Developing an accurate and visual sensing strategy for trace levels of fluoroquinolone residues that pose threat to food safety and human health is highly desired but remains challenging.Herein,a target selfcalibratio...Developing an accurate and visual sensing strategy for trace levels of fluoroquinolone residues that pose threat to food safety and human health is highly desired but remains challenging.Herein,a target selfcalibration ratiometric fluorescent sensing platform has been designed for sensitive visual detection of levofloxacin(LEV)based on fluorescent europium metal-organic framework(Eu-MOF)probe.Specifically,the Eu-MOF was facilely synthesized via directly mixing Eu^(3+)with 1,10-phenanthroline-2,9-dicarboxylic acid(PDA)ligand at room temperature,which exhibited well-stable red fluorescence at 612 nm.Upon the addition of target LEV,the significant fluorescence quenching from Eu^(3+)was observed owing to the inner filter effect between the Eu-MOF and LEV.While the intrinsic fluorescence for LEV at 462nm was gradually enhanced,thereby realizing the self-calibration ratiometric fluorescence responses to LEV.Through this strategy,LEV can be detected down to 27 nmol/L.Furthermore,a test paper-based Eu-MOF integrated with the smartphone assisted RGB color analysis was exploited for the quantitative monitoring of LEV through the multi-color changes from red to blue,thus achieved portable,convenient and visual detection of LEV in honey and milk samples.Therefore,the developed strategy could provide a useful tool for supporting the practical on-site test in food samples.展开更多
Fluid dynamic research on rectangular and trapezoidal fins is aimed at increasing heat transfer by means of large surfaces.The trapezoidal cavity form is compared with its thermal and flow performance,and it is reveal...Fluid dynamic research on rectangular and trapezoidal fins is aimed at increasing heat transfer by means of large surfaces.The trapezoidal cavity form is compared with its thermal and flow performance,and it is revealed that trapezoidal fins tend to be more efficient,particularly when material optimization is critical.Motivated by the increasing need for sustainable energy management,this work analyses the thermal performance of inclined trapezoidal and rectangular porous fins utilising a unique hybrid nanofluid.The effectiveness of nanoparticles in a working fluid is primarily determined by their thermophysical properties;hence,optimising these properties can significantly improve overall performance.This study considers the dispersion of Graphene Oxide(GO)and Molybdenum Disulfide in the base fluid,engine oil.Temperature profiles are analysed by altering the radiative,porosity,wet porous,and angle of inclination parameters.Surface and contour plots are constructed by using the Lobatto IIIa Collocation Method with BVP5C solver in MATLAB and Gradient Descent Optimisation to predict the combined heat transfer rate.According to the study,fluid temperature consistently decreases when the angle of inclination,wet porous parameter,porosity parameter,and radiative parameter increase,suggesting significantly improved heat dissipation.The trapezoidal fin consistently exhibits a superior heat transfer mechanism than a rectangular fin.It is found that the trapezoidal fin transmits heat at a rate that is 0.05%higher than that of the rectangular fin.Validation of the present study is done through the comparison of previous studies.This research provides useful design insights for sophisticated engineering uses,including electrical cooling devices,heat exchangers,radiators,and solar heaters.展开更多
A digital phase-locked loop （DPLL） based on a new digital phase-frequency detector is presented. The self-calibration technique is employed to acquire wide lock range,low jitter, and fast acquisition. The DPLL works...A digital phase-locked loop （DPLL） based on a new digital phase-frequency detector is presented. The self-calibration technique is employed to acquire wide lock range,low jitter, and fast acquisition. The DPLL works from 60 to 600MHz at a supply voltage of 1.8V. It also features a fraetional-N synthesizer with digital 2nd-order sigma-delta noise shaping, which can achieve a short lock time,a high frequency resolution,and an improved phase-noise spectrum. The DPLL has been implemented in SMIC 0. 18μm 1.8V 1P6M CMOS technology. The peak-to-peak jitter is less than 0. 8% of the output clock period and the lock time is less than 150 times of the reference clock period after the pre-divider.展开更多
A capacitor self-calibration circuit used in a successive approximation analog-to-digital converter （SA-ADC） is presented. This capacitor self-calibration circuit can calibrate erroneous data and work with the ADC b...A capacitor self-calibration circuit used in a successive approximation analog-to-digital converter （SA-ADC） is presented. This capacitor self-calibration circuit can calibrate erroneous data and work with the ADC by adding an additional clock period. This circuit is used in a 10 bit 32 Msample/s time-interleaved SA- ADC. The chip is implemented with Chart 0. 25 μm 2. 5 V process and totally occupies an area of 1.4 mm× 1.3 mm. After calibration, the simulated signal-to-noise ratio （SNR） is 59. 586 1 dB and the spurious-free dynamic range （SFDR） is 70. 246 dB at 32 MHz. The measured signal-to-noise and distortion ratio （SINAD） is 44. 82 dB and the SFDR is 63. 760 4 dB when the ADC samples a 5.8 MHz sinusoid wave.展开更多
Microstructured roll workpieces have been widely used as functional components in the precision industries. Current researches on quality control have focused on surface profile measurement of microstructured roll wor...Microstructured roll workpieces have been widely used as functional components in the precision industries. Current researches on quality control have focused on surface profile measurement of microstructured roll workpieces, and types of measurement systems and measurement methods have been developed. However, low measurement efficiency and low measurement accuracy caused by setting errors are the common disadvantages for surface profile measurement of microstructured roll workpieces. In order to shorten the measurement time and enhance the measurement accuracy, a method for self-calibration and compensation of setting errors is proposed for surface profile measurement of microstructured roll workpieces. A measurement system is constructed for the measurement, in which a precision spindle is employed to rotate the roll workpiece and an air-bearing displacement sensor with a micro-stylus probe is employed to scan the microstructured surface of the roll workpiece. The resolution of the displacement sensor is 0.14 nm and that of the rotary encoder of the spindle was 0.15r~. Geometrical and mathematical models are established for analyzing the influences of the setting errors of the roll workpiece and the displacement sensor with respect to the axis of the spindle, including the eccentric error of the roll workpiece, the offset error of the sensor axis and the zero point error of the sensor output. Measurement experiments are carded out on a roll workpiece on which periodic microstructures are a period of 133 i^m along the circumferential direction. Experimental results demonstrate the feasibility of the self-compensation method. The proposed method can be used to detect and compensate the setting errors without using any additional accurate artifact.展开更多
