电源因型号多、接口复杂所导致的检验效率低、准确性问题,本文提出并实现了一套手工检验与数字化检验工装相结合的数字化军检方案。该方案的核心是设计两类专用工装:其一为以MCU为控制核心的固定式检测设备,集成RS422、CAN等多种通信接口与触摸屏人机界面,具备参数测量、协议解析与使能控制功能;其二为面向中大型电源箱的便携式测试工装,采用Type-C接口供电,并设计了可配置的对外辅助供电接口,提升了现场应用的适应性。应用结果表明,该方案能够有效模拟真实应用环境,通过高精度数据采集与自动化交互控制,显著提高了检验数据的准确性与校验效率,为定制加固电源的质量监督提供了高效智能的解决方案,有力推动了军检工作的专业化与系统化发展。 展开更多
关键词 数字化检验 测试工装 定制加固电源
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Estimating daily surface downward shortwave radiation over rugged terrain without bright surface at 30 m on clear-sky days using CERES data
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作者 Hui Liang Bo Jiang +3 位作者 Jianghai Peng Shaopeng Li Jiakun Han Xiuwan Yin 《International Journal of Digital Earth》 2023年第2期4317-4345,共29页
In this study,the authors propose a model,called the Daily Downward Shortwave Radiation Random Forest Model over Rugged Terrain(DSRMT),to accurately calculate the downward shortwave radiation over a terrain without br... In this study,the authors propose a model,called the Daily Downward Shortwave Radiation Random Forest Model over Rugged Terrain(DSRMT),to accurately calculate the downward shortwave radiation over a terrain without bright surface on clear days at a daily scale(DSRdaily−rugged).It was built by using the random forest method based on the comprehensive samples from CERES4_SYN1deg_Ed4A within 17 typical mountainous regions.DSRMT could directly estimate DSRdaily-rugged from the instantaneous direct and diffuse solar radiation on a flat surface during 10:30–14:30hrs on each day by comparing with the terrain factors from a digital elevation model,broadband albedo from the Global Land Surface Satellite,and ancillary information.The in-situ validation results showed that it generally delivered superior performance in estimating DSRdailyrugged at any time during 10:30–14:30hrs,especially at noon,yielding a validated root mean-squared error(RMSE)of 24.90–29.22 Wm−2 and mean absolute error(MAE)of 19.16–22.94 Wm−2,and the average weighted DSRdaily-rugged were usually more accurate with the RMSE and MAE of 21.63 and 17.14 Wm−2.Overall,DSRMT was found to deliver satisfactory performance because of its high accuracy,robustness,ease of implementation,and efficiency,so it has the strong potential to be widely used in practice. 展开更多
关键词 Daily downward shortwave radiation rugged terrain estimation modeling DSRMT CERES4 remote sensing
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QuEChERS-液相色谱串联高分辨质谱法检测果蔬中34种农药残留 被引量:3
