Monte Carlo （MC） method is the gold standard dose calculation algorithm. Determination of the electron beam parameters for MC simulation is often estimated using trial and error methods. However, this can be tedious...Monte Carlo （MC） method is the gold standard dose calculation algorithm. Determination of the electron beam parameters for MC simulation is often estimated using trial and error methods. However, this can be tedious and time-consuming. This paper aims to validate MC simulated data using 1D gamma analysis for 6MV photon beam to obtain the optimal parameters. BEAMnrc codes were used to generate phase space files for conventional field sizes 10 × 10 cm^2, 6 × 6 cm^2, 4 × 4 cm^2 and small field sizes 2 ×2 cm^2, 1 ×1 cm^2, 0.5 ×0.5 cm^2. For conventional field sizes, simulations were benchmarked against Golden Beam Data （GBD）. Simulations for small fields were benchmarked against measurements obtained using EDGE Detector and PTW Diode SRS detector in a Sun Nuclear 3D scanner. Dose profiles in water were calculated using DOSXYZnrc codes. Initial reference parameters were approximated using average percentage dose differences of different mean electron energy and electron beam radial distribution （Full Width at Half Maximum, FWHM）. Subsequently, the optimal parameters were validated by 1D gamma analysis using varying gamma criteria from γ3%%/0.3mm to γ2.0%/2.0mm for depth dose and lateral dose profiles. Comparisons were performed along the central region at depth dose 1.6 cm . Optimal parameters were found to be unique for small field sizes. As field size decreases, smaller FWHM were required to match measured data. By using 95% passing rate, a generic set of optimal electron beam parameters in a MC model for all field sizes could be accurately determined. Our findings provide MC users a set of optimal parameters with sufficient accuracy for MC simulation work.展开更多
In order to assess the effects of calibration data series length on the performance and optimal parameter values of a hydrological model in ungauged or data-limited catchments （data are non-continuous and fragmental ...In order to assess the effects of calibration data series length on the performance and optimal parameter values of a hydrological model in ungauged or data-limited catchments （data are non-continuous and fragmental in some catchments）, we used non-continuous calibration periods for more independent streamflow data for SIMHYD （simple hydrology） model calibration. Nash-Sutcliffe efficiency and percentage water balance error were used as performance measures. The particle swarm optimization （PSO） method was used to calibrate the rainfall-runoff models. Different lengths of data series ranging from one year to ten years, randomly sampled, were used to study the impact of calibration data series length. Fifty-five relatively unimpaired catchments located all over Australia with daily precipitation, potential evapotranspiration, and streamflow data were tested to obtain more general conclusions. The results show that longer calibration data series do not necessarily result in better model performance. In general, eight years of data are sufficient to obtain steady estimates of model performance and parameters for the SIMHYD model. It is also shown that most humid catchments require fewer calibration data to obtain a good performance and stable parameter values. The model performs better in humid and semi-humid catchments than in arid catchments. Our results may have useful and interesting implications for the efficiency of using limited observation data for hydrological model calibration in different climates.展开更多
Purpose-The indoor vibration compaction test(IVCT)was a key step in controlling the compaction quality for high-speed railway graded aggregate(HRGA),which currently had a research gap on the assessment indicators and ...Purpose-The indoor vibration compaction test(IVCT)was a key step in controlling the compaction quality for high-speed railway graded aggregate(HRGA),which currently had a research gap on the assessment indicators and compaction parameters.Design/methodology/approach-To address these issues,a novel multi-indicator IVCT method was proposed,including physical indicator dry density(ρd)and mechanical indicators dynamic stiffness(Krb)and bearing capacity coefficient(K20).Then,a series of IVCTs on HRGA under different compaction parameters were conducted with an improved vibration compactor,which could monitor the physical-mechanical indicators in real-time.Finally,the optimal vibration compaction parameters,including the moisture content(ω),the diameter-to-maximum particle size ratio(Rd),the thickness-to-maximum particle size ratio(Rh),the vibration frequency(f),the vibration mass(Mc)and the eccentric distance(re),were determined based on the evolution characteristics for the physical-mechanical indicators during compaction.Findings-All results indicated that theρd gradually increased and then stabilized,and the Krb initially increased and then decreased.Moreover,the inflection time of the Krb was present as the optimal compaction time(Tlp)during compaction.Additionally,optimal compaction was achieved whenωwas the water-holding content after mud pumping,Rd was 3.4,Rh was 3.5,f was the resonance frequency,and the ratio between the excitation force and the Mc was 1.8.Originality/value-The findings of this paper were significant for the quality control of HRGA compaction.展开更多
