Mg–3Nd–0.2Zn–0.4Zr(NZ30K,wt.%)alloy is a new kind of high-performance metallic biomaterial.The combination of the NZ30K Magnesium(Mg)alloy and selective laser melting(SLM)process seems to be an ideal solution to pr...Mg–3Nd–0.2Zn–0.4Zr(NZ30K,wt.%)alloy is a new kind of high-performance metallic biomaterial.The combination of the NZ30K Magnesium(Mg)alloy and selective laser melting(SLM)process seems to be an ideal solution to produce porous Mg degradable implants.However,the microstructure evolution and mechanical properties of the SLMed NZ30K Mg alloy were not yet studied systematically.Therefore,the fabrication defects,microstructure,and mechanical properties of the SLMed NZ30K alloy under different processing parameters were investigated.The results show that there are two types of fabrication defects in the SLMed NZ30K alloy,gas pores and unfused defects.With the increase of the laser energy density,the porosity sharply decreases to the minimum first and then slightly increases.The minimum porosity is 0.49±0.18%.While the microstructure varies from the large grains with lamellar structure inside under low laser energy density,to the large grains with lamellar structure inside&the equiaxed grains&the columnar grains under middle laser energy density,and further to the fine equiaxed grains&the columnar grains under high laser energy density.The lamellar structure in the large grain is a newly observed microstructure for the NZ30K Mg alloy.Higher laser energy density leads to finer grains,which enhance all the yield strength(YS),ultimate tensile strength(UTS)and elongation,and the best comprehensive mechanical properties obtained are YS of 266±2.1 MPa,UTS of 296±5.2 MPa,with an elongation of 4.9±0.68%.The SLMed NZ30K Mg alloy with a bimodal-grained structure consisting of fine equiaxed grains and coarser columnar grains has better elongation and a yield drop phenomenon.展开更多
The relationships between the selective laser melting(SLM)processing parameters including laser power,scanning speed and hatch space,the relative density,the microstructure,and resulting mechanical properties of Ti-6A...The relationships between the selective laser melting(SLM)processing parameters including laser power,scanning speed and hatch space,the relative density,the microstructure,and resulting mechanical properties of Ti-6Al-2Zr-1Mo-1V alloy were investigated in this work.The result shows that laser power acts a dominant role in determining the relative density in comparison with scanning speed and hatch space.The optimal SLM process window for fabricating relative density>99%samples is located in the energy density range of 34.72 J·mm^(-3)to 52.08 J·mm^(-3),where the laser power range is between 125 W and 175 W.An upward trend is found in the micro-hardness as the energy density is increased.The optimum SLM processing parameters of Ti-6Al-2Zr-1Mo-1V alloy are:laser power of 150 W,scanning speed of 1,600 mm·s^(-1),hatch space of 0.08 mm,and layer thickness of 0.03 mm.The highest ultimate tensile strength,yield strength,and ductility under the optimum processing parameter are achieved,which are 1,205 MPa,1,099 MPa,and 8%,respectively.The results of this study can be used to guide SLM production Ti-6Al-2Zr-1Mo-1V alloy parts.展开更多
The influence of processing parameters on the coating surface roughness of LD10 aluminum alloy treated by the power source with positive and negative pulse in the alkaline electrolyte was discussed.Lots of experiments...The influence of processing parameters on the coating surface roughness of LD10 aluminum alloy treated by the power source with positive and negative pulse in the alkaline electrolyte was discussed.Lots of experiments were done with different processing parameters including the positive final voltage,the negative final voltage,the frequency,the duty ratio,the processing time and electrolyte temperature.And the surface roughness tester TR200 was used to measure the coating surface roughness.The influence of the processing time on the surface roughness is the smallest,less than 0.2μm.The surface roughness decreases gradually with the duty ratio decreasing or the frequency increasing;it decreases gradually with each of the other parameters increasing,and then increases gradually after achieving the minimum value.Appropriately by selecting processing parameters,the coating with Ra 0.6 can be obtained.展开更多
Laser additive manufacturing(LAM)of titanium(Ti)alloys has emerged as a transformative technology with vast potential across multiple industries.To recap the state of the art,Ti alloys processed by two essential LAM t...Laser additive manufacturing(LAM)of titanium(Ti)alloys has emerged as a transformative technology with vast potential across multiple industries.To recap the state of the art,Ti alloys processed by two essential LAM techniques(i.e.,laser powder bed fusion and laser-directed energy deposition)will be reviewed,covering the aspects of processes,materials and post-processing.The impacts of process parameters and strategies for optimizing parameters will be elucidated.Various types of Ti alloys processed by LAM,includingα-Ti,(α+β)-Ti,andβ-Ti alloys,will be overviewed in terms of micro structures and benchmarking properties.Furthermore,the post-processing methods for improving the performance of L AM-processed Ti alloys,including conventional and novel heat treatment,hot isostatic pressing,and surface processing(e.g.,ultrasonic and laser shot peening),will be systematically reviewed and discussed.The review summarizes the process windows,properties,and performance envelopes and benchmarks the research achievements in LAM of Ti alloys.The outlooks of further trends in LAM of Ti alloys are also highlighted at the end of the review.This comprehensive review could serve as a valuable resource for researchers and practitioners,promoting further advancements in LAM-built Ti alloys and their applications.展开更多
Austenitic stainless steel(ASS)is a common material used in high-pressure hydrogen systems.Prolonged exposure to high-pressure hydrogen can cause hydrogen embrittlement(HE),raising significant safety concerns.Selectiv...Austenitic stainless steel(ASS)is a common material used in high-pressure hydrogen systems.Prolonged exposure to high-pressure hydrogen can cause hydrogen embrittlement(HE),raising significant safety concerns.Selective Laser Melting(SLM),known for its high precision,is a promising additive manufacturing technology that has been widely adopted across various industries.Studies have reported that under certain SLM manufacturing conditions and process parameters,the HE resistance of SLM ASS is significantly better than that of conventionally manufactured(CM)ASS,showing great potential for application in high-pressure hydrogen systems.Thus,studying the HE of SLM ASS is crucial for further improving the safety of high-pressure hydrogen systems.This paper provides an overview of the SLM process,reviews the mechanisms of HE and their synergistic effects,and analyzes the HE characteristics of SLM ASS.Additionally,it examines the influence of unique microstructures and SLM process variables on HE of SLM ASS and offers recommendations for future research to enhance the safety of high-pressure hydrogen systems.展开更多
