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Enhanced magnetic properties in a Fe-based amorphous alloy via ultrasonic vibration rapid processing 被引量:1
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作者 Hong-Zhen Li Sajad Sohrabi +4 位作者 Xin Li Lu-Yao Li Jiang Ma Huan-Lin Peng Chao Yang 《Rare Metals》 2025年第4期2853-2860,共8页
In general,the rapid growth of α-Fe clusters is a challenge in high Fe-content Fe-based amorphous alloys,negatively affecting their physical properties.Herein,we introduce an efficient and rapid post-treatment techni... In general,the rapid growth of α-Fe clusters is a challenge in high Fe-content Fe-based amorphous alloys,negatively affecting their physical properties.Herein,we introduce an efficient and rapid post-treatment technique known as ultrasonic vibration rapid processing(UVRP),which enables the formation of high-density strong magnetic α-Fe clusters,thereby enhancing the soft magnetic properties of Fe_(78)Si(13)B_(9) amorphous alloy ribbon. 展开更多
关键词 enhancing soft magnetic properties soft magnetic properties physical propertieshereinwe Fe based amorphous alloy amorphous alloy ribbon ultrasonic vibration rapid processing uvrp which Fe clusters ultrasonic vibration rapid processing
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Damping capacity of high strength-damping aluminum alloys prepared by rapid solidification and powder metallurgy process 被引量:6
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作者 李国丛 马岳 +2 位作者 何晓磊 李伟 李沛勇 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2012年第5期1112-1117,共6页
Two kinds of high strength-damping aluminum alloys (LZ7) were fabricated by rapid solidification and powder metallurgy (RS-PM) process. One material was extruded to profile aluminum directly and the other was extr... Two kinds of high strength-damping aluminum alloys (LZ7) were fabricated by rapid solidification and powder metallurgy (RS-PM) process. One material was extruded to profile aluminum directly and the other was extruded to bar and then rolled to sheet. The damping capacity over a temperature range of 25-300 ℃was studied with damping mechanical thermal analyzer (DMTA) and the microstructures were investigated by optical microscopy (OM), scanning electron microscopy (SEM) and transmission electron microscopy (TEM). The experimental results show that the damping capacity increases with the test temperature elevating. Internal friction value of rolled sheet aluminum is up to 11.5×10^-2 and that of profile aluminum is as high as 6.0×10^-2 and 7.5×10^-2 at 300 ℃, respectively. Microstructure analysis shows the shape of precipitation phase of rolled alloy is more regular and the distribution is more homogeneous than that of profile alloy. Meanwhile, the interface between particulate and matrix of rolled sheet alloy is looser than that of profile alloy. Maybe the differences at interface can explain why damping capacity of rolled sheet alloy is higher than that of profile alloys at high temperature (above 120 ℃). 展开更多
关键词 damping capacity rapid solidification and powder metallurgy process composite materials damping mechanism
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Point-defect engineering of nanoporous CuBi_(2)O_(4) photocathode via rapid thermal processing for enhanced photoelectrochemical activity 被引量:2
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作者 Li Qu Runfa Tan +5 位作者 Arumugam Sivanantham Min Je Kang Yoo Jae Jeong Dong Hyun Seo Sungkyu Kim In Sun Cho 《Journal of Energy Chemistry》 SCIE EI CAS CSCD 2022年第8期201-209,I0007,共10页