On the basis of local measurements of hydraulic conductivity, geostatistical methods have been found to be useful in heterogeneity characterization of a hydraulic conductivity field on a regional scale. However, the m...On the basis of local measurements of hydraulic conductivity, geostatistical methods have been found to be useful in heterogeneity characterization of a hydraulic conductivity field on a regional scale. However, the methods are not suited to directly integrate dynamic production data, such as, hydraulic head and solute concentration, into the study of conductivity distribution. These data, which record the flow and transport processes in the medium, are closely related to the spatial distribution of hydraulic conductivity. In this study, a three-dimensional gradient-based inverse method--the sequential self-calibration （SSC） method--is developed to calibrate a hydraulic conductivity field, initially generated by a geostatistical simulation method, conditioned on tracer test results. The SSC method can honor both local hydraulic conductivity measurements and tracer test data. The mismatch between the simulated hydraulic conductivity field and the reference true one, measured by its mean square error （MSE）, is reduced through the SSC conditional study. In comparison with the unconditional results, the SSC conditional study creates the mean breakthrough curve much closer to the reference true curve, and significantly reduces the prediction uncertainty of the solute transport in the observed locations. Further, the reduction of uncertainty is spatially dependent, which indicates that good locations, geological structure, and boundary conditions will affect the efficiency of the SSC study results.展开更多
To overcome the influence of on-orbit extreme temperature environment on the tool pose(position and orientation) accuracy of a space robot,a new self-calibration method based on a measurement camera(hand-eye vision) a...To overcome the influence of on-orbit extreme temperature environment on the tool pose(position and orientation) accuracy of a space robot,a new self-calibration method based on a measurement camera(hand-eye vision) attached to its end-effector was presented.Using the relative pose errors between the two adjacent calibration positions of the space robot,the cost function of the calibration was built,which was different from the conventional calibration method.The particle swarm optimization algorithm(PSO) was used to optimize the function to realize the geometrical parameter identification of the space robot.The above calibration method was carried out through self-calibration simulation of a six-DOF space robot whose end-effector was equipped with hand-eye vision.The results showed that after calibration there was a significant improvement of tool pose accuracy in a set of independent reference positions,which verified the feasibility of the method.At the same time,because it was unnecessary for this method to know the transformation matrix from the robot base to the calibration plate,it reduced the complexity of calibration model and shortened the error propagation chain,which benefited to improve the calibration accuracy.展开更多
In this study,the problem of bundle adjustment was revisited,and a novel algorithm based on block matrix Cholesky decomposition was proposed to solve the thorny problem of self-calibration bundle adjustment.The innova...In this study,the problem of bundle adjustment was revisited,and a novel algorithm based on block matrix Cholesky decomposition was proposed to solve the thorny problem of self-calibration bundle adjustment.The innovation points are reflected in the following aspects:①The proposed algorithm is not dependent on the Schur complement,and the calculation process is simple and clear;②The complexities of time and space tend to O(n)in the context of world point number is far greater than that of images and cameras,so the calculation magnitude and memory consumption can be reduced significantly;③The proposed algorithm can carry out self-calibration bundle adjustment in single-camera,multi-camera,and variable-camera modes;④Some measures are employed to improve the optimization effects.Experimental tests showed that the proposed algorithm has the ability to achieve state-of-the-art performance in accuracy and robustness,and it has a strong adaptability as well,because the optimized results are accurate and robust even if the initial values have large deviations from the truth.This study could provide theoretical guidance and technical support for the image-based positioning and 3D reconstruction in the fields of photogrammetry,computer vision and robotics.展开更多
A key problem that plagues camera self-calibration, namely that the classical self-calibration algorithms are very sensitive to the initial values of the camera intrinsic parameters, is analyzed and a practical soluti...A key problem that plagues camera self-calibration, namely that the classical self-calibration algorithms are very sensitive to the initial values of the camera intrinsic parameters, is analyzed and a practical solution is provided. The effect of the camera intrinsic parameters, mainly the principal point and the skew factor is first discussed. Then a practical method via a controlled motion of the camera is introduced so as to obtain an accurate estimation of these parameters. Feasibility of this approach is illustrated by carrying out comprehensive experiments using synthetic data as well as real image sequences. Unreasonable initial values can often make self-calibration impossible, yet a precise initialization guarantees a better and successful reconstruction. Trying to obtain a more reasonable initialization is worthwhile the effort in camera self-calibration.展开更多
An improved self-calibrating algorithm for visual servo based on adaptive genetic algorithm is proposed in this paper. Our approach introduces an extension of Mendonca-Cipolla and G. Chesi＇s self-calibration for the ...An improved self-calibrating algorithm for visual servo based on adaptive genetic algorithm is proposed in this paper. Our approach introduces an extension of Mendonca-Cipolla and G. Chesi＇s self-calibration for the positionbased visual servo technique which exploits the singular value property of the essential matrix. Specifically, a suitable dynamic online cost function is generated according to the property of the three singular values. The visual servo process is carried out simultaneous to the dynamic self-calibration, and then the cost function is minimized using the adaptive genetic algorithm instead of the gradient descent method in G. Chesi＇s approach. Moreover, this method overcomes the limitation that the initial parameters must be selected close to the true value, which is not constant in many cases. It is not necessary to know exactly the camera intrinsic parameters when using our approach, instead, coarse coding bounds of the five parameters are enough for the algorithm, which can be done once and for all off-line. Besides, this algorithm does not require knowledge of the 3D model of the object. Simulation experiments are carried out and the results demonstrate that the proposed approach provides a fast convergence speed and robustness against unpredictable perturbations of camera parameters, and it is an effective and efficient visual servo algorithm.展开更多
