In this study,the characteristics and solidification behavior of Ti-48Al-3Nb-1.5Ta powder produced by supreme-speed plasma rotating electrode process(SS-PREP®)were investigated.The microstructure,phase and charac...In this study,the characteristics and solidification behavior of Ti-48Al-3Nb-1.5Ta powder produced by supreme-speed plasma rotating electrode process(SS-PREP®)were investigated.The microstructure,phase and characteristics were analyzed by scanning electron microscopy,X-ray diffraction and other methods.The atomization mechanism is direct drop formation.The relationship between the particle size and cooling rate is vc=3.14×10^(-7)·d^(-2)+1.18×10^(-2)·d^(3/2),and the relationship between secondary dendrite arm space and the particle size isλ=0.028d+0.11,as well as the relationship between SDAS and cooling rate isλ=4.84×10^(-5)·T^(-1.43).With increase in particle size,the surface structure gradually changes from the featureless smooth structure to dendritic and cellular dendritic morphology,and the flow ability becomes better.The carbides mainly exist within 5 nm of the surface and the oxidation layer is about 20 nm thick.Ti-48Al-3Nb-1.5Ta powder was mainly composed ofα2 phase andγphase.With increase in particle size,the content ofγphase increases,and the hardness decreases accordingly.The 106–250μm particles are composed of multiple grains with the grain size of 70–80μm.The microstructure,phase composition and hardness of different TiAl powders with the same size are similar,but the elastic modulus is different.展开更多
In counter-rotating electrochemical machining （CRECM）, a revolving cathode tool with hollow windows of various shapes is used to fabricate convex structures on a revolving part. During this process, the anode workpi...In counter-rotating electrochemical machining （CRECM）, a revolving cathode tool with hollow windows of various shapes is used to fabricate convex structures on a revolving part. During this process, the anode workpiece and the cathode tool rotate relative to each other at the same rotation speed. In contrast to the conventional schemes of ECM machining with linear motion of a block tool electrode, this scheme of ECM is unique, and has not been adequately studied yet. In this paper, the finite element method （FEM） is used to simulate the anode shaping process during CRECM, and the simulation process which involves a meshing model, a moving boundary, and a simulation algorithm is described. The simulated anode profiles of the convex structure at different processing times show that the CRECM process can be used to fabricate convex structures of various shapes with different heights. Besides, the variation of the inter-electrode gap indicates that this process can also reach a relative equilibrium state like that in conventional ECM. A rectangular convex and a circular convex are successfully fabricated on revolving parts. The experimental results indicate relatively good agreement with the simulation results. The proposed simulation process is valid for convex shaping prediction and feasibility studies as well.展开更多
In order to investigate the influence of processing parameters on the granularity distribution of superalloy powders during the atomization of plasma rotating electrode processing (PREP), in this paper FGH95 superallo...In order to investigate the influence of processing parameters on the granularity distribution of superalloy powders during the atomization of plasma rotating electrode processing (PREP), in this paper FGH95 superalloy powders is prepared under different processing conditions by PREP and the influence of PREP processing parameters on the granularity distribution of FGH95 superalloy powders is discussed based on fractal geometry theory. The results show that with the increase of rotating velocity of the self-consuming electrode, the fractal dimension of the granularity distribution increases linearly, which results in the increase of the proportion of smaller powders. The change of interval between plasma gun and the self-consuming electrode has a little effect on the granularity distribution, also the fractal dimension of the granularity distribution changed a little correspondingly.展开更多
In order to understand the relation between microstructure of superalloypowders and its solidification progress, the processing parameters are optimized during plasmarotating electrode processing (PREP). It was predic...In order to understand the relation between microstructure of superalloypowders and its solidification progress, the processing parameters are optimized during plasmarotating electrode processing (PREP). It was predicted from the results that the droplet velocities,droplet temperature, and fractional solidification with flight time about FGH95 superalloy droplethave been carried out based on Newtonian heat transfer formulation coupled with the classicalheterogeneous nucleation and the specific solidification process. It has been found that the dropletdynamic and thermal behavior is strongly affected by the distribution of droplet diameters, theproportion of cooling atmosphere, but is relatively unaffected by the droplet superheat.展开更多
The surface microstructure and the surface segregation of FGH 95 nickel-basedsuperalloy powders prepared through plasma rotating electrode processing (PREP) have beeninvestigated by using SEM and AES. The results indi...The surface microstructure and the surface segregation of FGH 95 nickel-basedsuperalloy powders prepared through plasma rotating electrode processing (PREP) have beeninvestigated by using SEM and AES. The results indicate that the surface microstructure of powderschanges from dendrite into cellular stricture as the particle size of powders decrease, and thepredominant precipitates solidified on the particle surfaces were identified as MC' type carbidesenriched with Nb and Ti. It was also indicated that along with the depth of particle surfaces, thesegregation layer of S, C and O elements are thick, and that of Ti, Cr elements are thin for largesire powders while they are in reverse for median size particles.展开更多
基金financially supported by the Key R&D Program of Shaanxi(Program No.2022GY-388).