Engineering point defects such as metal and oxygen vacancies play a crucial role in manipulating the electrical,optical,and catalytic properties of oxide semiconductors for solar water splitting.Herein,we synthesized ... Engineering point defects such as metal and oxygen vacancies play a crucial role in manipulating the electrical,optical,and catalytic properties of oxide semiconductors for solar water splitting.Herein,we synthesized nanoporous CuBi_(2)O_(4)(np-CBO)photocathodes and engineered their surface point defects via rapid thermal processing(RTP)in controlled atmospheres(O_(2),N_(2),and vacuum).We found that the O_(2)-RTP treatment of np-CBO increased the charge carrier density effectively without hampering the nanoporous morphology,which was attributed to the formation of copper vacancies(VCu).Further analyses revealed that the amounts of oxygen vacancies(Vo)and Cu^(1+)were reduced simultaneously,and the relative electrochemical active surface area increased after the O_(2)-RTP treatment.Notably,the point defects(VC_(u),Cu^(1+),and Vo)regulated np-CBO achieved a superb water-splitting photocurrent density of-1.81 m A cm^(-2) under simulated sunlight illumination,which is attributed to the enhanced charge transport and transfer properties resulting from the regulated surface point defects.Finally,the reversibility of the formation of the point defects was checked by sequential RTP treatments(O_(2)-N_(2)-O_(2)-N_(2)),demonstrating the strong dependence of photocurrent response on the RTP cycles.Conclusively,the surface point defect engineering via RTP treatment in a controlled atmosphere is a rapid and facile strategy to promote charge transport and transfer properties of photoelectrodes for efficient solar water-splitting. 展开更多
关键词 NANOPOROUS Copper bismuth oxide rapid thermal processing Copper vacancy Charge transport
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Structure and electrochemical properties of hypo-stoichiometric hydro-gen storage alloys prepared by twin-roller rapid quenching process 被引量:1
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作者 ZHOU Liu LU Dongsheng +4 位作者 LI Weishan HU Shejun CAI Yuepeng TANG Renheng XIAO Fangming 《Rare Metals》 SCIE EI CAS CSCD 2005年第4期336-340,共5页
The stoichiometric alloy MlB5.0 and the hypo-stoichiometric alloy MlB4.85 were prepared by twin-roller rapid quenching process, and their structure and electrochemical properties were studied. The results of XRD show ... The stoichiometric alloy MlB5.0 and the hypo-stoichiometric alloy MlB4.85 were prepared by twin-roller rapid quenching process, and their structure and electrochemical properties were studied. The results of XRD show that both of the alloys have a typical single-phase hexagonal CaCus-type structure. The cell volume of the hylpo-stoichiometric alloy M1B4.85 is slightly larger than that of the stoichiometric alloy M1B5.0, although its lattice constant cla is smaller. Under 2 C discharging rate, i.e. 640 mA/g, the M1B4.85 has a discharge capacity of 320 mAh/g, which is higher than that of the M1Bs.o, 312 mAh/g. Nevertheless, the capacities of the M1B4.85 and the M1Bs.o decline 24.7% and 20.2% after 400 cycles, respectively. The relationship of electrochemical performances of the alloys with their structures is discussed. 展开更多
关键词 hydrogen storage alloys STRUCTURE electrochemical properties XRD electrochemical methods stoichiometry twin-roller rapid quenching process
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Preparation and modification of VO_2 thin film on R-sapphire substrate by rapid thermal process