Laser tracking system （LTS） is an advanced device for large size 3D coordinates measuring with the advantages of broad range, high speed and high accuracy. However, its measuring accuracy is highly dominated by the ...Laser tracking system （LTS） is an advanced device for large size 3D coordinates measuring with the advantages of broad range, high speed and high accuracy. However, its measuring accuracy is highly dominated by the geometric errors of the tracking mirror mechanism. Proper calibration of LTS is essential prior to the use of it for metrology. A kinematics model that describes not only the motion but also the geometric variations of LTS is developed. Through error analysis of the proposed model, it is claimed that gimbals axis misalignments and tracking mirror center off-set are the key contributors to measuring errors of LTS. A self-calibration method is presented of calibrating LTS with planar constraints. Various calibration strategies utilizing single-plane and multiple-plane constraints are proposed for different situations. For each calibration strategy, issues about the error parameter estimation of LTS are exploded to find out in which conditions these parameters can be uniquely estimated. Moreover, these conditions reveal the applicability of the planar constraints to LTS self-calibration. Intensive studies have been made to check validity of the theoretical results. The results show that the measuring accuracy of LTS has increased by 5 times since this technique for calibration is used.展开更多
In the field of converting simulation surveying and traditional close range photogrammetry, it has been developed so far to survey objects by commercial digital camera and this technique is applied widely in every par...In the field of converting simulation surveying and traditional close range photogrammetry, it has been developed so far to survey objects by commercial digital camera and this technique is applied widely in every part of production. In order to get three-dimensional information of objects, commercial digital camera must be examined. For a long time, digital camera has been examined by DLT. Then there must be a high-precision control field. For realizing surveying without control points, a method for self-calibration is proposed.展开更多
Aiming at piezoresistive pressure sensors, this paper studies simulation of standard pressure by using benchmark current source and self-calibration of the sampling data characteristics. A data fusion algorithm for sa...Aiming at piezoresistive pressure sensors, this paper studies simulation of standard pressure by using benchmark current source and self-calibration of the sampling data characteristics. A data fusion algorithm for sample set is presented which transforms a surface problem into a curve fitting and interpolation problem. The simulation result shows that benchmark current source simulating pressure is successful and data fusion algorithm is effective. The maximum measurement error is only 0.098 kPa and maximum relative error is 0.92% at 0-45 kPa and -10-45~C.展开更多
Rectangular explosive charges are usually used in military or civilian explosive transportation and storage.The effects of shape parameters and detonation positions on the peak overpressure and maximum impulse of blas...Rectangular explosive charges are usually used in military or civilian explosive transportation and storage.The effects of shape parameters and detonation positions on the peak overpressure and maximum impulse of blasts lack comprehensive investigation,which is significant for the design of blast-resistant structures.In this paper,the side-length ratio of the rectangle,orientation,and detonation position of the charge are chosen as controlling parameters to investigate their influence on blast loads in the scaled distances of the gauges ranging from 0.63 to 10.54 m/kg^(1/3) with well validated 3D numerical simulations.The results show that there is a large difference in the near-field spatial distribution of the blast load of the rectangular charge;if the blast load of the rectangular charge is simply evaluated with the spherical charge,the maximum peak overpressure(maximum impulse)will be underestimated by a factor of 7.46(4.84).This must be taken seriously by blast-resistant structure designers.With the increase in the scaled distance,when the critical scaled distance is greater than 6.32(7.38)m/kg^(1/3),the influence of the charge shape on the maximum peak overpressure(maximum impulse)of the spatial blast load can be ignored.In general,the impact of detonation of the charge at the end on the maximum peak overpressure is greater compared with central detonation,but for the impact of the maximum impulse,it is necessary to pay attention to the side-length ratio of the rectangular charge and the specific detonation position on the end face.Furthermore,the structural response of steel plates placed at different azimuths under the blast load of a rectangular charge is preliminarily analyzed,and the results show that the deformation and energy of the plates are consistent with the distribution of the blast load.These analysis results provide a reference for the explosion protection design in near-field air explosions.展开更多
Determining earth pressure on jacked pipes is essential for ensuring lining safety and calculating jacking force,especially for deep-buried pipes.To better reflect the soil arching effect resulting from the excavation...Determining earth pressure on jacked pipes is essential for ensuring lining safety and calculating jacking force,especially for deep-buried pipes.To better reflect the soil arching effect resulting from the excavation of rectangular jacked pipes and the distribution of the earth pressure on jacked pipes,we present an analytical solution for predicting the vertical earth pressure on deep-buried rectangular pipe jacking tunnels,incorporating the tunnelling-induced ground loss distribution.Our proposed analytical model consists of the upper multi-layer parabolic soil arch and the lower friction arch.The key parameters(i.e.,width and height of friction arch B and height of parabolic soil arch H 1)are determined according to the existing research,and an analytical solution for K l is derived based on the distribution characteristics of the principal stress rotation angle.With consideration for the transition effect of the mechanical characteristics of the parabolic arch zone,an analytical solution for soil load transfer is derived.The prediction results of our analytical solution are compared with tests and simulation results to validate the effectiveness of the proposed analytical solution.Finally,the effects of different parameters on the soil pressure are discussed.展开更多
In this study,a self-calibrating near-infrared fluorescence probe was designed and synthesized based on the dual-fluorophore strategy utilizing methylene blue and coumarin.The probe utilized methylene blue(emission sp...In this study,a self-calibrating near-infrared fluorescence probe was designed and synthesized based on the dual-fluorophore strategy utilizing methylene blue and coumarin.The probe utilized methylene blue(emission spectrum range:640-740 nm)and coumarin fluorophore(emission spectrum range:440-600 nm)as signal output units,thereby achieving effective spectral separation and highly selective detection of HClO.Under physiological pH conditions,HClO triggers an oxidation-cleavage reaction,releasing methylene blue and coumarin,which emit distinct red and green fluorescence,respectively.This dual-emission feature enabled rapid HClO detection with two-channel detection limits of 25.13 nmol·L^(-1)(green channel)and 31.55 nmol·L^(-1)(red channel).Furthermore,in cell imaging experiments,this probe demonstrated excellent cell membrane permeability and low cytotoxicity,successfully enabling the monitoring of both endogenous and exogenous HClO in living cells.By incorporating a twochannel self-calibration system,the probe effectively mitigated signal variations caused by instrumental or environmental interference,substantially improving detection sensitivity and reliability.展开更多