文摘In this study,the characteristics and solidification behavior of Ti-48Al-3Nb-1.5Ta powder produced by supreme-speed plasma rotating electrode process(SS-PREP®)were investigated.The microstructure,phase and characteristics were analyzed by scanning electron microscopy,X-ray diffraction and other methods.The atomization mechanism is direct drop formation.The relationship between the particle size and cooling rate is vc=3.14×10^(-7)·d^(-2)+1.18×10^(-2)·d^(3/2),and the relationship between secondary dendrite arm space and the particle size isλ=0.028d+0.11,as well as the relationship between SDAS and cooling rate isλ=4.84×10^(-5)·T^(-1.43).With increase in particle size,the surface structure gradually changes from the featureless smooth structure to dendritic and cellular dendritic morphology,and the flow ability becomes better.The carbides mainly exist within 5 nm of the surface and the oxidation layer is about 20 nm thick.Ti-48Al-3Nb-1.5Ta powder was mainly composed ofα2 phase andγphase.With increase in particle size,the content ofγphase increases,and the hardness decreases accordingly.The 106–250μm particles are composed of multiple grains with the grain size of 70–80μm.The microstructure,phase composition and hardness of different TiAl powders with the same size are similar,but the elastic modulus is different.
基金supported by the Program for New Century Excellent Talents in University of China(NCET-10-0074)
文摘In counter-rotating electrochemical machining （CRECM）, a revolving cathode tool with hollow windows of various shapes is used to fabricate convex structures on a revolving part. During this process, the anode workpiece and the cathode tool rotate relative to each other at the same rotation speed. In contrast to the conventional schemes of ECM machining with linear motion of a block tool electrode, this scheme of ECM is unique, and has not been adequately studied yet. In this paper, the finite element method （FEM） is used to simulate the anode shaping process during CRECM, and the simulation process which involves a meshing model, a moving boundary, and a simulation algorithm is described. The simulated anode profiles of the convex structure at different processing times show that the CRECM process can be used to fabricate convex structures of various shapes with different heights. Besides, the variation of the inter-electrode gap indicates that this process can also reach a relative equilibrium state like that in conventional ECM. A rectangular convex and a circular convex are successfully fabricated on revolving parts. The experimental results indicate relatively good agreement with the simulation results. The proposed simulation process is valid for convex shaping prediction and feasibility studies as well.
文摘In order to investigate the influence of processing parameters on the granularity distribution of superalloy powders during the atomization of plasma rotating electrode processing (PREP), in this paper FGH95 superalloy powders is prepared under different processing conditions by PREP and the influence of PREP processing parameters on the granularity distribution of FGH95 superalloy powders is discussed based on fractal geometry theory. The results show that with the increase of rotating velocity of the self-consuming electrode, the fractal dimension of the granularity distribution increases linearly, which results in the increase of the proportion of smaller powders. The change of interval between plasma gun and the self-consuming electrode has a little effect on the granularity distribution, also the fractal dimension of the granularity distribution changed a little correspondingly.
基金This work was financially supported by National Defence Committee of Science and Technolgy (No. 95-YJ-20)
文摘In order to understand the relation between microstructure of superalloypowders and its solidification progress, the processing parameters are optimized during plasmarotating electrode processing (PREP). It was predicted from the results that the droplet velocities,droplet temperature, and fractional solidification with flight time about FGH95 superalloy droplethave been carried out based on Newtonian heat transfer formulation coupled with the classicalheterogeneous nucleation and the specific solidification process. It has been found that the dropletdynamic and thermal behavior is strongly affected by the distribution of droplet diameters, theproportion of cooling atmosphere, but is relatively unaffected by the droplet superheat.
基金This work is financially supported by The National Defence Committee of ChineseTechnology(No.95-YJ-20)
文摘The surface microstructure and the surface segregation of FGH 95 nickel-basedsuperalloy powders prepared through plasma rotating electrode processing (PREP) have beeninvestigated by using SEM and AES. The results indicate that the surface microstructure of powderschanges from dendrite into cellular stricture as the particle size of powders decrease, and thepredominant precipitates solidified on the particle surfaces were identified as MC' type carbidesenriched with Nb and Ti. It was also indicated that along with the depth of particle surfaces, thesegregation layer of S, C and O elements are thick, and that of Ti, Cr elements are thin for largesire powders while they are in reverse for median size particles.