To overcome the shortage of complex equipment,large volume,and high energy consumption in space capsule manufacturing,a novel sliding pressure Joule heat fuse additive manufacturing technique with reduced volume and l...To overcome the shortage of complex equipment,large volume,and high energy consumption in space capsule manufacturing,a novel sliding pressure Joule heat fuse additive manufacturing technique with reduced volume and low energy consumption was proposed.But the unreasonable process parameters may lead to the inferior consistency of the forming quality of single-channel multilayer in Joule heat additive manufacturing process,and it is difficult to reach the condition for forming thinwalled parts.Orthogonal experiments were designed to fabricate single-channel multilayer samples with varying numbers of layers,and their forming quality was evaluated.The influence of printing current,forming speed,and contact pressure on the forming quality of the single-channel multilayer was analyzed.The optimal process parameters were obtained and the quality characterization of the experiment results was conducted.Results show that the printing current has the most significant influence on the forming quality of the single-channel multilayer.Under the optimal process parameters,the forming section is well fused and the surface is continuously smooth.The surface roughness of a single-channel 3-layer sample is 0.16μm,and the average Vickers hardness of cross section fusion zone is 317 HV,which lays a foundation for the subsequent use of Joule heat additive manufacturing technique to form thinwall parts.展开更多
Transpiration cooling is crucial for the performance of aerospace engine components,relying heavily on the processing quality and accuracy of microchannels.Laser powder bed fusion(LPBF)offers the potential for integra...Transpiration cooling is crucial for the performance of aerospace engine components,relying heavily on the processing quality and accuracy of microchannels.Laser powder bed fusion(LPBF)offers the potential for integrated manufacturing of complex parts and precise microchannel fabrication,essential for engine cooling applications.However,optimizing LPBF’s extensive process parameters to control processing quality and microchannel accuracy effectively remains a significant challenge,especially given the time-consuming and labor-intensive nature of handling numerous variables and the need for thorough data analysis and correlation discovery.This study introduced a combined methodology of high-throughput experiments and Gaussian process algorithms to optimize the processing quality and accuracy of nickel-based high-temperature alloy with microchannel structures.250 parameter combinations,including laser power,scanning speed,channel diameter,and spot compensation,were designed across ten high-throughput specimens.This setup allowed for rapid and efficient evaluation of processing quality and microchannel accuracy.Employing Bayesian optimization,the Gaussian process model accurately predicted processing outcomes over a broad parameter range.The correlation between various processing parameters,processing quality and accuracy was revealed,and various optimized process combinations were summarized.Verification through computed Tomography testing of the specimens confirmed the effectiveness and precision of this approach.The approach introduced in this research provides a way for quickly and efficiently optimizing the process parameters and establishing process-property relationships for LPBF,which has broad application value.展开更多
Specialized vanadium(V)-iron(Fe)-based alloy additives utilized in the production of V-containing steels were investigated.Vanadium slag from the Panzhihua region of China was utilized as a raw material to optimize pr...Specialized vanadium(V)-iron(Fe)-based alloy additives utilized in the production of V-containing steels were investigated.Vanadium slag from the Panzhihua region of China was utilized as a raw material to optimize process parameters for the preparation of V-Fe-based alloy via silicon thermal reduction.Experiments were conducted to investigate the effects of reduction temperature,holding time,and slag composition on alloy-slag separation,alloy microstructure,and the oxide content of residual slag,with an emphasis on the recovery of valuable metal elements.The results indicated that the optimal process conditions for silicon thermal reduction were achieved at reduction temperature of 1823 K,holding time of 240 min,and slag composition of 45 wt.%SiO_(2),40 wt.%CaO,and 15 wt.%Al_(2)O_(3).The resulting V-Fe-based alloy predominantly consisted of Fe-based phases such as Fe,titanium(Ti),silicon(Si)and manganese(Mn),with Si,V,as well as chromium(Cr)concentrated in the intercrystalline phase of the Fe-based alloy.The recoveries of Fe,Mn,Cr,V,and Ti under the optimal conditions were 96.30%,91.96%,86.53%,80.29%,and 74.82%,respectively.The key components of the V-Fe-based alloy obtained were 41.96 wt.%Si,27.55 wt.%Fe,12.13 wt.%Mn,5.53 wt.%V,4.86 wt.%Cr,and 3.74 wt.%Ti,thereby enabling the comprehensive recovery of the valuable metal from vanadium slag.展开更多
Silicone material extrusion(MEX)is widely used for processing liquids and pastes.Owing to the uneven linewidth and elastic extrusion deformation caused by material accumulation,products may exhibit geometric errors an...Silicone material extrusion(MEX)is widely used for processing liquids and pastes.Owing to the uneven linewidth and elastic extrusion deformation caused by material accumulation,products may exhibit geometric errors and performance defects,leading to a decline in product quality and affecting its service life.This study proposes a process parameter optimization method that considers the mechanical properties of printed specimens and production costs.To improve the quality of silicone printing samples and reduce production costs,three machine learning models,kernel extreme learning machine(KELM),support vector regression(SVR),and random forest(RF),were developed to predict these three factors.Training data were obtained through a complete factorial experiment.A new dataset is obtained using the Euclidean distance method,which assigns the elimination factor.It is trained with Bayesian optimization algorithms for parameter optimization,the new dataset is input into the improved double Gaussian extreme learning machine,and finally obtains the improved KELM model.The results showed improved prediction accuracy over SVR and RF.Furthermore,a multi-objective optimization framework was proposed by combining genetic algorithm technology with the improved KELM model.The effectiveness and reasonableness of the model algorithm were verified by comparing the optimized results with the experimental results.展开更多
A series of tests were carried microstructures of 2124 aluminum alloy in increase of aging time, temperature and low-to-peak-to-low manner. No significant out to investigate the effects of process parameters on mechan...A series of tests were carried microstructures of 2124 aluminum alloy in increase of aging time, temperature and low-to-peak-to-low manner. No significant out to investigate the effects of process parameters on mechanical properties and creep aging process. The results show that creep strain and creep rate increase with the applied stress. The hardness of specimen varies with aging time and stress in a effect of temperature on hardness of material is seen in the range of 185-195 ℃. The optimum mechanical properties are obtained at the conditions of （200 MPa, 185 ℃, 8 h） as the result of the coexistence of strengthening S＂ and S＇ phases in the matrix by transmission electron microscopy （TEM）. TEM observation shows that applied stress promotes the formation and growth of precioitates and no obvious stress orientation effect is observed in the matrix.展开更多