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作者 朱乃伟 胡明 +2 位作者 夏晓旭 韦晓莹 梁继然 《Chinese Physics B》 SCIE EI CAS CSCD 2014年第4期649-654,共6页
The VO2 thin film with high performance of metal-insulator transition (MIT) is prepared on R-sapphire substrate for the first time by magnetron sputtering with rapid thermal process (RTP). The electrical character... The VO2 thin film with high performance of metal-insulator transition (MIT) is prepared on R-sapphire substrate for the first time by magnetron sputtering with rapid thermal process (RTP). The electrical characteristic and THz transmittance of MIT in VO2 film are studied by four-point probe method and THz time domain spectrum (THz-TDS). X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS), atomic force microscopy (AFM), and search engine marketing (SEM) are employed to analyze the crystalline structure, valence state, surface morphology of the film. Results indicate that the properties of VO2 film which is oxidized from the metal vanadium film in oxygen atmosphere are improved with a follow- up RTP modification in nitrogen atmosphere. The crystallization and components of VO2 film are improved and the film becomes compact and uniform. A better phase transition performance is shown that the resistance changes nearly 3 orders of magnitude with a 2-~C hysteresis width and the THz transmittances are reduced by 64% and 60% in thermal and optical excitation respectively. 展开更多
关键词 rapid thermal process V02 thin film phase transition MODIFICATION
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High Temperature Rapid Tempering Process of SS400 Steel With Thermomechanical Simulation Tester
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作者 XING Shu-qing CHEN Zheng-zong +1 位作者 MA Yong-lin LI Hui-qin 《Journal of Iron and Steel Research International》 SCIE EI CAS CSCD 2012年第2期43-49,共7页
The effect of refined precipitations and dispersed phases on the toughness of SS400 steel was investigated by rapid tempering with thermomechanical simulation tester, and the electromagnetic induction rapid tempering ... The effect of refined precipitations and dispersed phases on the toughness of SS400 steel was investigated by rapid tempering with thermomechanical simulation tester, and the electromagnetic induction rapid tempering process was simulated. The conventional tempering and rapid tempering process were proceeded respectively, and both samples were quenched in 10~ of agitated iced brine. The tempering temperatures were designed as 560, 620 and 680℃, respectively. Rapid tempering specimens were heated at a heating rate of 20 ℃/s, and all samples of these three tempering temperatures were maintained 30, 40 and 50 s with the Gleeble1500-D tester, respectively. The impact test at --40 ℃ were carried out on a Charpy impact machine (CBD-300) with a maximum measurement range of 300 J and the microstructures were analyzed in detail using optical microscope (OM) and scanning electron microscope (SEM). The experiment results show that the upper bainite, martensite and small amount of austenite were obtained in the rapidly quenched samples. In comparison to the conventional process, the matrix microstructure was changed from the larger size and bulk ferrite to the refined banding structure, and the cementites were obviously refined and precipitated inside the grains and along the grain boundaries. The cryogenic impact test implies that the maximum values of impact toughness with holding time of 30 or 50 s are achieved at tempering temperature of 620℃. Furthermore, a favorite value of impact toughness with holding time of 40 s is available. 展开更多