This study investigates the nonlinear dynamic properties of rotating functionally graded sandwich rectangular plates in a thermal environment.The nonlinear vibration equations for a rotating metal-ceramic functionally...This study investigates the nonlinear dynamic properties of rotating functionally graded sandwich rectangular plates in a thermal environment.The nonlinear vibration equations for a rotating metal-ceramic functionally graded sandwich rectangular plate in a thermal environment are derived using classical thin plate theory and Hamilton’s principle,considering geometric nonlinearity,temperature-dependent material properties,and power law distribution of components through the thickness.With cantilever boundary conditions,the flexural nonlinear differential equations of the rectangular sandwich plate are obtained via the Galerkin method.Since the natural vibration differential equations exhibit nonlinear characteristics,the multiscale method is employed to derive the expression for nonlinear natural frequency.An example analysis reveals how the natural frequency of a functionally graded sandwich rectangular plate varies with rotational speed and temperature.Results show that the nonlinear/linear frequency ratio increases with rotational angular velocity Ω and thickness-to-length ratio h/a,follows a cosine-like periodic pattern with the setting angle,and shows a sharp decrease followed by a rapid increase with increasing width-to-length ratio b/a.The derived analytical solutions for nonlinear frequency provide valuable insights for assessing the dynamic characteristics of functionally graded structures.展开更多
The growing need for enhanced heat dissipation is compelling the development of more effective heat exchangers.Innovation inspired by nature bionics,four types of leaf-shaped pin fins were proposed and four combinatio...The growing need for enhanced heat dissipation is compelling the development of more effective heat exchangers.Innovation inspired by nature bionics,four types of leaf-shaped pin fins were proposed and four combinations of them were considered.The leaf-shaped design of the cooling pin fin enhances uniformity and synergy,effectively creating an optimized flow path that boosts cooling performance.Eight three-dimensional conjugate heat transfer models in staggered arrangement were developed using ANSYS-Fluent software.Aluminum6061material was used as the heat sinkmaterial and single-phase liquid water flowed through the rectangular channel where the Reynolds(R_(e))number varies from 40 to 100.Using the same boundary conditions as the software simulations,two leaf-shaped channels were printed to validate numerical models.Velocity field and temperature differences of the eight proposed leaf-shaped pin fins configurations were discussed by comparison with cylindrical pin fins.Based on the findings of this study,at a Reynolds number of 80,the Leaf B Staggered Array(LBSA)records a maximum temperature that is 0.72 K lower than that of the cylindrical pin fins arrangement.Additionally,the LBSA exhibits a reduction in the friction factor by approximately 33.3%relative to the circular pin fins array under the same R_(e).This implies that the design of LBSA has been optimized to provide better heat dissipation performance while maintaining lower energy consumption.Furthermore,the LBSA demonstrates the most favorable thermal-hydraulic performance index(TPI),which is 1.18 times higher than that of the circular pin fins arrangement at R_(e)=80.The temperature reduction and friction factor reduction of the lobed channel is more pronounced than that of the conventional cooling channel,highlighting its potential to increase heat transfer efficiency and reduce energy consumption in practical applications.展开更多
To investigate groundwater influence on stability and rockburst mechanism of deep hard-rock rectangular tunnels,water-immersed treatment and uniaxial compressive acoustic emission(AE)experiments were conducted on rect...To investigate groundwater influence on stability and rockburst mechanism of deep hard-rock rectangular tunnels,water-immersed treatment and uniaxial compressive acoustic emission(AE)experiments were conducted on rectangular tunnel specimens.Energy dissipation characteristics,AE evolution characteristics and damage evolution characteristics of rectangular tunnels were analysed under waterimmersed condition.Under water-immersed condition,tunnel specimens were quite sensitive to water.Average peak stress and average peak strain energy exhibited negative exponential decay with waterimmersed time.Among them,after 12 d of water immersion,average peak stress of specimens decreased by 28%.Average total strain energy decreased by 70%.Average elastic strain energy decreased by 71%and average dissipated strain energy decreased by 68%.After 62 d of water immersion,average peak stress of specimens decreased by 34%.Average total strain energy decreased by 78%.Average elastic strain energy decreased by 79%and average dissipated strain energy decreased by 75%.Water weakened bonding among mineral particles.Moreover,it undermined load-bearing capacity and diminished energystorage properties.Under high stress,massive releasable elastic strain energy stored in natural specimens within pre-peak stage may abruptly release after peak stress.This caused rapid crack development and connection in specimens.During accumulation and release of elastic strain energy,initial failure typically occurred at sidewalls.This failure location was not affected by water.Compared with natural specimens,Specimens immersed in water for 62 d had the lowest peak values of cumulative amplitude,cumulative AE energy and cumulative AE count.After 62 d of water immersion,peak values of cumulative amplitude,cumulative AE energy and cumulative AE count of specimens decreased by 84%,97%and 99%.Compared with AE damage model,fitting degree of energy damage model was higher.For natural specimens,fitting degree of energy damage model was 0.96.For specimens immersed in water for 12 d,fitting degree of energy damage model was 0.96.For specimens immersed in water for 62 d,fitting degree of energy damage model was 0.72.Therefore,an energy damage model had more remarkable applicability and reliability.By establishing dynamic mapping relationship between energy and damage in the model,accuracy of rockburst early warning has been significantly improved.This provided scientific basis for support structure design of rectangular tunnels and regulation of high strain energy.展开更多
The behavior of single-phase flow and conjugate heat transfer in micro-channel heat sinks(MCHS)subjected to auniform heat flux is investigated by means of numerical simulations.Various geometrical configurations areex...The behavior of single-phase flow and conjugate heat transfer in micro-channel heat sinks(MCHS)subjected to auniform heat flux is investigated by means of numerical simulations.Various geometrical configurations areexamined,particularly,the combinations of rectangular solid and perforated blocks,used to create a disturbancein the flow.The analysis focuses on several key aspects and related metrics,including the temperature distribution,the mean Fanning friction factor,the pressure drop,the Nusselt number,and the overall heat transfer coefficientacross a range of Reynolds numbers(80–870).It is shown that the introduction of such blocks significantlyenhances the heat transfer performances of the MCHS compared to the straight-through flow channel.Specifically,a case is found where the Nusselt number increases by 2.3 times relative to the reference case.The integrationof perforated blocks facilitates the generation of vorticity within the channel,promoting the mixing of coldand hot fluids.Notably,MCHS incorporating perforated rectangular blocks exhibit more pronounced heat transferbenefits at Reynolds numbers smaller than 400.展开更多
基金supported by the National Natural Science Foundation of China(Nos.32260247 and 22064010)the Natural Science Foundation of Jiangxi Province(Nos.20232BAB215071 and 20224BAB213009).