To study the influence of roll casting process parameters on temperature and thermal-stress fields for the AZ31 magnesium alloy sheets,three-dimensional geometric and 3D finite element models for roll casting were est...To study the influence of roll casting process parameters on temperature and thermal-stress fields for the AZ31 magnesium alloy sheets,three-dimensional geometric and 3D finite element models for roll casting were established based on the symmetry of roll casting by ANSYS software.Meshing method and smart-sizing algorithm were used to divide finite element mesh in ANSYS software.A series of researches on the temperature and stress distributions during solidification process with different process parameters were done by 3D finite element method.The temperatures of both the liquid-solid two-phase zone and liquid phase zone were elevated with increasing pouring temperature.With the heat transfer coefficient increasing,the two-phase region for liquid-solid becomes smaller.With the pouring temperature increasing and the increase of casting speed,the length of two-phase zone rises.The optimized of process parameters（casting speed 2 m/min,pouring temperature 640 ℃ and heat transfer coefficient 15 kW/（m2·℃） with the water pouring at roller exit was used to produce magnesium alloy AZ31 sheet,and equiaxed grains with the average grain size of 50 μm were achieved after roll casting.The simulation results give better understanding of the temperature variation in phase transformation zone and the formation mechanism of hot cracks in plates during roll casting and help to design the optimized process parameters of roll casting for Mg alloy.展开更多
A modified version of the NCAR/RegCM2 has been developed at the National Climate Center （NCC）, China Meteorological Administration, through a series of sensitivity experiments and multi-year simulations and hindcast...A modified version of the NCAR/RegCM2 has been developed at the National Climate Center （NCC）, China Meteorological Administration, through a series of sensitivity experiments and multi-year simulations and hindcasts, with a special emphasis on the adequate choice of physical parameterization schemes suitable for the East Asian monsoon climate. This regional climate model is nested with the NCC/IAP （Institute of Atmospheric Physics） T63 coupled GCM to make an experimental seasonal prediction for China and East Asia. The four-year （2001 to 2004） prediction results are encouraging. This paper is the first part of a two-part paper, and it mainly describes the sensitivity study of the physical process paraxneterization represented in the model. The systematic errors produced by the different physical parameterization schemes such as the land surface processes, convective precipitation, cloud-radiation transfer process, boundary layer process and large-scale terrain features have been identified based on multi-year and extreme flooding event simulations. A number of comparative experiments has shown that the mass flux scheme （MFS） and Betts-Miller scheme （BM） for convective precipitation, the LPMI （land surface process model I） and LPMII （land surface process model Ⅱ） for the land surface process, the CCM3 radiation transfer scheme for cloud-radiation transfer processes, the TKE （turbulent kinetic energy） scheme for the boundary layer processes and the topography treatment schemes for the Tibetan Plateau are suitable for simulations and prediction of the East Asia monsoon climate in rainy seasons. Based on the above sensitivity study, a modified version of the RegCM2 （RegCM_NCC） has been set up for climate simulations and seasonal predictions.展开更多
The effect of processing parameters such as hot rolling and heat treatment on microstructure and mechanical properties was investigated for a new 0.27mass% C and Ni, Mo-free low alloy martensitic abrasion resistant st...The effect of processing parameters such as hot rolling and heat treatment on microstructure and mechanical properties was investigated for a new 0.27mass% C and Ni, Mo-free low alloy martensitic abrasion resistant steel. The three-body impact abrasive wear behavior was also analyzed. The results showed that two-step controlled rolling besides quenching at 880 ℃ and tempering at 170 ℃ could result in optimal mechanical property., the Brinell hardness, tensile strength, elongation and --40 ℃ impact toughness were 531, 1530 MPa, 11.8% and 58 J, re- spectively. The microstructure was of fine lath martensite with little retained austenite. Three-body impact abrasive wear results showed that wear mechanism was mainly of plastic deformation fatigue when the impact energy was 2 J, and the relative wear resistance was 1.04 times higher than that of the same grade compared steel under the same working condition. The optimal hardness and toughness match was the main reason of higher wear resistance.展开更多
Two batches of commercial IN738LC alloy powders with different Zr contents were printed under the same parameters.The influences of Zr content(0.024 wt.% and 0.12 wt.%,respectively) in powders on crack density,distrib...Two batches of commercial IN738LC alloy powders with different Zr contents were printed under the same parameters.The influences of Zr content(0.024 wt.% and 0.12 wt.%,respectively) in powders on crack density,distribution,formation mechanism and mechanical properties of selective laser melting(SLM)-treated parts were systematically studied.It was found that the crack density(area ratio) increases from 0.15% to 0.87% in the XOY plane and from 0.21% to 1.81% in the XOZ plane along with the Zr content increase from 0.024 wt.% to 0.12 wt.% in the original powders.Solidification cracks are formed along the epitaxially grown <001>-oriented columnar grain boundaries in molten pool center.The ultimate tensile strength of Sample 1(0.024 wt.% Zr) is 1113 MPa,and there are dimples in tensile fracture.With an increase in the Zr content to 0.12 wt.%(Sample 2),the ultimate tensile strength of Sample 2 decreases to 610 MPa,and there are numerous original cracks and exposed columnar grain boundaries in tensile fracture.The optimization of printing parameters of Sample 2 considerably increases the ultimate tensile strength by 55.2% to 947 MPa,and the plasticity is greatly improved.展开更多
Cu-Cr-W composite coatings were prepared by mechanical alloying(MA)method using different powder ratios,rotational speeds and milling time.The micro structures and chemical compositions of as-synthesized coatings were...Cu-Cr-W composite coatings were prepared by mechanical alloying(MA)method using different powder ratios,rotational speeds and milling time.The micro structures and chemical compositions of as-synthesized coatings were analyzed by scanning electron microscopy(SEM)and energy-dispersive spectroscopy(EDS).Phases of ball-milled powders were identified by X-ray diffraction(XRD).The results indicate that the coating fabricated with powder ratio of 40 wt%Cu-Cr-W has better surface and cross-sectional microstructures and higher microhardness.The comparisons of cross-sectional micro structures of the coatings fabricated at different rotational speeds suggest that rotational speed of 300 r·min-1is the optimal for fabrication the coating,and the optimal milling time for the formation of coating is 7 h.The results of microhardness test show that the hardness of the substrate is largely improved because of the as-fabricated coatings.The results of the friction and wear tests indicate that the wear resistance of the copper substrate is improved after the deposition of Cu-Cr-W coating on it.The coating fabricated for 7 h exhibits the lowest friction coefficient,indicating its favorable friction and wear resistance.The formation mechanism of the coating was elucidated.According to the investigations in this work,the Cu-Cr-W coating fabricated by MA method is considered to be effective to reinforce the copper substrate.展开更多