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作者 罗景阳 周长民 +5 位作者 刘鑫 袁帅 李巧莲 李娇 张承昕 王岩松 《食品研究与开发》 2025年第13期165-176,共12页
采用QuEChERS(quick,easy,cheap,effective,rugged and safe)-液相色谱串联高分辨质谱法建立蔬菜水果样品中34种农药残留的检测方法,并建立数据库。样品提取条件为4 g无水硫酸镁、1.5 g无水乙酸钠、1 g氯化钠和10 mL乙腈(1%乙酸),净化... 采用QuEChERS(quick,easy,cheap,effective,rugged and safe)-液相色谱串联高分辨质谱法建立蔬菜水果样品中34种农药残留的检测方法,并建立数据库。样品提取条件为4 g无水硫酸镁、1.5 g无水乙酸钠、1 g氯化钠和10 mL乙腈(1%乙酸),净化剂条件为10 mg石墨化碳黑、500 mg乙二胺-N-丙基硅烷化硅胶、600 mg MgSO_(4)和200 mg C_(18),在乙腈-水流动相条件下,选择C_(18)色谱柱进行目标物分离,采用一级全扫描-触发二级全扫描模式进行检测,检测结果通过保留时间、一级精确分子质量和二级碎片进行定性,通过一级精确分子质量对样品进行定量,以韭菜、菠菜、茄子、葡萄、桃和香蕉为代表样品,采用基质匹配标准曲线法进行定量。结果表明,各农药在相应线性范围内呈现良好的线性关系,R2均大于0.99,检出限为1~5μg/kg,定量限为2~10μg/kg,回收率为70.06%~119.79%,精密度为0.23%~13.77%。该方法具有简便快速、准确度高、灵敏度好的特点,适用于蔬菜水果中34种农药的检测。 展开更多
关键词 农药残留 高分辨质谱 QuEChERS(quick EASY cheap effective rugged and safe) 水果 蔬菜
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气相色谱法测定陈皮和柑普茶中11种有机磷农药残留
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作者 黄锐南 林嘉华 +2 位作者 蒋颖佩 聂新强 林小葵 《中国卫生工程学》 2025年第6期766-768,771,共4页
目的建立陈皮、柑普茶中敌敌畏、甲拌磷、灭线磷、甲基异柳磷、氧化乐果、对硫磷、氯唑磷、毒死蜱、乐果、甲胺磷、甲基对硫磷等11种有机磷农药气相色谱检测方法。方法使用乙腈溶液超声提取样品,将提取液氮吹浓缩至近干,加入正己烷复溶... 目的建立陈皮、柑普茶中敌敌畏、甲拌磷、灭线磷、甲基异柳磷、氧化乐果、对硫磷、氯唑磷、毒死蜱、乐果、甲胺磷、甲基对硫磷等11种有机磷农药气相色谱检测方法。方法使用乙腈溶液超声提取样品,将提取液氮吹浓缩至近干,加入正己烷复溶,分散固相萃取(QuEChERS)进行净化,离心取上清液经过毛细管色谱柱进行分离,通过气相色谱-FPD检测器测定,以色谱峰出峰时间定性,峰面积定量。结果11种有机磷农药均在0.01~1.00μg/ml范围内显现线性关系,各相关系数均>0.999;定量限为0.01 mg/kg;加标回收率为77.66%~100.40%;相对标准偏差为0.92%~6.02%。结论建立的陈皮、柑普茶中11种有机磷农药气相色谱检测方法准确可靠、重现性好,为高效检测陈皮、柑普茶中相关指标提供科学的方法。 展开更多
关键词 陈皮 柑普茶 有机磷农药 分散固相萃取 气相色谱
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前处理新技术DMsPE与传统QuEChERS技术在果蔬中烟碱类农残检测应用效果比较
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作者 王丹 管益涛 +2 位作者 孙广雷 史亚萍 李勤 《中国卫生工程学》 2025年第4期444-447,451,共5页
目的比较分散微固相萃取(DMsPE)与分散固相萃取(QuEChERS)技术在烟碱类农药残留检测前处理应用的效果,从而获得更快速、简便、回收率高、最低溶剂耗损的前处理手段。方法通过对潍坊市市售蔬菜水果中3种烟碱类农药(环氧虫啶、噻虫嗪、吡... 目的比较分散微固相萃取(DMsPE)与分散固相萃取(QuEChERS)技术在烟碱类农药残留检测前处理应用的效果,从而获得更快速、简便、回收率高、最低溶剂耗损的前处理手段。方法通过对潍坊市市售蔬菜水果中3种烟碱类农药(环氧虫啶、噻虫嗪、吡虫啉)分析检测,使用DMsPE与QuEChERS前处理技术,对检测结果进行比对分析。结果实验数据显示,传统QuEChERS前处理技术和DMsPE技术在果蔬空白基质中平均加标回收率分别为74.7%~108.0%、89.6%~105.0%,RSD分别为0.29%~14.70%、0.11%~5.26%,QuEChERS技术处理后的LOD值为0.001~0.002 mg/kg,DMsPE技术下的LOD值为0.001 mg/kg。在不同果蔬种类基质中,QuEChERS技术的基质效应为0.97~1.78,DMsPE技术的基质效应为0.96~1.82。结论较传统QuEChERS技术,DMsPE有较好的回收率和重复性表现。对于不同基质,DMsPE的测定数值中基质效应有一定程度的减弱,且DMsPE前处理技术使用提取溶剂量较小,降低实验室环境负荷,方法简便易操作,可以满足精准度的实验需求,针对果蔬中烟碱类农残检测的各项指标也均符合国标要求。 展开更多
关键词 分散微固相萃取 分散固相萃取 果蔬 烟碱类 应用效果比较
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