关键词 SS400 steel rapid tempering process thermomechanical simulation tester PRECIPITATION cryogenic impact toughness
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Effects of processing parameters on figuration during the GMAW rapid prototyping process 被引量:7
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作者 尹玉环 胡绳荪 +1 位作者 张晓博 何滨华 《China Welding》 EI CAS 2006年第4期30-33,共4页
As a deposition technology, gas metal arc welding (GMAW) has shown new promise for rapid prototyping of metallic parts. During the process of metal forming using the arc of GMA W, low heat input and stable droplet t... As a deposition technology, gas metal arc welding (GMAW) has shown new promise for rapid prototyping of metallic parts. During the process of metal forming using the arc of GMA W, low heat input and stable droplet transition are critical to high quality figuration. The effects of various processing parameters on figuration quality were studied in the experiment of GMA W rapid prototyping using the wire of ERSO-6 , including welding voltage, wire feeding rate, welding speed and so on. The optimal parameters for ERSO-6 are obtained. Simultaneously, it is verified that the rapid prototyping parts with favorable structures and quality can be achieved under the conditions of low heat input and stable droplet transition. 展开更多
关键词 rapid prototyping gas metal arc welding processing parameters figuration
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Design of Rapid Thermal Processing for Large Diameter Wafer
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作者 YANG Hong-guan WEN Li-qun DAI Da-kang YU Biao 《Semiconductor Photonics and Technology》 CAS 2006年第4期265-269,共5页
The relationship between the arrangement of tungsten-halogen lamps and the uniformity of irradiance received by the wafer is discussed, and a sort of axial-symmetrical lamps-array is designed to guarantee that the irr... The relationship between the arrangement of tungsten-halogen lamps and the uniformity of irradiance received by the wafer is discussed, and a sort of axial-symmetrical lamps-array is designed to guarantee that the irradiation on the edge is approximately the same as the one on the center of the wafer. The magnitude of temperature on the wafer vs. the power of tungsten-halogen lamps is calculated numerically. 展开更多
关键词 rapid thermal processing rapid thermal annealing Tungsten-halogen lamp Large diameter wafer
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On-line detection system of weld-based rapid prototyping process based on structured light 被引量:2
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作者 李永哲 张广军 +1 位作者 熊俊 吴林 《China Welding》 EI CAS 2013年第1期1-5,共5页
In order to realize the closed-loop control for rapid prototyping process based on gas metal arc welding, the geometric parameters of weld beads should be detected. In this study, a vision sensor system consisting of ... In order to realize the closed-loop control for rapid prototyping process based on gas metal arc welding, the geometric parameters of weld beads should be detected. In this study, a vision sensor system consisting of a linear laser projector and a CCD camera was designed to collect images of weld beads. Then, an image processing approach which combines with a Gaassian filter and an improved gravity method was used to extract the centerline of a light stripe based on VC ++. Feature points of the centerline were identical directly by means of an image fusion algorithm. Experimental results show that image fusion is an effective approach to measure the width and height of the weld bead with high accuracy. This method can identify beads effectively in multi-pass welding and avoid designing different modes to suit all kinds of shapes. 展开更多