Striving for cleaner production is a sought-after manufacturing philosophy.Friction stir welding(FSW)is a joiningtechnique with par excellence and far less invasive to the environment than even best conventional weldi...Striving for cleaner production is a sought-after manufacturing philosophy.Friction stir welding(FSW)is a joiningtechnique with par excellence and far less invasive to the environment than even best conventional welding processes.It is energyefficient and free from consumables,affluent and radiations.It is,thus,accepted as a clean welding process that can produceacceptable quality joints.It suffers from some major challenges of defects of its own kind that subject the process open toimprovements so as to prove itself a reliable production process.This study presents a holistic characterization of defects commonlyfound in FSW joints.The finding of the present study reveals that most defects are caused by inadequate heat generation,impropermaterial movement around the pin and inadequate material consolidation behind the pin.The amount of heat generation andmaterial stirring depends on several FSW parameters which may lead to the defect formation,if not selected properly.The resultsreported in this work are derived from sound literature support and experimentation.Prescriptions are made in the form ofcharacteristics of defects such as likelihood of their location,main responsible parameters along with the recommendations forminimizing them.展开更多
To further decrease the fuel consumption of blast furnace in Tangshan Guofeng Iron and Steel Co Ltd, measures of improving the quality of sinter and pellet and the performances of raw materials were put forward throug...To further decrease the fuel consumption of blast furnace in Tangshan Guofeng Iron and Steel Co Ltd, measures of improving the quality of sinter and pellet and the performances of raw materials were put forward through phase analysis and physical and chemical performance testing. The measures of increasing the grade of sinter, decreasing the sinter reduction degradation index at low temperature, and increasing the sinter soft melt performance at elevated temperature, as well as the reasonable process parameters of sintering were described in detail.展开更多
Response surface methodology (RSM) was employed in the present work and a second orderquadratic equation for high hydrostatic pressure (HHP) inactivation was built. Theadequacy of the model equation for predicting the...Response surface methodology (RSM) was employed in the present work and a second orderquadratic equation for high hydrostatic pressure (HHP) inactivation was built. Theadequacy of the model equation for predicting the optimum response values was verifiedeffectively by the validation data. Effects of temperature, pressure, and pressureholding time on HHP inactivation of Escherichia coli ATCC 8739 were explored. Byanalyzing the response surface plots and their corresponding contour plots as well assolving the quadratic equation, the optimum process parameters for inactivation E. coliof six log cycles were obtained as: temperature 32.2℃, pressure 346.4 MPa, and pressureholding time 12.6min.展开更多
The unsatisfied surface quality seriously impedes the wide application of incremental sheet forming(ISF)in industrial field.As a novel approach,the interpolator method is a promising strategy to enhance the surface qu...The unsatisfied surface quality seriously impedes the wide application of incremental sheet forming(ISF)in industrial field.As a novel approach,the interpolator method is a promising strategy to enhance the surface quality in ISF.However,the mechanism for the improvement of surface quality and the influence of interpolator properties on surface roughness are not well understood.In this paper,the influences of process variables(i.e.tool diameter,step size and thickness of interpolators)on the forming process(e.g.surface roughness,forming force and geometric error)are investigated through a systematic experimental approach of central composite design(CCD)in two-point incremental sheet forming(TPIF).It is obtained that the increase in thickness of interpolators decreases the surface roughness in direction vertical to the tool path while increases the surface roughness in direction horizontal to the tool path.Nevertheless,the combined influence between thickness of interpolators and process parameters(tool diameter and step size)is limited.Meanwhile,the placement of interpolator has little influence on the effective forming force of blank.In addition,the geometric error enlarges with the increase of step size and thickness of interpolator while decreases firstly and then increase with an increase in tool diameter.Finally,the influencing mechanism of the interpolator method on surface quality can be attributed to the decrease of thecontact pressure due to the increase of contact area with the unchanged contact force.Meanwhile,the interpolator method eliminates the sliding friction on the surface of blank due to the stable relative position between the blank and the interpolator.展开更多
The element partitioning in a Pb-Bi concentrate oxygen-rich bath smelting process was studied using thermodynamic equilibrium simulation method.Effects of oxygen to feed ratio(OFR)and sulfur dioxide partial pressure(p...The element partitioning in a Pb-Bi concentrate oxygen-rich bath smelting process was studied using thermodynamic equilibrium simulation method.Effects of oxygen to feed ratio(OFR)and sulfur dioxide partial pressure(pSO2)on the partitionings of Bi,Pb,As,Sb,Cu and Ag were analyzed and compared with industrial data.The results suggested that the optimal OFR was between 6.3 and 6.8 kmol/t to maximize Bi,Pb,Cu and Ag partitioning in the metal phase.Further increase of OFR led to the drop of metal partitioning and increase of slag liquidus temperature.High pSO2 led to high deportment of Bi and Pb in the gas phase mainly in the form of sulfides,suggesting that a low pSO2 was conducive for reducing the dust ratio.展开更多
基金financial supports from the National Natural Science Foundation of China(52130104,51821001)High Technology and Key Development Project of Ningbo,China(2019B10102)。
文摘Mg–3Nd–0.2Zn–0.4Zr(NZ30K,wt.%)alloy is a new kind of high-performance metallic biomaterial.The combination of the NZ30K Magnesium(Mg)alloy and selective laser melting(SLM)process seems to be an ideal solution to produce porous Mg degradable implants.However,the microstructure evolution and mechanical properties of the SLMed NZ30K Mg alloy were not yet studied systematically.Therefore,the fabrication defects,microstructure,and mechanical properties of the SLMed NZ30K alloy under different processing parameters were investigated.The results show that there are two types of fabrication defects in the SLMed NZ30K alloy,gas pores and unfused defects.With the increase of the laser energy density,the porosity sharply decreases to the minimum first and then slightly increases.The minimum porosity is 0.49±0.18%.While the microstructure varies from the large grains with lamellar structure inside under low laser energy density,to the large grains with lamellar structure inside&the equiaxed grains&the columnar grains under middle laser energy density,and further to the fine equiaxed grains&the columnar grains under high laser energy density.The lamellar structure in the large grain is a newly observed microstructure for the NZ30K Mg alloy.Higher laser energy density leads to finer grains,which enhance all the yield strength(YS),ultimate tensile strength(UTS)and elongation,and the best comprehensive mechanical properties obtained are YS of 266±2.1 MPa,UTS of 296±5.2 MPa,with an elongation of 4.9±0.68%.The SLMed NZ30K Mg alloy with a bimodal-grained structure consisting of fine equiaxed grains and coarser columnar grains has better elongation and a yield drop phenomenon.