We propose a method to determine the optimal power of the microwave resonance transition that simultaneously improves the signal-to-noise ratio and reduces line width based on saturation broadening theory and experime...We propose a method to determine the optimal power of the microwave resonance transition that simultaneously improves the signal-to-noise ratio and reduces line width based on saturation broadening theory and experiment. Saturation broadening spectra of the ground state hyperfine transition of trapped 199Hg＋ ions are measured and analyzed. The value of the optimal microwave power is obtained by using the proposed method and is verified. Rabi oscillations decay spectra of trapped 199Hg＋ ions are observed and the optimal microwave irradiation time for the maximum transition signal intensity is determined. This work will help to improve the short-term frequency stability of the mercury ion microwave frequency standard.展开更多
In order to improve the strength and stiffness of shield cutterhead, the method of fuzzy mathematics theory in combination with the finite element analysis is adopted. An optimal design model of structural parameters ...In order to improve the strength and stiffness of shield cutterhead, the method of fuzzy mathematics theory in combination with the finite element analysis is adopted. An optimal design model of structural parameters for shield cutterhead is formulated,based on the complex engineering technical requirements. In the model, as the objective function of the model is a composite function of the strength and stiffness, the response surface method is applied to formulate the approximate function of objective function in order to reduce the solution scale of optimal problem. A multi-objective genetic algorithm is used to solve the cutterhead structure design problem and the change rule of the stress-strain with various structural parameters as well as their optimal values were researched under specific geological conditions. The results show that compared with original cutterhead structure scheme, the obtained optimal scheme of the cutterhead structure can greatly improve the strength and stiffness of the cutterhead, which can be seen from the reduction of its maximum equivalent stress by 21.2%, that of its maximum deformation by 0.75%, and that of its mass by 1.04%.展开更多
The aim of the study is to determine the optimal structural parameters for a plastic centrifugal pump inducer within the framework of an orthogonal experimental method.For this purpose,a numerical study of the related...The aim of the study is to determine the optimal structural parameters for a plastic centrifugal pump inducer within the framework of an orthogonal experimental method.For this purpose,a numerical study of the related flow field is performed using CFX.The shaft power and the head of the pump are taken as the evaluation indicators.Accordingly,the examined variables are the thickness(S),the blade cascade degree(t),the blade rim angle(β1),the blade hub angle(β2)and the hub length(L).The impact of each structural parameter on each evaluation index is examined and special attention is paid to the following combinations:S2 mm,t 2,β1235°,β2360°and L 140 mm(corresponding to a maximum head of 98.15 m);S 5 mm,t 1.6,β1252°,β2350°and L 140 mm(corresponding to a minimum shaft power of 63.06 KW).Moreover,using least squares and fish swarm algorithms,the pump shaft power and head are further optimized,yielding the following optimal combination:S 5 mm,t 1.9,β1252°,β2360°and L 145 mm(corresponding to the maximum head of 91.90 m,and a minimum shaft power of 64.83 KW).展开更多
The method for optimizing the hydraulic fracturing parameters of the cube development infill well pad was proposed,aiming at the well pattern characteristic of“multi-layer and multi-period”of the infill wells in Sic...The method for optimizing the hydraulic fracturing parameters of the cube development infill well pad was proposed,aiming at the well pattern characteristic of“multi-layer and multi-period”of the infill wells in Sichuan Basin.The fracture propagation and inter-well interference model were established based on the evolution of 4D in-situ stress,and the evolution characteristics of stress and the mechanism of interference between wells were analyzed.The research shows that the increase in horizontal stress difference and the existence of natural fractures/faults are the main reasons for inter-well interference.Inter-well interference is likely to occur near the fracture zones and between the infill wells and parent wells that have been in