文摘Developing an accurate and visual sensing strategy for trace levels of fluoroquinolone residues that pose threat to food safety and human health is highly desired but remains challenging.Herein,a target selfcalibration ratiometric fluorescent sensing platform has been designed for sensitive visual detection of levofloxacin(LEV)based on fluorescent europium metal-organic framework(Eu-MOF)probe.Specifically,the Eu-MOF was facilely synthesized via directly mixing Eu^(3+)with 1,10-phenanthroline-2,9-dicarboxylic acid(PDA)ligand at room temperature,which exhibited well-stable red fluorescence at 612 nm.Upon the addition of target LEV,the significant fluorescence quenching from Eu^(3+)was observed owing to the inner filter effect between the Eu-MOF and LEV.While the intrinsic fluorescence for LEV at 462nm was gradually enhanced,thereby realizing the self-calibration ratiometric fluorescence responses to LEV.Through this strategy,LEV can be detected down to 27 nmol/L.Furthermore,a test paper-based Eu-MOF integrated with the smartphone assisted RGB color analysis was exploited for the quantitative monitoring of LEV through the multi-color changes from red to blue,thus achieved portable,convenient and visual detection of LEV in honey and milk samples.Therefore,the developed strategy could provide a useful tool for supporting the practical on-site test in food samples.
基金supported by the“Regional Innovation System&Education(RISE)”through the Seoul RISE Center,funded by the Ministry of Education(MOE)and the Seoul Metropolitan Government(2025-RISE-01-027-04).
文摘Fluid dynamic research on rectangular and trapezoidal fins is aimed at increasing heat transfer by means of large surfaces.The trapezoidal cavity form is compared with its thermal and flow performance,and it is revealed that trapezoidal fins tend to be more efficient,particularly when material optimization is critical.Motivated by the increasing need for sustainable energy management,this work analyses the thermal performance of inclined trapezoidal and rectangular porous fins utilising a unique hybrid nanofluid.The effectiveness of nanoparticles in a working fluid is primarily determined by their thermophysical properties;hence,optimising these properties can significantly improve overall performance.This study considers the dispersion of Graphene Oxide(GO)and Molybdenum Disulfide in the base fluid,engine oil.Temperature profiles are analysed by altering the radiative,porosity,wet porous,and angle of inclination parameters.Surface and contour plots are constructed by using the Lobatto IIIa Collocation Method with BVP5C solver in MATLAB and Gradient Descent Optimisation to predict the combined heat transfer rate.According to the study,fluid temperature consistently decreases when the angle of inclination,wet porous parameter,porosity parameter,and radiative parameter increase,suggesting significantly improved heat dissipation.The trapezoidal fin consistently exhibits a superior heat transfer mechanism than a rectangular fin.It is found that the trapezoidal fin transmits heat at a rate that is 0.05%higher than that of the rectangular fin.Validation of the present study is done through the comparison of previous studies.This research provides useful design insights for sophisticated engineering uses,including electrical cooling devices,heat exchangers,radiators,and solar heaters.
文摘A digital phase-locked loop （DPLL） based on a new digital phase-frequency detector is presented. The self-calibration technique is employed to acquire wide lock range,low jitter, and fast acquisition. The DPLL works from 60 to 600MHz at a supply voltage of 1.8V. It also features a fraetional-N synthesizer with digital 2nd-order sigma-delta noise shaping, which can achieve a short lock time,a high frequency resolution,and an improved phase-noise spectrum. The DPLL has been implemented in SMIC 0. 18μm 1.8V 1P6M CMOS technology. The peak-to-peak jitter is less than 0. 8% of the output clock period and the lock time is less than 150 times of the reference clock period after the pre-divider.
文摘A capacitor self-calibration circuit used in a successive approximation analog-to-digital converter （SA-ADC） is presented. This capacitor self-calibration circuit can calibrate erroneous data and work with the ADC by adding an additional clock period. This circuit is used in a 10 bit 32 Msample/s time-interleaved SA- ADC. The chip is implemented with Chart 0. 25 μm 2. 5 V process and totally occupies an area of 1.4 mm× 1.3 mm. After calibration, the simulated signal-to-noise ratio （SNR） is 59. 586 1 dB and the spurious-free dynamic range （SFDR） is 70. 246 dB at 32 MHz. The measured signal-to-noise and distortion ratio （SINAD） is 44. 82 dB and the SFDR is 63. 760 4 dB when the ADC samples a 5.8 MHz sinusoid wave.
文摘Microstructured roll workpieces have been widely used as functional components in the precision industries. Current researches on quality control have focused on surface profile measurement of microstructured roll workpieces, and types of measurement systems and measurement methods have been developed. However, low measurement efficiency and low measurement accuracy caused by setting errors are the common disadvantages for surface profile measurement of microstructured roll workpieces. In order to shorten the measurement time and enhance the measurement accuracy, a method for self-calibration and compensation of setting errors is proposed for surface profile measurement of microstructured roll workpieces. A measurement system is constructed for the measurement, in which a precision spindle is employed to rotate the roll workpiece and an air-bearing displacement sensor with a micro-stylus probe is employed to scan the microstructured surface of the roll workpiece. The resolution of the displacement sensor is 0.14 nm and that of the rotary encoder of the spindle was 0.15r~. Geometrical and mathematical models are established for analyzing the influences of the setting errors of the roll workpiece and the displacement sensor with respect to the axis of the spindle, including the eccentric error of the roll workpiece, the offset error of the sensor axis and the zero point error of the sensor output. Measurement experiments are carded out on a roll workpiece on which periodic microstructures are a period of 133 i^m along the circumferential direction. Experimental results demonstrate the feasibility of the self-compensation method. The proposed method can be used to detect and compensate the setting errors without using any additional accurate artifact.