关键词 weld-based rapid prototyping linear structured light image processing image fusion
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Crystallization process in rapidly solidified Al-Nd-Ni amorphous alloy prepa red by melt spinning 被引量:2
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作者 肖于德 黎文献 马正青 《中国有色金属学会会刊:英文版》 CSCD 2004年第4期665-669,共5页
Rapidly solidified ribbons of Al90Nd7Ni3 metallic glasses were prepare d by using melt spinning. Crystallization process of the totally amorphous ribbo ns was investigated by differential scanning calorimetry and X-ra... Rapidly solidified ribbons of Al90Nd7Ni3 metallic glasses were prepare d by using melt spinning. Crystallization process of the totally amorphous ribbo ns was investigated by differential scanning calorimetry and X-ray diffraction analysis,under continuous heating regime. The results show that,under continuo us heating regime,the metallic glass devitrifies via two main stages: primary c rystallization,resulting in two-phase mixture of α(Al) plus residual amor phous phase,and secondary crystallization,corresponding to some inter-metalli c phases appearing,successively including Al11Nd3,Al3Ni,and some un known phases,in the Al amorphous/crystal matrix. Four peaks appear on the conti nuous heating DSC curves. Their peak temperatures are respectively 470.8,(570. 8,) (585.6,) and 731.6 K at infinitesimal heating rate,and their activation energies of the respective phase transformation are 183.0,294.7,232.5 and 269.1 kJ/mol. The values of Avrami exponent of the four reactions decrease with increasing relative transformation degree. At the earlier stage of phase trans formation,the values of n are larger than 4,and at the later stage the val ues of n become close to some value from 0.5 to 2.0. 展开更多
关键词 AI-Nd-Ni 非晶合金 快速凝固 晶化 相变 DSC
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Rapid Forming Process and Device of Small-size Booster Explosive Pellet
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作者 马贵春 张树生 +1 位作者 张景林 支海波 《Defence Technology(防务技术)》 SCIE EI CAS 2006年第3期191-193,共3页
关键词 调压器 炸药 压制过程 成型工艺 火工品
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Search condition of purification materials and their proper processing for the rapid infiltration method
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作者 Tatsuhide Hamasaki Yoko Fujikawa +1 位作者 Daisuke Yoneda Masataka Sugahara 《Chinese Journal Of Geochemistry》 EI CAS 2006年第B08期114-115,共2页
关键词 磷酸 渗透作用 纯化方法 热处理 土壤化学
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Devitrification process in rapidly solidified Al-Ni-Cu-Nd metallic glass
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作者 肖于德 黎文献 +3 位作者 D.Jacovkis N.Clavaguera M.T.Clavaguera-Mora J.Rodriguez-Viejo 《Journal of Central South University of Technology》 EI 2003年第3期163-167,共5页