production for a long time.When communication channels are formed between the infill wells and parent wells,it can increase the productivity of parent wells in the short term.However,it will have a delayed negative impact on the long-term sustained production of both infill wells and parent wells.The change trend of in-situ stress caused by parent well production is basically consistent with the decline trend of pore pressure.The lateral disturbance range of in-situ stress is initially the same as the fracture length and reaches 1.5 to 1.6 times that length after 2.5 years.The key to avoiding inter-well interference is to optimize the fracturing parameters.By adopting the M-shaped well pattern,the optimal well spacing for the infill wells is 300 m,the cluster spacing is 10 m,and the liquid volume per stage is 1800 m^(3).展开更多
This work proposes an optimization method for gas storage operation parameters under multi-factor coupled constraints to improve the peak-shaving capacity of gas storage reservoirs while ensuring operational safety.Pr...This work proposes an optimization method for gas storage operation parameters under multi-factor coupled constraints to improve the peak-shaving capacity of gas storage reservoirs while ensuring operational safety.Previous research primarily focused on integrating reservoir,wellbore,and surface facility constraints,often resulting in broad constraint ranges and slow model convergence.To solve this problem,the present study introduces additional constraints on maximum withdrawal rates by combining binomial deliverability equations with material balance equations for closed gas reservoirs,while considering extreme peak-shaving demands.This approach effectively narrows the constraint range.Subsequently,a collaborative optimization model with maximum gas production as the objective function is established,and the model employs a joint solution strategy combining genetic algorithms and numerical simulation techniques.Finally,this methodology was applied to optimize operational parameters for Gas Storage T.The results demonstrate:(1)The convergence of the model was achieved after 6 iterations,which significantly improved the convergence speed of the model;(2)The maximum working gas volume reached 11.605×10^(8) m^(3),which increased by 13.78%compared with the traditional optimization method;(3)This method greatly improves the operation safety and the ultimate peak load balancing capability.The research provides important technical support for the intelligent decision of injection and production parameters of gas storage and improving peak load balancing ability.展开更多
Specialized vanadium(V)-iron(Fe)-based alloy additives utilized in the production of V-containing steels were investigated.Vanadium slag from the Panzhihua region of China was utilized as a raw material to optimize pr...Specialized vanadium(V)-iron(Fe)-based alloy additives utilized in the production of V-containing steels were investigated.Vanadium slag from the Panzhihua region of China was utilized as a raw material to optimize process parameters for the preparation of V-Fe-based alloy via silicon thermal reduction.Experiments were conducted to investigate the effects of reduction temperature,holding time,and slag composition on alloy-slag separation,alloy microstructure,and the oxide content of residual slag,with an emphasis on the recovery of valuable metal elements.The results indicated that the optimal process conditions for silicon thermal reduction were achieved at reduction temperature of 1823 K,holding time of 240 min,and slag composition of 45 wt.%SiO_(2),40 wt.%CaO,and 15 wt.%Al_(2)O_(3).The resulting V-Fe-based alloy predominantly consisted of Fe-based phases such as Fe,titanium(Ti),silicon(Si)and manganese(Mn),with Si,V,as well as chromium(Cr)concentrated in the intercrystalline phase of the Fe-based alloy.The recoveries of Fe,Mn,Cr,V,and Ti under the optimal conditions were 96.30%,91.96%,86.53%,80.29%,and 74.82%,respectively.The key components of the V-Fe-based alloy obtained were 41.96 wt.%Si,27.55 wt.%Fe,12.13 wt.%Mn,5.53 wt.%V,4.86 wt.%Cr,and 3.74 wt.%Ti,thereby enabling the comprehensive recovery of the valuable metal from vanadium slag.展开更多
It is a challenging issue to obtain the minimum amplitude control for linear systems subject to amplitudebounded disturbances.The difficulty is how to accurately give the quantitative relationship between the system H...It is a challenging issue to obtain the minimum amplitude control for linear systems subject to amplitudebounded disturbances.The difficulty is how to accurately give the quantitative relationship between the system H∞norm and control parameters.An optimal-Lyapunov-function-based controller design concept is proposed,and a minimum amplitude control scheme is presented under amplitude-bounded disturbances.Firstly,the optimal Lyapunov function is proposed by analyzing the geometric characteristics of the system H∞norm,and the necessary and sufficient condition of the optimal Lyapunov