基金This study is partially supported by the Program of Outstanding Overseas Youth Chinese Scholar,the National Natural Science Foundation of China (No. 40528003)partially supported by USA National Science Foundation.
文摘On the basis of local measurements of hydraulic conductivity, geostatistical methods have been found to be useful in heterogeneity characterization of a hydraulic conductivity field on a regional scale. However, the methods are not suited to directly integrate dynamic production data, such as, hydraulic head and solute concentration, into the study of conductivity distribution. These data, which record the flow and transport processes in the medium, are closely related to the spatial distribution of hydraulic conductivity. In this study, a three-dimensional gradient-based inverse method--the sequential self-calibration （SSC） method--is developed to calibrate a hydraulic conductivity field, initially generated by a geostatistical simulation method, conditioned on tracer test results. The SSC method can honor both local hydraulic conductivity measurements and tracer test data. The mismatch between the simulated hydraulic conductivity field and the reference true one, measured by its mean square error （MSE）, is reduced through the SSC conditional study. In comparison with the unconditional results, the SSC conditional study creates the mean breakthrough curve much closer to the reference true curve, and significantly reduces the prediction uncertainty of the solute transport in the observed locations. Further, the reduction of uncertainty is spatially dependent, which indicates that good locations, geological structure, and boundary conditions will affect the efficiency of the SSC study results.
基金Projects(60775049,60805033) supported by the National Natural Science Foundation of ChinaProject(2007AA704317) supported by the National High Technology Research and Development Program of China
文摘To overcome the influence of on-orbit extreme temperature environment on the tool pose(position and orientation) accuracy of a space robot,a new self-calibration method based on a measurement camera(hand-eye vision) attached to its end-effector was presented.Using the relative pose errors between the two adjacent calibration positions of the space robot,the cost function of the calibration was built,which was different from the conventional calibration method.The particle swarm optimization algorithm(PSO) was used to optimize the function to realize the geometrical parameter identification of the space robot.The above calibration method was carried out through self-calibration simulation of a six-DOF space robot whose end-effector was equipped with hand-eye vision.The results showed that after calibration there was a significant improvement of tool pose accuracy in a set of independent reference positions,which verified the feasibility of the method.At the same time,because it was unnecessary for this method to know the transformation matrix from the robot base to the calibration plate,it reduced the complexity of calibration model and shortened the error propagation chain,which benefited to improve the calibration accuracy.
基金National Natural Science Foundation of China(Nos.41571410,41977067,42171422)。
文摘In this study,the problem of bundle adjustment was revisited,and a novel algorithm based on block matrix Cholesky decomposition was proposed to solve the thorny problem of self-calibration bundle adjustment.The innovation points are reflected in the following aspects:①The proposed algorithm is not dependent on the Schur complement,and the calculation process is simple and clear;②The complexities of time and space tend to O(n)in the context of world point number is far greater than that of images and cameras,so the calculation magnitude and memory consumption can be reduced significantly;③The proposed algorithm can carry out self-calibration bundle adjustment in single-camera,multi-camera,and variable-camera modes;④Some measures are employed to improve the optimization effects.Experimental tests showed that the proposed algorithm has the ability to achieve state-of-the-art performance in accuracy and robustness,and it has a strong adaptability as well,because the optimized results are accurate and robust even if the initial values have large deviations from the truth.This study could provide theoretical guidance and technical support for the image-based positioning and 3D reconstruction in the fields of photogrammetry,computer vision and robotics.
文摘A key problem that plagues camera self-calibration, namely that the classical self-calibration algorithms are very sensitive to the initial values of the camera intrinsic parameters, is analyzed and a practical solution is provided. The effect of the camera intrinsic parameters, mainly the principal point and the skew factor is first discussed. Then a practical method via a controlled motion of the camera is introduced so as to obtain an accurate estimation of these parameters. Feasibility of this approach is illustrated by carrying out comprehensive experiments using synthetic data as well as real image sequences. Unreasonable initial values can often make self-calibration impossible, yet a precise initialization guarantees a better and successful reconstruction. Trying to obtain a more reasonable initialization is worthwhile the effort in camera self-calibration.
基金the National Natural Science Foundation of China (No.60675048)Science and Technology Research Project of the Ministry of Education (No.204181).
文摘An improved self-calibrating algorithm for visual servo based on adaptive genetic algorithm is proposed in this paper. Our approach introduces an extension of Mendonca-Cipolla and G. Chesi＇s self-calibration for the positionbased visual servo technique which exploits the singular value property of the essential matrix. Specifically, a suitable dynamic online cost function is generated according to the property of the three singular values. The visual servo process is carried out simultaneous to the dynamic self-calibration, and then the cost function is minimized using the adaptive genetic algorithm instead of the gradient descent method in G. Chesi＇s approach. Moreover, this method overcomes the limitation that the initial parameters must be selected close to the true value, which is not constant in many cases. It is not necessary to know exactly the camera intrinsic parameters when using our approach, instead, coarse coding bounds of the five parameters are enough for the algorithm, which can be done once and for all off-line. Besides, this algorithm does not require knowledge of the 3D model of the object. Simulation experiments are carried out and the results demonstrate that the proposed approach provides a fast convergence speed and robustness against unpredictable perturbations of camera parameters, and it is an effective and efficient visual servo algorithm.
基金National Natural Science Foundation of China (No. 50475038).
文摘Laser tracking system （LTS） is an advanced device for large size 3D coordinates measuring with the advantages of broad range, high speed and high accuracy. However, its measuring accuracy is highly dominated by the geometric errors of the tracking mirror mechanism. Proper calibration of LTS is essential prior to the use of it for metrology. A kinematics model that describes not only the motion but also the geometric variations of LTS is developed. Through error analysis of the proposed model, it is claimed that gimbals axis misalignments and tracking mirror center off-set are the key contributors to measuring errors of LTS. A self-calibration method is presented of calibrating LTS with planar constraints. Various calibration strategies utilizing single-plane and multiple-plane constraints are proposed for different situations. For each calibration strategy, issues about the error parameter estimation of LTS are exploded to find out in which conditions these parameters can be uniquely estimated. Moreover, these conditions reveal the applicability of the planar constraints to LTS self-calibration. Intensive studies have been made to check validity of the theoretical results. The results show that the measuring accuracy of LTS has increased by 5 times since this technique for calibration is used.