基金supported by Liaoning Doctoral Research Start-up Fund project(Grant No.2023-BS-215).
文摘The relationships between the selective laser melting(SLM)processing parameters including laser power,scanning speed and hatch space,the relative density,the microstructure,and resulting mechanical properties of Ti-6Al-2Zr-1Mo-1V alloy were investigated in this work.The result shows that laser power acts a dominant role in determining the relative density in comparison with scanning speed and hatch space.The optimal SLM process window for fabricating relative density>99%samples is located in the energy density range of 34.72 J·mm^(-3)to 52.08 J·mm^(-3),where the laser power range is between 125 W and 175 W.An upward trend is found in the micro-hardness as the energy density is increased.The optimum SLM processing parameters of Ti-6Al-2Zr-1Mo-1V alloy are:laser power of 150 W,scanning speed of 1,600 mm·s^(-1),hatch space of 0.08 mm,and layer thickness of 0.03 mm.The highest ultimate tensile strength,yield strength,and ductility under the optimum processing parameter are achieved,which are 1,205 MPa,1,099 MPa,and 8%,respectively.The results of this study can be used to guide SLM production Ti-6Al-2Zr-1Mo-1V alloy parts.
基金The work was supported by the Innovation Fund for Small Technology-based Firms for Harbin DS Numerical Control Equipment Co.,Ltd.Samples,the micro-arcoxidation equipment and chemicals were provided by thecompany。
文摘The influence of processing parameters on the coating surface roughness of LD10 aluminum alloy treated by the power source with positive and negative pulse in the alkaline electrolyte was discussed.Lots of experiments were done with different processing parameters including the positive final voltage,the negative final voltage,the frequency,the duty ratio,the processing time and electrolyte temperature.And the surface roughness tester TR200 was used to measure the coating surface roughness.The influence of the processing time on the surface roughness is the smallest,less than 0.2μm.The surface roughness decreases gradually with the duty ratio decreasing or the frequency increasing;it decreases gradually with each of the other parameters increasing,and then increases gradually after achieving the minimum value.Appropriately by selecting processing parameters,the coating with Ra 0.6 can be obtained.
基金financially supported by the 2022 MTC Young Individual Research Grants under Singapore Research,Innovation and Enterprise(RIE)2025 Plan(No.M22K3c0097)the Natural Science Foundation of US(No.DMR-2104933)the sponsorship of the China Scholarship Council(No.202106130051)。
文摘Laser additive manufacturing(LAM)of titanium(Ti)alloys has emerged as a transformative technology with vast potential across multiple industries.To recap the state of the art,Ti alloys processed by two essential LAM techniques(i.e.,laser powder bed fusion and laser-directed energy deposition)will be reviewed,covering the aspects of processes,materials and post-processing.The impacts of process parameters and strategies for optimizing parameters will be elucidated.Various types of Ti alloys processed by LAM,includingα-Ti,(α+β)-Ti,andβ-Ti alloys,will be overviewed in terms of micro structures and benchmarking properties.Furthermore,the post-processing methods for improving the performance of L AM-processed Ti alloys,including conventional and novel heat treatment,hot isostatic pressing,and surface processing(e.g.,ultrasonic and laser shot peening),will be systematically reviewed and discussed.The review summarizes the process windows,properties,and performance envelopes and benchmarks the research achievements in LAM of Ti alloys.The outlooks of further trends in LAM of Ti alloys are also highlighted at the end of the review.This comprehensive review could serve as a valuable resource for researchers and practitioners,promoting further advancements in LAM-built Ti alloys and their applications.
基金finncially supported by the National Natural Science Foundation of China(No.52075183)the Guangdong Basic and Applied Research Fundamental(No.2023A1515010692)the Key-Area Research and Development Program of Guangdong Province(Nos.2024B1111080002 and 2020B0404020004).
文摘Austenitic stainless steel(ASS)is a common material used in high-pressure hydrogen systems.Prolonged exposure to high-pressure hydrogen can cause hydrogen embrittlement(HE),raising significant safety concerns.Selective Laser Melting(SLM),known for its high precision,is a promising additive manufacturing technology that has been widely adopted across various industries.Studies have reported that under certain SLM manufacturing conditions and process parameters,the HE resistance of SLM ASS is significantly better than that of conventionally manufactured(CM)ASS,showing great potential for application in high-pressure hydrogen systems.Thus,studying the HE of SLM ASS is crucial for further improving the safety of high-pressure hydrogen systems.This paper provides an overview of the SLM process,reviews the mechanisms of HE and their synergistic effects,and analyzes the HE characteristics of SLM ASS.Additionally,it examines the influence of unique microstructures and SLM process variables on HE of SLM ASS and offers recommendations for future research to enhance the safety of high-pressure hydrogen systems.