function parameter matrix is given.Secondly,the optimal Lyapunov function parameter matrix is constructed in the parameterized matrix equation,and the accurate quantitative relationship between the system H∞norm and control parameters is given.Finally,the control parameter optimization method is proposed according to the quantitative relationship between the system H∞norm and control parameters.Unlike robust optimization control methods,the presented minimum amplitude control scheme avoids the improper selection of the Lyapunov function in the controller design,and provides a novel way to design the minimum amplitude control under the given control accuracy.A buck converter example is given to illustrate the effectiveness and practicability of the presented scheme.展开更多
Silicone material extrusion(MEX)is widely used for processing liquids and pastes.Owing to the uneven linewidth and elastic extrusion deformation caused by material accumulation,products may exhibit geometric errors an...Silicone material extrusion(MEX)is widely used for processing liquids and pastes.Owing to the uneven linewidth and elastic extrusion deformation caused by material accumulation,products may exhibit geometric errors and performance defects,leading to a decline in product quality and affecting its service life.This study proposes a process parameter optimization method that considers the mechanical properties of printed specimens and production costs.To improve the quality of silicone printing samples and reduce production costs,three machine learning models,kernel extreme learning machine(KELM),support vector regression(SVR),and random forest(RF),were developed to predict these three factors.Training data were obtained through a complete factorial experiment.A new dataset is obtained using the Euclidean distance method,which assigns the elimination factor.It is trained with Bayesian optimization algorithms for parameter optimization,the new dataset is input into the improved double Gaussian extreme learning machine,and finally obtains the improved KELM model.The results showed improved prediction accuracy over SVR and RF.Furthermore,a multi-objective optimization framework was proposed by combining genetic algorithm technology with the improved KELM model.The effectiveness and reasonableness of the model algorithm were verified by comparing the optimized results with the experimental results.展开更多
The high temperature deformation behaviors of α＋β type titanium alloy TC11 （Ti-6.5Al-3.5Mo-1.5Zr-0.3Si） with coarse lamellar starting microstructure were investigated based on the hot compression tests in the tem...The high temperature deformation behaviors of α＋β type titanium alloy TC11 （Ti-6.5Al-3.5Mo-1.5Zr-0.3Si） with coarse lamellar starting microstructure were investigated based on the hot compression tests in the temperature range of 950-1100 ℃ and the strain rate range of 0.001-10 s-1. The processing maps at different strains were then constructed based on the dynamic materials model, and the hot compression process parameters and deformation mechanism were optimized and analyzed, respectively. The results show that the processing maps exhibit two domains with a high efficiency of power dissipation and a flow instability domain with a less efficiency of power dissipation. The types of domains were characterized by convergence and divergence of the efficiency of power dissipation, respectively. The convergent domain in a＋fl phase field is at the temperature of 950-990 ℃ and the strain rate of 0.001-0.01 s^-1, which correspond to a better hot compression process window of α＋β phase field. The peak of efficiency of power dissipation in α＋β phase field is at 950 ℃ and 0.001 s 1, which correspond to the best hot compression process parameters of α＋β phase field. The convergent domain in β phase field is at the temperature of 1020-1080 ℃ and the strain rate of 0.001-0.1 s^-l, which correspond to a better hot compression process window of β phase field. The peak of efficiency of power dissipation in ℃ phase field occurs at 1050 ℃ over the strain rates from 0.001 s^-1 to 0.01 s^-1, which correspond to the best hot compression process parameters of ,8 phase field. The divergence domain occurs at the strain rates above 0.5 s^-1 and in all the tested temperature range, which correspond to flow instability that is manifested as flow localization and indicated by the flow softening phenomenon in stress-- strain curves. The deformation mechanisms of the optimized hot compression process windows in a＋β and β phase fields are identified to be spheroidizing and dynamic recrystallizing controlled by self-diffusion mechanism, respectively. The microstructure observation of the deformed specimens in different domains matches very well with the optimized results.展开更多