In the present study, rapidly solidified ribbons of Al87 Ni7Cu3 Nd3 metallic glass was prepared by usingmelt spinning. Devitrification process of the totally amorphous ribbons was investigated by high temperature X-ra... In the present study, rapidly solidified ribbons of Al87 Ni7Cu3 Nd3 metallic glass was prepared by usingmelt spinning. Devitrification process of the totally amorphous ribbons was investigated by high temperature X-raydiffraction analysis, combining with differential scanning calorimetry, under continuous and isothermal heating re-gime. The X-ray diffraction intensity and full width at the half maximum (FWHM) were analyzed to investigate theincrease of crystallized amount and growth of α-Al crystal particles. The results show that under continuous heatingregime, the metallic glass devitrifies via two main stages: primary crystallization, resulting in two-phase mixture ofα-Al plus residual amorphous phase, and secondary crystallization, corresponding to rapid precipitation of some in-ter-metallic phases in the form of dispersion or eutectic mixture. Under isothermal heating regime, only Al crystalprecipitates from the Al-rich amorphous matrix at low temperature, and when heating at 280 ℃ only Al crystal pre-cipitates within a short time, and then Al8 Cu4 Nd forms, followed by Al3 Ni, in the residual amorphous phase. Whenheating at higher temperature or for longer time, Aln Nd3 forms, the amorphous phase disappears, and the ribbonsdevelop into polycrystalline morphologies with multiply phase mixture of a-Al, Al8 Cu4 Nd, Al3 Ni, and Al11 Nd3. 展开更多
关键词 rapid SOLIDIFICATION Al-rich AMORPHOUS alloy DEVITRIFICATION process phase TRANSFORMATION
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Rapid Tooling-Rapid Abrading Process Integratedwith Rapid Prototyping
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作者 Wulanmuqi Deng Jiati(State 863/CIMS Design Automation LaboratoryManufacturing System institute 720)(Beijing University of Aeronautics & AstronauticsBeijing 100083P.R.China) 《Computer Aided Drafting,Design and Manufacturing》 1999年第2期28-33,共6页
The paper is to outline a new process for manufacturing rapid graphite electrode. It detailsthe steps in Providing integration with Rapid Prototyping (RP) into rapid electrode abrading Process.The key to this combinat... The paper is to outline a new process for manufacturing rapid graphite electrode. It detailsthe steps in Providing integration with Rapid Prototyping (RP) into rapid electrode abrading Process.The key to this combination is the successful model or patted creating using the RP technology.Significantly reduced lead-time, shortened learns curve, lowered revision changes cost and eliminatedor reduced mold polishing are the consequent results. high quality Electrical Discharge Machining(EDM) electrodes are sometimes difficult to be manufactured rapidly and are very time-consumingby conventional methods, even using Computer Numerical Control (CNC) machines. Abradingprovides a simple way to create etuemely detailed and complex electrode to make molds in toolingmaking industries. Integration with the rapid development of the Rapid Prototyping & Manufacturing(RP&M) technology, the rapid electrode abrading process has been regarded as one of the majorbreakthrough in tooling making technology. 展开更多
关键词 rapid Tooling Abrading process Electrode Manufacturing rapid Prototyping
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基于图像处理的核电高强钢筋连接套筒内螺纹螺距快速测量方法
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作者 牛虎利 李泉金 +1 位作者 杨佳俊 张嘉钰 《机床与液压》 北大核心 2025年第13期126-131,共6页
针对传统测量方法进行核电高强钢筋连接套筒内螺纹螺距测量时存在的效率低和易损坏工件等问题,提出一种基于改进SIFT算法的内螺纹螺距图像测量方法。利用高精度图像采集设备获取内螺纹图像,并对图像进行去噪处理,以提升图像细节。通过... 针对传统测量方法进行核电高强钢筋连接套筒内螺纹螺距测量时存在的效率低和易损坏工件等问题,提出一种基于改进SIFT算法的内螺纹螺距图像测量方法。利用高精度图像采集设备获取内螺纹图像,并对图像进行去噪处理,以提升图像细节。通过形态学处理提取齿顶和齿根骨架中心线,并采用改进的SIFT算法进行两幅骨架中心线纵坐标匹配。最后,测量这两幅骨架中心线在纵坐标上的距离得到螺距。结果表明:相较于传统测量方法,基于图像处理的测量方法测得的螺距相对误差均在3%以内,测量精度满足核电建设检测要求,为提高核电建设中钢筋连接的安全性和稳定性提供了有力支持。 展开更多
关键词 图像处理 内螺纹螺距 快速测量方法 SIFT算法
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突发事件应对中“快速、从重行政处罚”的教义学分析——以《行政处罚法》第49条为中心