基金Shaanxi Province Qin Chuangyuan“Scientist+Engineer”Team Construction Project(2022KXJ-071)2022 Qin Chuangyuan Achievement Transformation Incubation Capacity Improvement Project(2022JH-ZHFHTS-0012)+1 种基金Shaanxi Province Key Research and Development Plan-“Two Chains”Integration Key Project-Qin Chuangyuan General Window Industrial Cluster Project(2023QCY-LL-02)Xixian New Area Science and Technology Plan(2022-YXYJ-003,2022-XXCY-010)。
文摘To overcome the shortage of complex equipment,large volume,and high energy consumption in space capsule manufacturing,a novel sliding pressure Joule heat fuse additive manufacturing technique with reduced volume and low energy consumption was proposed.But the unreasonable process parameters may lead to the inferior consistency of the forming quality of single-channel multilayer in Joule heat additive manufacturing process,and it is difficult to reach the condition for forming thinwalled parts.Orthogonal experiments were designed to fabricate single-channel multilayer samples with varying numbers of layers,and their forming quality was evaluated.The influence of printing current,forming speed,and contact pressure on the forming quality of the single-channel multilayer was analyzed.The optimal process parameters were obtained and the quality characterization of the experiment results was conducted.Results show that the printing current has the most significant influence on the forming quality of the single-channel multilayer.Under the optimal process parameters,the forming section is well fused and the surface is continuously smooth.The surface roughness of a single-channel 3-layer sample is 0.16μm,and the average Vickers hardness of cross section fusion zone is 317 HV,which lays a foundation for the subsequent use of Joule heat additive manufacturing technique to form thinwall parts.
基金project supported by the National Natural Science Foundation of China(Grant Nos.52225503 and 52405380)National Key Research and Development Program(Grant Nos.2023YFB4603303 and 2023YFB4603304)+4 种基金Key Research and Development Program of Jiangsu Province(Grant Nos.BE2022069 and BE2022069-3)National Natural Science Foundation of China for Creative Research Groups(Grant No.51921003)The 15th Batch of“Six Talents Peaks”Innovative Talents Team Program of Jiangsu province(Grant Nos.TD-GDZB-001)Shanghai Aerospace Science and Technology Innovation Fund Project(Grant No.SAST2023-066)The Fundamental Research Funds for the Central Universities(Grant Nos.NS2023035 and NP2024128)。
文摘Transpiration cooling is crucial for the performance of aerospace engine components,relying heavily on the processing quality and accuracy of microchannels.Laser powder bed fusion(LPBF)offers the potential for integrated manufacturing of complex parts and precise microchannel fabrication,essential for engine cooling applications.However,optimizing LPBF’s extensive process parameters to control processing quality and microchannel accuracy effectively remains a significant challenge,especially given the time-consuming and labor-intensive nature of handling numerous variables and the need for thorough data analysis and correlation discovery.This study introduced a combined methodology of high-throughput experiments and Gaussian process algorithms to optimize the processing quality and accuracy of nickel-based high-temperature alloy with microchannel structures.250 parameter combinations,including laser power,scanning speed,channel diameter,and spot compensation,were designed across ten high-throughput specimens.This setup allowed for rapid and efficient evaluation of processing quality and microchannel accuracy.Employing Bayesian optimization,the Gaussian process model accurately predicted processing outcomes over a broad parameter range.The correlation between various processing parameters,processing quality and accuracy was revealed,and various optimized process combinations were summarized.Verification through computed Tomography testing of the specimens confirmed the effectiveness and precision of this approach.The approach introduced in this research provides a way for quickly and efficiently optimizing the process parameters and establishing process-property relationships for LPBF,which has broad application value.
基金the financial support provided by the National Key R&D Program of China(Grant No.2023YFC3903900)the Science and Technology Innovation Talent Program of Hubei Province(Grant No.2022EJD002)+1 种基金the Sichuan Science and Technology Program(Grant No.2025ZNSFSC0378)the Key Laboratory of Green Chemistry of Sichuan Institutes of Higher Education(Grant No.LZJ2303).
文摘Specialized vanadium(V)-iron(Fe)-based alloy additives utilized in the production of V-containing steels were investigated.Vanadium slag from the Panzhihua region of China was utilized as a raw material to optimize process parameters for the preparation of V-Fe-based alloy via silicon thermal reduction.Experiments were conducted to investigate the effects of reduction temperature,holding time,and slag composition on alloy-slag separation,alloy microstructure,and the oxide content of residual slag,with an emphasis on the recovery of valuable metal elements.The results indicated that the optimal process conditions for silicon thermal reduction were achieved at reduction temperature of 1823 K,holding time of 240 min,and slag composition of 45 wt.%SiO_(2),40 wt.%CaO,and 15 wt.%Al_(2)O_(3).The resulting V-Fe-based alloy predominantly consisted of Fe-based phases such as Fe,titanium(Ti),silicon(Si)and manganese(Mn),with Si,V,as well as chromium(Cr)concentrated in the intercrystalline phase of the Fe-based alloy.The recoveries of Fe,Mn,Cr,V,and Ti under the optimal conditions were 96.30%,91.96%,86.53%,80.29%,and 74.82%,respectively.The key components of the V-Fe-based alloy obtained were 41.96 wt.%Si,27.55 wt.%Fe,12.13 wt.%Mn,5.53 wt.%V,4.86 wt.%Cr,and 3.74 wt.%Ti,thereby enabling the comprehensive recovery of the valuable metal from vanadium slag.
基金supported by the National Key R&D Program of China(No.2022YFA1005204l)。
文摘Silicone material extrusion(MEX)is widely used for processing liquids and pastes.Owing to the uneven linewidth and elastic extrusion deformation caused by material accumulation,products may exhibit geometric errors and performance defects,leading to a decline in product quality and affecting its service life.This study proposes a process parameter optimization method that considers the mechanical properties of printed specimens and production costs.To improve the quality of silicone printing samples and reduce production costs,three machine learning models,kernel extreme learning machine(KELM),support vector regression(SVR),and random forest(RF),were developed to predict these three factors.Training data were obtained through a complete factorial experiment.A new dataset is obtained using the Euclidean distance method,which assigns the elimination factor.It is trained with Bayesian optimization algorithms for parameter optimization,the new dataset is input into the improved double Gaussian extreme learning machine,and finally obtains the improved KELM model.The results showed improved prediction accuracy over SVR and RF.Furthermore,a multi-objective optimization framework was proposed by combining genetic algorithm technology with the improved KELM model.The effectiveness and reasonableness of the model algorithm were verified by comparing the optimized results with the experimental results.