Aim To obtain an optimizing range of the main configuration parameters of double swirls combustion system (DSCS) Methods To analyze the influence of DS combustion cham-ber configuration parameters on fuel spray and mi...Aim To obtain an optimizing range of the main configuration parameters of double swirls combustion system (DSCS) Methods To analyze the influence of DS combustion cham-ber configuration parameters on fuel spray and mixing by means of the fuel jet developmentperiphery charts obtained by the high speed photography with a modeling test device deve-loped by authors,and to examine it by the tests on a single cylinder diesel engine.Resultsand Conclusion The mixing process can be divided into four phases.The optimizing range of the ration of the inner chamber diameter to the cylinder bore,d2/D,is 0.4-0.7; and the outerchamber diameter,d1 the height of the circular ridge to the piston top face,h1,the radius of outer/inner chamber circle,R1,R2 ,the max depth of outer/inner chamber bowl,H1,H2,etc. are also important展开更多
Most previous land-surface model calibration studies have defined globalranges for their parameters to search for optimal parameter sets. Little work has been conducted tostudy the impacts of realistic versus global r...Most previous land-surface model calibration studies have defined globalranges for their parameters to search for optimal parameter sets. Little work has been conducted tostudy the impacts of realistic versus global ranges as well as model complexities on the calibrationand uncertainty estimates. The primary purpose of this paper is to investigate these impacts byemploying Bayesian Stochastic Inversion (BSI) to the Chameleon Surface Model (CHASM). The CHASM wasdesigned to explore the general aspects of land-surface energy balance representation within acommon modeling framework that can be run from a simple energy balance formulation to a complexmosaic type structure. The BSI is an uncertainty estimation technique based on Bayes theorem,importance sampling, and very fast simulated annealing. The model forcing data and surface flux datawere collected at seven sites representing a wide range of climate and vegetation conditions. Foreach site, four experiments were performed with simple and complex CHASM formulations as well asrealistic and global parameter ranges. Twenty eight experiments were conducted and 50 000 parametersets were used for each run. The results show that the use of global and realistic ranges givessimilar simulations for both modes for most sites, but the global ranges tend to produce someunreasonable optimal parameter values. Comparison of simple and complex modes shows that the simplemode has more parameters with unreasonable optimal values. Use of parameter ranges and modelcomplexities have significant impacts on frequency distribution of parameters, marginal posteriorprobability density functions, and estimates of uncertainty of simulated sensible and latent heatfluxes. Comparison between model complexity and parameter ranges shows that the former has moresignificant impacts on parameter and uncertainty estimations.展开更多
With the help of FESEM, high resolution electron backscatter diffraction can investigate the grains/subgrains as small as a few tens of nanometers with a good angular resolution （~0.5°）. Fast development of EBS...With the help of FESEM, high resolution electron backscatter diffraction can investigate the grains/subgrains as small as a few tens of nanometers with a good angular resolution （~0.5°）. Fast development of EBSD speed （up to 1100 patterns per second） contributes that the number of published articles related to EBSD has been increasing sharply year by year. This paper reviews the sample preparation, parameters optimization and analysis of EBSD technique, emphasizing on the investigation of ultrafine grained and nanostructured materials processed by severe plastic deformation （SPD）. Detailed and practical parameters of the electropolishing, silica polishing and ion milling have been summarized. It is shown that ion milling is a real universal and promising polishing method for EBSD preparation of almost all materials. There exists a maximum value of indexed points as a function of step size. The optimum step size depends on the magnification and the board resolution/electronic step size. Grains/subgrains and texture, and grain boundary structure are readily obtained by EBSD. Strain and stored energy may be analyzed by EBSD.展开更多
The paper analyzes the factors influencing machine tool selection. By using fuzzy mathematics theory, we establish a theorietical model for optimal machine tool selection considering geometric features, clamping size,...The paper analyzes the factors influencing machine tool selection. By using fuzzy mathematics theory, we establish a theorietical model for optimal machine tool selection considering geometric features, clamping size, machining range, machining precision and surface roughness. By means of fuzzy comprehensive evaluation method, the membership degree of machine tool selection and the largest comprehensive evaluation index are determined. Then the reasonably automatic selection of machine tool is realized in the generative computer aided process planning （CAPP） system. Finally, the finite element model based on ABAQUS is established and the cutting process of machine tool is simulated. According to the theoretical and empirical cutting parameters and the curve of surface residual stress, the optimal cutting parameters can be determined.展开更多