文摘In the field of converting simulation surveying and traditional close range photogrammetry, it has been developed so far to survey objects by commercial digital camera and this technique is applied widely in every part of production. In order to get three-dimensional information of objects, commercial digital camera must be examined. For a long time, digital camera has been examined by DLT. Then there must be a high-precision control field. For realizing surveying without control points, a method for self-calibration is proposed.
基金Project supported by the National Natural Science Foundation of China （Grant No.40265001）, and the Science Foundation of Yunnan Province （Grant No.2002C0038M）
文摘Aiming at piezoresistive pressure sensors, this paper studies simulation of standard pressure by using benchmark current source and self-calibration of the sampling data characteristics. A data fusion algorithm for sample set is presented which transforms a surface problem into a curve fitting and interpolation problem. The simulation result shows that benchmark current source simulating pressure is successful and data fusion algorithm is effective. The maximum measurement error is only 0.098 kPa and maximum relative error is 0.92% at 0-45 kPa and -10-45~C.
基金supported by the National Science Foundation of China(Grant No.14102428)the Fundamental Research Funds for the Central Universities(Grant Nos.WK2090000019 and YD2480002002)the Open Research Fund of Anhui Province Key Laboratory of Green Building and Assembly Construction,Anhui Institute of Building Research&Design(Grant No.2021-JKYL-005).
文摘Rectangular explosive charges are usually used in military or civilian explosive transportation and storage.The effects of shape parameters and detonation positions on the peak overpressure and maximum impulse of blasts lack comprehensive investigation,which is significant for the design of blast-resistant structures.In this paper,the side-length ratio of the rectangle,orientation,and detonation position of the charge are chosen as controlling parameters to investigate their influence on blast loads in the scaled distances of the gauges ranging from 0.63 to 10.54 m/kg^(1/3) with well validated 3D numerical simulations.The results show that there is a large difference in the near-field spatial distribution of the blast load of the rectangular charge;if the blast load of the rectangular charge is simply evaluated with the spherical charge,the maximum peak overpressure(maximum impulse)will be underestimated by a factor of 7.46(4.84).This must be taken seriously by blast-resistant structure designers.With the increase in the scaled distance,when the critical scaled distance is greater than 6.32(7.38)m/kg^(1/3),the influence of the charge shape on the maximum peak overpressure(maximum impulse)of the spatial blast load can be ignored.In general,the impact of detonation of the charge at the end on the maximum peak overpressure is greater compared with central detonation,but for the impact of the maximum impulse,it is necessary to pay attention to the side-length ratio of the rectangular charge and the specific detonation position on the end face.Furthermore,the structural response of steel plates placed at different azimuths under the blast load of a rectangular charge is preliminarily analyzed,and the results show that the deformation and energy of the plates are consistent with the distribution of the blast load.These analysis results provide a reference for the explosion protection design in near-field air explosions.
基金Project(2022YJS073)supported by the Fundamental Research Funds for the Central Universities,ChinaProject(2024YFE0198500)supported by the National Key Research and Development Program of China:Intergovernmental International Science and Technology Innovation CooperationProject(U2469207)supported by the National Natural Science Foundation Railway Innovation and Development Joint Fund Project,China。
文摘Determining earth pressure on jacked pipes is essential for ensuring lining safety and calculating jacking force,especially for deep-buried pipes.To better reflect the soil arching effect resulting from the excavation of rectangular jacked pipes and the distribution of the earth pressure on jacked pipes,we present an analytical solution for predicting the vertical earth pressure on deep-buried rectangular pipe jacking tunnels,incorporating the tunnelling-induced ground loss distribution.Our proposed analytical model consists of the upper multi-layer parabolic soil arch and the lower friction arch.The key parameters(i.e.,width and height of friction arch B and height of parabolic soil arch H 1)are determined according to the existing research,and an analytical solution for K l is derived based on the distribution characteristics of the principal stress rotation angle.With consideration for the transition effect of the mechanical characteristics of the parabolic arch zone,an analytical solution for soil load transfer is derived.The prediction results of our analytical solution are compared with tests and simulation results to validate the effectiveness of the proposed analytical solution.Finally,the effects of different parameters on the soil pressure are discussed.
文摘In this study,a self-calibrating near-infrared fluorescence probe was designed and synthesized based on the dual-fluorophore strategy utilizing methylene blue and coumarin.The probe utilized methylene blue(emission spectrum range:640-740 nm)and coumarin fluorophore(emission spectrum range:440-600 nm)as signal output units,thereby achieving effective spectral separation and highly selective detection of HClO.Under physiological pH conditions,HClO triggers an oxidation-cleavage reaction,releasing methylene blue and coumarin,which emit distinct red and green fluorescence,respectively.This dual-emission feature enabled rapid HClO detection with two-channel detection limits of 25.13 nmol·L^(-1)(green channel)and 31.55 nmol·L^(-1)(red channel).Furthermore,in cell imaging experiments,this probe demonstrated excellent cell membrane permeability and low cytotoxicity,successfully enabling the monitoring of both endogenous and exogenous HClO in living cells.By incorporating a twochannel self-calibration system,the probe effectively mitigated signal variations caused by instrumental or environmental interference,substantially improving detection sensitivity and reliability.
基金supported by the National Natural Science Foundation of China(No.11772090).