基金Project(51235010)supported by the National Natural Science Foundation of ChinaProject(2010CB731700)supported by the National Basic Research Program of ChinaProject(20120162110003)supported by PhD Programs Foundation of Ministry of Education of China
文摘A series of tests were carried microstructures of 2124 aluminum alloy in increase of aging time, temperature and low-to-peak-to-low manner. No significant out to investigate the effects of process parameters on mechanical properties and creep aging process. The results show that creep strain and creep rate increase with the applied stress. The hardness of specimen varies with aging time and stress in a effect of temperature on hardness of material is seen in the range of 185-195 ℃. The optimum mechanical properties are obtained at the conditions of （200 MPa, 185 ℃, 8 h） as the result of the coexistence of strengthening S＂ and S＇ phases in the matrix by transmission electron microscopy （TEM）. TEM observation shows that applied stress promotes the formation and growth of precioitates and no obvious stress orientation effect is observed in the matrix.
基金Project(CSTC 2010BB4301) supported by Natural Science Foundation Project of Chongqing,ChinaProject supported by the Open Fund for Key Laboratory of Manufacture and Test Techniques for Automobile Parts of Ministry of Education Chongqing University of Technology,2003,China
文摘To study the influence of roll casting process parameters on temperature and thermal-stress fields for the AZ31 magnesium alloy sheets,three-dimensional geometric and 3D finite element models for roll casting were established based on the symmetry of roll casting by ANSYS software.Meshing method and smart-sizing algorithm were used to divide finite element mesh in ANSYS software.A series of researches on the temperature and stress distributions during solidification process with different process parameters were done by 3D finite element method.The temperatures of both the liquid-solid two-phase zone and liquid phase zone were elevated with increasing pouring temperature.With the heat transfer coefficient increasing,the two-phase region for liquid-solid becomes smaller.With the pouring temperature increasing and the increase of casting speed,the length of two-phase zone rises.The optimized of process parameters（casting speed 2 m/min,pouring temperature 640 ℃ and heat transfer coefficient 15 kW/（m2·℃） with the water pouring at roller exit was used to produce magnesium alloy AZ31 sheet,and equiaxed grains with the average grain size of 50 μm were achieved after roll casting.The simulation results give better understanding of the temperature variation in phase transformation zone and the formation mechanism of hot cracks in plates during roll casting and help to design the optimized process parameters of roll casting for Mg alloy.
文摘A modified version of the NCAR/RegCM2 has been developed at the National Climate Center （NCC）, China Meteorological Administration, through a series of sensitivity experiments and multi-year simulations and hindcasts, with a special emphasis on the adequate choice of physical parameterization schemes suitable for the East Asian monsoon climate. This regional climate model is nested with the NCC/IAP （Institute of Atmospheric Physics） T63 coupled GCM to make an experimental seasonal prediction for China and East Asia. The four-year （2001 to 2004） prediction results are encouraging. This paper is the first part of a two-part paper, and it mainly describes the sensitivity study of the physical process paraxneterization represented in the model. The systematic errors produced by the different physical parameterization schemes such as the land surface processes, convective precipitation, cloud-radiation transfer process, boundary layer process and large-scale terrain features have been identified based on multi-year and extreme flooding event simulations. A number of comparative experiments has shown that the mass flux scheme （MFS） and Betts-Miller scheme （BM） for convective precipitation, the LPMI （land surface process model I） and LPMII （land surface process model Ⅱ） for the land surface process, the CCM3 radiation transfer scheme for cloud-radiation transfer processes, the TKE （turbulent kinetic energy） scheme for the boundary layer processes and the topography treatment schemes for the Tibetan Plateau are suitable for simulations and prediction of the East Asia monsoon climate in rainy seasons. Based on the above sensitivity study, a modified version of the RegCM2 （RegCM_NCC） has been set up for climate simulations and seasonal predictions.
基金Item Sponsored by National Basic Research Program of China(2010CB630801)
文摘The effect of processing parameters such as hot rolling and heat treatment on microstructure and mechanical properties was investigated for a new 0.27mass% C and Ni, Mo-free low alloy martensitic abrasion resistant steel. The three-body impact abrasive wear behavior was also analyzed. The results showed that two-step controlled rolling besides quenching at 880 ℃ and tempering at 170 ℃ could result in optimal mechanical property., the Brinell hardness, tensile strength, elongation and --40 ℃ impact toughness were 531, 1530 MPa, 11.8% and 58 J, re- spectively. The microstructure was of fine lath martensite with little retained austenite. Three-body impact abrasive wear results showed that wear mechanism was mainly of plastic deformation fatigue when the impact energy was 2 J, and the relative wear resistance was 1.04 times higher than that of the same grade compared steel under the same working condition. The optimal hardness and toughness match was the main reason of higher wear resistance.
基金the financial supports from the Major Project of Science and Technology of Gansu Province,China(No.17ZD2GC011)the Hongliu First-class Discipline Construction Plan of Lanzhou University of Technology,China(No.CGZH001).
文摘Two batches of commercial IN738LC alloy powders with different Zr contents were printed under the same parameters.The influences of Zr content(0.024 wt.% and 0.12 wt.%,respectively) in powders on crack density,distribution,formation mechanism and mechanical properties of selective laser melting(SLM)-treated parts were systematically studied.It was found that the crack density(area ratio) increases from 0.15% to 0.87% in the XOY plane and from 0.21% to 1.81% in the XOZ plane along with the Zr content increase from 0.024 wt.% to 0.12 wt.% in the original powders.Solidification cracks are formed along the epitaxially grown <001>-oriented columnar grain boundaries in molten pool center.The ultimate tensile strength of Sample 1(0.024 wt.% Zr) is 1113 MPa,and there are dimples in tensile fracture.With an increase in the Zr content to 0.12 wt.%(Sample 2),the ultimate tensile strength of Sample 2 decreases to 610 MPa,and there are numerous original cracks and exposed columnar grain boundaries in tensile fracture.The optimization of printing parameters of Sample 2 considerably increases the ultimate tensile strength by 55.2% to 947 MPa,and the plasticity is greatly improved.