In-situ enlargement of super-large-span tunnels can intensify excavation-induced unloading in the surrounding rock,increasing deformation demand and failure risk during construction.This study combines laboratory mode...In-situ enlargement of super-large-span tunnels can intensify excavation-induced unloading in the surrounding rock,increasing deformation demand and failure risk during construction.This study combines laboratory model tests with FLAC3D simulations to evaluate the stabilizing role of prestressed anchor cables and to establish an energy-balance framework for support optimization.Comparative model tests of existing and enlarged tunnel sections,with and without anchors,show that reinforcement increases load-carrying capacity,reduces displacement,and confines damage to more localized zones.The numerical simulations reproduce displacement fields,shear-strain localization,and plastic-zone evolution with good agreement against the experimental observations.The energy framework is implemented in the in-situ simulations by quantifying unloading-related energy release in the rock mass and reinforcement work contributed by the anchors,and by introducing an energy release–reinforcement ratio as a stability indicator.Parametric analyses indicate that anchor length,spacing,and prestress influence stability in a nonlinear manner,with diminishing returns once reinforcement extends beyond the mechanically dominant deformation zone.An efficient parameter window is identified that improves deformation and yielding control while avoiding unnecessary reinforcement.The results provide an energy-consistent and design-oriented basis for prestressed anchorage selection in large-span tunnel expansion.展开更多
Laser welding is a highly promising joining method for Al alloys.However,certain limitations such as elevated thermal input and keyhole instability are associated with its application in medium-thickness aluminium all...Laser welding is a highly promising joining method for Al alloys.However,certain limitations such as elevated thermal input and keyhole instability are associated with its application in medium-thickness aluminium alloy plates.To address these issues,circular oscillating laser welding combined with post-weld heat treatment was employed to improve the formation quality and mechanical properties of the welds.The effects of the frequency of circular oscillating laser on the forming quality,microstructure,and properties of the welds were analyzed.At an oscillation frequency of 200 Hz,the grain size in the weld zone was reduced compared to single laser welding,and the maximum tensile strength of the weld was observed to reach(264.96±1.33)MPa,representing approximately 61.19%of the base metal.Following the post-weld heat treatment of"solid solution and artificial aging",the grain boundary segregation was diminished.Nanoscale precipitated phases are present in the weld zone.Furthermore,the tensile strength was augmented to(386.35±5.65)MPa,representing approximately 89.23%of the strength of the base metal.The results of this study can provide a theoretical basis and technological reference for the circular oscillating laser welding of medium-thickness 2219-T 6 aluminium alloy plates.展开更多
Laser-assisted drilling combined with full-size polycrystalline diamond compact(PDC)bit is considered a feasible solution to enhance the drilling performance of engineering machinery.In this method,determining the opt...Laser-assisted drilling combined with full-size polycrystalline diamond compact(PDC)bit is considered a feasible solution to enhance the drilling performance of engineering machinery.In this method,determining the optimal collaborative control parameters that support rapid drilling is crucial for improving the combined performance.This study used average drilling speed,average torque,and total specificenergy for quantitative analysis to characterize the efficiencyand economy of combined rock breaking.Given the advantage of the response surface methodology in providing high-precision predictions with limited experimental data,regression models of the average drilling speed,average torque,and total specificenergy were established.The results showed that as the laser power and irradiation time increased,the average drilling speed firstincreased rapidly and then leveled off,while the average torque decreased sharply before decelerating.The total specificenergy initially decreased and then increased,with the combined drilling outperforming conventional mechanical drilling within specific parameter ranges.As the weight on bit increased,both the average torque and total specificenergy first decreased and then increased.With rising rotating speed,the average torque exhibited a trend of initial increase,then decrease,and finalincrease,whereas the total specificenergy increased slowly at firstand then sharply.Both parameters exhibited optimal values at which the average torque and total specific energy remained at minimal levels.For granite combined drilling,the optimal performance was achieved at a laser power of 3000 W,irradiation time of 31 s,the weight on bit of 2.4 kN,and the rotating speed of 97 r/min.展开更多