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作者 梅扬 余晓倩 《法治现代化研究》 2025年第4期147-161,共15页
《行政处罚法》第49条虽然赋予了行政机关在突发事件下快速、从重行政处罚的“特权”,但也为该项“特权”的行使划定了适用要件,以确保其既能够有效应对突发事件,又不过分限缩公民权利。具体而言,在适用前提上,行政机关应以应急状态在... 《行政处罚法》第49条虽然赋予了行政机关在突发事件下快速、从重行政处罚的“特权”,但也为该项“特权”的行使划定了适用要件,以确保其既能够有效应对突发事件,又不过分限缩公民权利。具体而言,在适用前提上,行政机关应以应急状态在法律层面的正式启动为判断标准,而非只要发生了重大传染病疫情等突发事件就可行使快速、从重行政处罚的“特权”。在适用对象上,行政机关只能针对违反突发事件应对措施的行为行使快速、从重行政处罚的“特权”,其中突发事件应对措施包括法定措施、普遍性行政措施、个性化行政措施三种类型。在适用目的上,行政机关行使快速、从重行政处罚的“特权”应以控制、减轻和消除突发事件引起的社会危害为限。在此前提下,快速处罚须遵循正当程序原则,从重处罚须接受过罚相当原则的制约,最终达致公私法益均衡之效果。 展开更多
关键词 突发事件 应急状态 快速行政处罚 适用要件 正当程序
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超声快速处理方法对石蜡包埋组织蛋白质、DNA及RNA的影响
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作者 李小红 罗佳娣 +1 位作者 梁青春 童中艺 《中南大学学报(医学版)》 北大核心 2025年第4期664-674,共11页
目的:石蜡包埋组织传统处理方法耗时长,而超声快速处理方法时间短,但其对组织蛋白质、DNA及RNA的影响尚未阐明。本研究拟通过苏木精-伊红(hematoxylin and eosin,HE)染色、免疫组织化学染色和分子病理检测探讨超声快速处理方法对石蜡包... 目的:石蜡包埋组织传统处理方法耗时长,而超声快速处理方法时间短,但其对组织蛋白质、DNA及RNA的影响尚未阐明。本研究拟通过苏木精-伊红(hematoxylin and eosin,HE)染色、免疫组织化学染色和分子病理检测探讨超声快速处理方法对石蜡包埋组织蛋白质、DNA及RNA的影响。方法:选取乳腺癌、结肠癌、肺癌、胃印戒细胞癌、肝癌及其他术后组织标本,使用已完成常规病理取材且诊断明确的剩余标本,每例标本取材2块,直径为1~3 mm,分为对照组(传统处理方法)和实验组(超声快速处理方法)。采用HE染色、免疫组织化学染色、DNA质量片段分析、荧光原位杂交-HER2基因检测、二代测序-EGFR、ALK基因检测、实时反转录聚合酶链反应(real-time reverse transcription PCR,real-time RT-PCR)-乳腺癌预后检测等分析超声快速处理方法对石蜡包埋组织蛋白质、DNA及RNA的影响,并与传统组织处理方法进行比较。结果:与对照组比较,实验组可以快速有效完成组织固定、脱水、透明、浸蜡过程,大幅度节约了病理诊断前处理标本需要的时间,且HE染色、免疫组织化学染色、DNA质量片段分析、荧光原位杂交-HER2基因检测、二代测序-EGFR、ALK基因检测、real-time RT-PCR-乳腺癌预后检测的结果与对照组完全一致。结论:超声快速处理方法可以快速有效缩短病理诊断前标本处理的时间,且不影响标本的DNA、RNA和蛋白质,可满足HE染色、免疫组织化学及分子病理检测。 展开更多
关键词 超声快速处理方法 苏木精-伊红染色 免疫组织化学染色 DNA质量 RNA质量 分子病理检测
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气相色谱质谱联用法分析海韵香精中醛酮酯类挥发性成分 被引量:1
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作者 王云龙 罗佳兴 +6 位作者 刘茜 张晓平 邹琳 武云杰 杨龙彦 付博 李坚 《化学与生物工程》 北大核心 2025年第4期51-57,63,共8页
为向食用香精稳定性检测提供品控支持,以海韵香精为研究对象,对其挥发性成分进行萃取,通过单因素实验和正交实验对萃取工艺进行了优化,建立了同时测定海韵香精中21种醛酮酯类挥发性成分的气相色谱质谱联用外标定量法。结果表明,海韵香... 为向食用香精稳定性检测提供品控支持,以海韵香精为研究对象,对其挥发性成分进行萃取,通过单因素实验和正交实验对萃取工艺进行了优化,建立了同时测定海韵香精中21种醛酮酯类挥发性成分的气相色谱质谱联用外标定量法。结果表明,海韵香精挥发性成分的最优萃取工艺为:萃取温度35℃、萃取时间6 min、料液比1∶4(g∶mL),从中共鉴定出45种挥发性物质,其中醛酮酯类有21种,占总含量的88.7%;21种醛酮酯类挥发性物质的检出限在0.042~0.272 mg·L^(-1)之间,定量限在0.140~0.907 mg·L^(-1)之间,加标回收率在90.19%~109.57%之间,精密度在1.24%~4.99%之间。该检测方法分析速度快、操作简便、结果准确、重复性好,可为食用香精中挥发性成分的检测提供理论支撑。 展开更多
关键词 气相色谱质谱联用 香精 工艺优化 快速检测
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工艺技术参数对平面流铸成型影响的研究进展
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作者 涂杨 张宁 孟利 《电工钢》 2025年第5期14-21,共8页
平面流铸是一种快速凝固成型技术,因其具有近终形连续生产金属薄带或丝材的能力,受到学术界和工业界的广泛关注。平面流铸工艺技术参数对带/丝成材的成型性与稳定性至关重要。本文总结了各工艺技术参数,包括铜辊的转速、熔液的压力差、... 平面流铸是一种快速凝固成型技术,因其具有近终形连续生产金属薄带或丝材的能力,受到学术界和工业界的广泛关注。平面流铸工艺技术参数对带/丝成材的成型性与稳定性至关重要。本文总结了各工艺技术参数,包括铜辊的转速、熔液的压力差、喷嘴与铜辊的间隙、喷嘴槽宽、过冷度、凝固速度、冷却速率与传热系数等对带材成型性的影响。同时对平面流铸工艺技术的未来发展进行了展望,采用深度学习中的神经网络算法进一步量化各技术参数影响作用,以及将平面流铸技术应用于晶体带材的工业化生产是其重要的发展方向。 展开更多
关键词 平面流铸 快速凝固 技术参数 带材成型 晶粒组织
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高温合金精密铸造工艺快速仿真平台与应用
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作者 曹仁臣 郭钊 +5 位作者 丁正一 吴文云 黄震 包超君 秦蓉 汪东红 《特种铸造及有色合金》 北大核心 2025年第1期29-34,共6页
针对精密铸造数值模拟中存在工艺参数操作繁琐、仿真效率低、系统性总结匮乏的问题,构建了基于浇注面定位技术和自动化仿真流程技术的高温合金精密铸造工艺快速仿真平台。该平台集成了从CAD设计到CAE仿真的过程,融合了浇注系统参数化、... 针对精密铸造数值模拟中存在工艺参数操作繁琐、仿真效率低、系统性总结匮乏的问题,构建了基于浇注面定位技术和自动化仿真流程技术的高温合金精密铸造工艺快速仿真平台。该平台集成了从CAD设计到CAE仿真的过程,融合了浇注系统参数化、铸造工艺参数设计、仿真结果动态显示和仿真报告下载等功能,建立了10类仿真模版和237套模型库,实现了自动化快速仿真。以某动力涡轮机匣为例,利用该平台构建仿真模型、参数设计变量和结果预测优化指标进行仿真计算。模拟结果与实际生产一致,仿真效率大幅提高。 展开更多
关键词 精密铸造 铸造工艺快速仿真 模版库
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