文摘This study investigates the nonlinear dynamic properties of rotating functionally graded sandwich rectangular plates in a thermal environment.The nonlinear vibration equations for a rotating metal-ceramic functionally graded sandwich rectangular plate in a thermal environment are derived using classical thin plate theory and Hamilton’s principle,considering geometric nonlinearity,temperature-dependent material properties,and power law distribution of components through the thickness.With cantilever boundary conditions,the flexural nonlinear differential equations of the rectangular sandwich plate are obtained via the Galerkin method.Since the natural vibration differential equations exhibit nonlinear characteristics,the multiscale method is employed to derive the expression for nonlinear natural frequency.An example analysis reveals how the natural frequency of a functionally graded sandwich rectangular plate varies with rotational speed and temperature.Results show that the nonlinear/linear frequency ratio increases with rotational angular velocity Ω and thickness-to-length ratio h/a,follows a cosine-like periodic pattern with the setting angle,and shows a sharp decrease followed by a rapid increase with increasing width-to-length ratio b/a.The derived analytical solutions for nonlinear frequency provide valuable insights for assessing the dynamic characteristics of functionally graded structures.
基金supported by the Shandong Provincial Natural Science Foundation,China(Grant ZR2024ME136).
文摘The growing need for enhanced heat dissipation is compelling the development of more effective heat exchangers.Innovation inspired by nature bionics,four types of leaf-shaped pin fins were proposed and four combinations of them were considered.The leaf-shaped design of the cooling pin fin enhances uniformity and synergy,effectively creating an optimized flow path that boosts cooling performance.Eight three-dimensional conjugate heat transfer models in staggered arrangement were developed using ANSYS-Fluent software.Aluminum6061material was used as the heat sinkmaterial and single-phase liquid water flowed through the rectangular channel where the Reynolds(R_(e))number varies from 40 to 100.Using the same boundary conditions as the software simulations,two leaf-shaped channels were printed to validate numerical models.Velocity field and temperature differences of the eight proposed leaf-shaped pin fins configurations were discussed by comparison with cylindrical pin fins.Based on the findings of this study,at a Reynolds number of 80,the Leaf B Staggered Array(LBSA)records a maximum temperature that is 0.72 K lower than that of the cylindrical pin fins arrangement.Additionally,the LBSA exhibits a reduction in the friction factor by approximately 33.3%relative to the circular pin fins array under the same R_(e).This implies that the design of LBSA has been optimized to provide better heat dissipation performance while maintaining lower energy consumption.Furthermore,the LBSA demonstrates the most favorable thermal-hydraulic performance index(TPI),which is 1.18 times higher than that of the circular pin fins arrangement at R_(e)=80.The temperature reduction and friction factor reduction of the lobed channel is more pronounced than that of the conventional cooling channel,highlighting its potential to increase heat transfer efficiency and reduce energy consumption in practical applications.
基金funded by the National Science and Technology Major Project(No.2025ZD1700904)the National Natural Science Foundation of China(Nos.52174093 and 52034009)+1 种基金Fundamental Research Funds for the Central Universities(No.2023ZKPYNY03)Fundamental Research Funds for the Central Universities(Ph.D.Top Innovative Talents Fund of CUMTB)(No.BBJ2025002)。
文摘To investigate groundwater influence on stability and rockburst mechanism of deep hard-rock rectangular tunnels,water-immersed treatment and uniaxial compressive acoustic emission(AE)experiments were conducted on rectangular tunnel specimens.Energy dissipation characteristics,AE evolution characteristics and damage evolution characteristics of rectangular tunnels were analysed under waterimmersed condition.Under water-immersed condition,tunnel specimens were quite sensitive to water.Average peak stress and average peak strain energy exhibited negative exponential decay with waterimmersed time.Among them,after 12 d of water immersion,average peak stress of specimens decreased by 28%.Average total strain energy decreased by 70%.Average elastic strain energy decreased by 71%and average dissipated strain energy decreased by 68%.After 62 d of water immersion,average peak stress of specimens decreased by 34%.Average total strain energy decreased by 78%.Average elastic strain energy decreased by 79%and average dissipated strain energy decreased by 75%.Water weakened bonding among mineral particles.Moreover,it undermined load-bearing capacity and diminished energystorage properties.Under high stress,massive releasable elastic strain energy stored in natural specimens within pre-peak stage may abruptly release after peak stress.This caused rapid crack development and connection in specimens.During accumulation and release of elastic strain energy,initial failure typically occurred at sidewalls.This failure location was not affected by water.Compared with natural specimens,Specimens immersed in water for 62 d had the lowest peak values of cumulative amplitude,cumulative AE energy and cumulative AE count.After 62 d of water immersion,peak values of cumulative amplitude,cumulative AE energy and cumulative AE count of specimens decreased by 84%,97%and 99%.Compared with AE damage model,fitting degree of energy damage model was higher.For natural specimens,fitting degree of energy damage model was 0.96.For specimens immersed in water for 12 d,fitting degree of energy damage model was 0.96.For specimens immersed in water for 62 d,fitting degree of energy damage model was 0.72.Therefore,an energy damage model had more remarkable applicability and reliability.By establishing dynamic mapping relationship between energy and damage in the model,accuracy of rockburst early warning has been significantly improved.This provided scientific basis for support structure design of rectangular tunnels and regulation of high strain energy.
基金funded by the Project of the Hubei Provincial Department of Science and Technology(Grant No.2022CFB957)the Project of Hubei Engineering University of Teaching Research(Grant No.JY2024032)+1 种基金Ministry of Education University-Industry Cooperation Collaborative Education Project(Grant No.220903584161245)College Students’Innovation and Entrepreneurship Training Program(Grant Nos.DC2024031,DC2024032).
文摘The behavior of single-phase flow and conjugate heat transfer in micro-channel heat sinks(MCHS)subjected to auniform heat flux is investigated by means of numerical simulations.Various geometrical configurations areexamined,particularly,the combinations of rectangular solid and perforated blocks,used to create a disturbancein the flow.The analysis focuses on several key aspects and related metrics,including the temperature distribution,the mean Fanning friction factor,the pressure drop,the Nusselt number,and the overall heat transfer coefficientacross a range of Reynolds numbers(80–870).It is shown that the introduction of such blocks significantlyenhances the heat transfer performances of the MCHS compared to the straight-through flow channel.Specifically,a case is found where the Nusselt number increases by 2.3 times relative to the reference case.The integrationof perforated blocks facilitates the generation of vorticity within the channel,promoting the mixing of coldand hot fluids.Notably,MCHS incorporating perforated rectangular blocks exhibit more pronounced heat transferbenefits at Reynolds numbers smaller than 400.