Electroless copper plating on diamond particles precoated with 1%Cr was carried out to evaluate the effects of various experimental parameters on coating quality and deposition rate to obtain the optimized reaction pa...Electroless copper plating on diamond particles precoated with 1%Cr was carried out to evaluate the effects of various experimental parameters on coating quality and deposition rate to obtain the optimized reaction parameters. The formulated samples under optimized parameters were characterized by X-ray diffraction, scanning electron microscopy, energy dispersive spectroscopy, X-ray photoelectron spectra and optical microscopy. The best parameters, where uniform and maximum coating thickness was achieved, are etching with 20%NaOH for 30 min, sensitization and activation with SnCl2 and PdCl2 for 5 and 20 min, respectively. The composition of the copper solution bath was 16 g/L CuSO4＆#183;5H2O, 35 mL/L formaldehyde （HCHO）, 23 g/L KNaC4H4O6 at 60 ℃, pH=13 and stirring at （350±15） r/min under ultrasonication.展开更多
文摘Monte Carlo （MC） method is the gold standard dose calculation algorithm. Determination of the electron beam parameters for MC simulation is often estimated using trial and error methods. However, this can be tedious and time-consuming. This paper aims to validate MC simulated data using 1D gamma analysis for 6MV photon beam to obtain the optimal parameters. BEAMnrc codes were used to generate phase space files for conventional field sizes 10 × 10 cm^2, 6 × 6 cm^2, 4 × 4 cm^2 and small field sizes 2 ×2 cm^2, 1 ×1 cm^2, 0.5 ×0.5 cm^2. For conventional field sizes, simulations were benchmarked against Golden Beam Data （GBD）. Simulations for small fields were benchmarked against measurements obtained using EDGE Detector and PTW Diode SRS detector in a Sun Nuclear 3D scanner. Dose profiles in water were calculated using DOSXYZnrc codes. Initial reference parameters were approximated using average percentage dose differences of different mean electron energy and electron beam radial distribution （Full Width at Half Maximum, FWHM）. Subsequently, the optimal parameters were validated by 1D gamma analysis using varying gamma criteria from γ3%%/0.3mm to γ2.0%/2.0mm for depth dose and lateral dose profiles. Comparisons were performed along the central region at depth dose 1.6 cm . Optimal parameters were found to be unique for small field sizes. As field size decreases, smaller FWHM were required to match measured data. By using 95% passing rate, a generic set of optimal electron beam parameters in a MC model for all field sizes could be accurately determined. Our findings provide MC users a set of optimal parameters with sufficient accuracy for MC simulation work.
基金supported by the National Basic Research Program of China (the 973 Program,Grant No.2010CB951102)the National Supporting Plan Program of China (Grants No.2007BAB28B01 and 2008BAB42B03)the National Natural Science Foundation of China (Grant No. 50709042),and the Regional Water Theme in the Water for a Healthy Country Flagship
文摘In order to assess the effects of calibration data series length on the performance and optimal parameter values of a hydrological model in ungauged or data-limited catchments （data are non-continuous and fragmental in some catchments）, we used non-continuous calibration periods for more independent streamflow data for SIMHYD （simple hydrology） model calibration. Nash-Sutcliffe efficiency and percentage water balance error were used as performance measures. The particle swarm optimization （PSO） method was used to calibrate the rainfall-runoff models. Different lengths of data series ranging from one year to ten years, randomly sampled, were used to study the impact of calibration data series length. Fifty-five relatively unimpaired catchments located all over Australia with daily precipitation, potential evapotranspiration, and streamflow data were tested to obtain more general conclusions. The results show that longer calibration data series do not necessarily result in better model performance. In general, eight years of data are sufficient to obtain steady estimates of model performance and parameters for the SIMHYD model. It is also shown that most humid catchments require fewer calibration data to obtain a good performance and stable parameter values. The model performs better in humid and semi-humid catchments than in arid catchments. Our results may have useful and interesting implications for the efficiency of using limited observation data for hydrological model calibration in different climates.