基金financially supported by the National Nature Science Foundation of China (No.51475232)the Jiangsu Province Natural Science Foundation (No.BK20141411)a Project Founded by the Priority Academic Program Development of Jiangsu Higher Education Institution
文摘Cu-Cr-W composite coatings were prepared by mechanical alloying(MA)method using different powder ratios,rotational speeds and milling time.The micro structures and chemical compositions of as-synthesized coatings were analyzed by scanning electron microscopy(SEM)and energy-dispersive spectroscopy(EDS).Phases of ball-milled powders were identified by X-ray diffraction(XRD).The results indicate that the coating fabricated with powder ratio of 40 wt%Cu-Cr-W has better surface and cross-sectional microstructures and higher microhardness.The comparisons of cross-sectional micro structures of the coatings fabricated at different rotational speeds suggest that rotational speed of 300 r·min-1is the optimal for fabrication the coating,and the optimal milling time for the formation of coating is 7 h.The results of microhardness test show that the hardness of the substrate is largely improved because of the as-fabricated coatings.The results of the friction and wear tests indicate that the wear resistance of the copper substrate is improved after the deposition of Cu-Cr-W coating on it.The coating fabricated for 7 h exhibits the lowest friction coefficient,indicating its favorable friction and wear resistance.The formation mechanism of the coating was elucidated.According to the investigations in this work,the Cu-Cr-W coating fabricated by MA method is considered to be effective to reinforce the copper substrate.
基金the University Grants Commission (UGC) for its financial assistance (vide sanction order No. F.3-40/2012(SAP-Ⅱ)) under its SAP (DRS-Ⅰ) sanctioned to the Department of Mechanical Engineering for the project entitled Friction Stir Welding and Ultrasonic Machiningfinancially supported by the King Saud University, Vice Deanship of Research Chairs
文摘Striving for cleaner production is a sought-after manufacturing philosophy.Friction stir welding(FSW)is a joiningtechnique with par excellence and far less invasive to the environment than even best conventional welding processes.It is energyefficient and free from consumables,affluent and radiations.It is,thus,accepted as a clean welding process that can produceacceptable quality joints.It suffers from some major challenges of defects of its own kind that subject the process open toimprovements so as to prove itself a reliable production process.This study presents a holistic characterization of defects commonlyfound in FSW joints.The finding of the present study reveals that most defects are caused by inadequate heat generation,impropermaterial movement around the pin and inadequate material consolidation behind the pin.The amount of heat generation andmaterial stirring depends on several FSW parameters which may lead to the defect formation,if not selected properly.The resultsreported in this work are derived from sound literature support and experimentation.Prescriptions are made in the form ofcharacteristics of defects such as likelihood of their location,main responsible parameters along with the recommendations forminimizing them.
文摘To further decrease the fuel consumption of blast furnace in Tangshan Guofeng Iron and Steel Co Ltd, measures of improving the quality of sinter and pellet and the performances of raw materials were put forward through phase analysis and physical and chemical performance testing. The measures of increasing the grade of sinter, decreasing the sinter reduction degradation index at low temperature, and increasing the sinter soft melt performance at elevated temperature, as well as the reasonable process parameters of sintering were described in detail.
文摘Response surface methodology (RSM) was employed in the present work and a second orderquadratic equation for high hydrostatic pressure (HHP) inactivation was built. Theadequacy of the model equation for predicting the optimum response values was verifiedeffectively by the validation data. Effects of temperature, pressure, and pressureholding time on HHP inactivation of Escherichia coli ATCC 8739 were explored. Byanalyzing the response surface plots and their corresponding contour plots as well assolving the quadratic equation, the optimum process parameters for inactivation E. coliof six log cycles were obtained as: temperature 32.2℃, pressure 346.4 MPa, and pressureholding time 12.6min.
基金support from the National Natural Science Foundation of China(51575028)National Natural Science Foundation of China(51605258)the Fundamental Research Funds for the Central Universities of China(YWF-18-BJ-J-75)。
文摘The unsatisfied surface quality seriously impedes the wide application of incremental sheet forming(ISF)in industrial field.As a novel approach,the interpolator method is a promising strategy to enhance the surface quality in ISF.However,the mechanism for the improvement of surface quality and the influence of interpolator properties on surface roughness are not well understood.In this paper,the influences of process variables(i.e.tool diameter,step size and thickness of interpolators)on the forming process(e.g.surface roughness,forming force and geometric error)are investigated through a systematic experimental approach of central composite design(CCD)in two-point incremental sheet forming(TPIF).It is obtained that the increase in thickness of interpolators decreases the surface roughness in direction vertical to the tool path while increases the surface roughness in direction horizontal to the tool path.Nevertheless,the combined influence between thickness of interpolators and process parameters(tool diameter and step size)is limited.Meanwhile,the placement of interpolator has little influence on the effective forming force of blank.In addition,the geometric error enlarges with the increase of step size and thickness of interpolator while decreases firstly and then increase with an increase in tool diameter.Finally,the influencing mechanism of the interpolator method on surface quality can be attributed to the decrease of thecontact pressure due to the increase of contact area with the unchanged contact force.Meanwhile,the interpolator method eliminates the sliding friction on the surface of blank due to the stable relative position between the blank and the interpolator.
基金financial supports from the National Key R&D Program of China(2018YFC1901604)the Natural Science Foundation of Hunan Province,China(2018JJ3662)+1 种基金the China Scholarship Council(201706375005)the China Postdoctoral Science Foundation(2018M632988)。
文摘The element partitioning in a Pb-Bi concentrate oxygen-rich bath smelting process was studied using thermodynamic equilibrium simulation method.Effects of oxygen to feed ratio(OFR)and sulfur dioxide partial pressure(pSO2)on the partitionings of Bi,Pb,As,Sb,Cu and Ag were analyzed and compared with industrial data.The results suggested that the optimal OFR was between 6.3 and 6.8 kmol/t to maximize Bi,Pb,Cu and Ag partitioning in the metal phase.Further increase of OFR led to the drop of metal partitioning and increase of slag liquidus temperature.High pSO2 led to high deportment of Bi and Pb in the gas phase mainly in the form of sulfides,suggesting that a low pSO2 was conducive for reducing the dust ratio.