基金funded by the National Key R&D Program“Transportation Infrastructure”project(No.2022YFB2603400)the Technology Research and Development Plan Program of China State Railway Group Co.,Ltd.(No.Q2024T001)the National project pre research project of Suzhou City University(No.2023SGY019).
文摘Purpose-The indoor vibration compaction test(IVCT)was a key step in controlling the compaction quality for high-speed railway graded aggregate(HRGA),which currently had a research gap on the assessment indicators and compaction parameters.Design/methodology/approach-To address these issues,a novel multi-indicator IVCT method was proposed,including physical indicator dry density(ρd)and mechanical indicators dynamic stiffness(Krb)and bearing capacity coefficient(K20).Then,a series of IVCTs on HRGA under different compaction parameters were conducted with an improved vibration compactor,which could monitor the physical-mechanical indicators in real-time.Finally,the optimal vibration compaction parameters,including the moisture content(ω),the diameter-to-maximum particle size ratio(Rd),the thickness-to-maximum particle size ratio(Rh),the vibration frequency(f),the vibration mass(Mc)and the eccentric distance(re),were determined based on the evolution characteristics for the physical-mechanical indicators during compaction.Findings-All results indicated that theρd gradually increased and then stabilized,and the Krb initially increased and then decreased.Moreover,the inflection time of the Krb was present as the optimal compaction time(Tlp)during compaction.Additionally,optimal compaction was achieved whenωwas the water-holding content after mud pumping,Rd was 3.4,Rh was 3.5,f was the resonance frequency,and the ratio between the excitation force and the Mc was 1.8.Originality/value-The findings of this paper were significant for the quality control of HRGA compaction.
基金Supported by the National Natural Science Foundation of China under Grant Nos 11074282 and 11474320
文摘We propose a method to determine the optimal power of the microwave resonance transition that simultaneously improves the signal-to-noise ratio and reduces line width based on saturation broadening theory and experiment. Saturation broadening spectra of the ground state hyperfine transition of trapped 199Hg＋ ions are measured and analyzed. The value of the optimal microwave power is obtained by using the proposed method and is verified. Rabi oscillations decay spectra of trapped 199Hg＋ ions are observed and the optimal microwave irradiation time for the maximum transition signal intensity is determined. This work will help to improve the short-term frequency stability of the mercury ion microwave frequency standard.
基金Project(51074180) supported by the National Natural Science Foundation of ChinaProject(2012AA041801) supported by the National High Technology Research and Development Program of China+2 种基金Project(2007CB714002) supported by the National Basic Research Program of ChinaProject(2013GK3003) supported by the Technology Support Plan of Hunan Province,ChinaProject(2010FJ1002) supported by Hunan Science and Technology Major Program,China
文摘In order to improve the strength and stiffness of shield cutterhead, the method of fuzzy mathematics theory in combination with the finite element analysis is adopted. An optimal design model of structural parameters for shield cutterhead is formulated,based on the complex engineering technical requirements. In the model, as the objective function of the model is a composite function of the strength and stiffness, the response surface method is applied to formulate the approximate function of objective function in order to reduce the solution scale of optimal problem. A multi-objective genetic algorithm is used to solve the cutterhead structure design problem and the change rule of the stress-strain with various structural parameters as well as their optimal values were researched under specific geological conditions. The results show that compared with original cutterhead structure scheme, the obtained optimal scheme of the cutterhead structure can greatly improve the strength and stiffness of the cutterhead, which can be seen from the reduction of its maximum equivalent stress by 21.2%, that of its maximum deformation by 0.75%, and that of its mass by 1.04%.
基金project of the“The University Synergy Innovation Program of Anhui Province(GXXT-2019-004)”,“Natural Science Research Project of Anhui Universities(KJ2021ZD0144)”,“Wuhu Key R&D Project:Research and Industrialization of Intelligent Control Method of Engine Energy-Feeding Hydraulic Semi-Active Mount”.
文摘The aim of the study is to determine the optimal structural parameters for a plastic centrifugal pump inducer within the framework of an orthogonal experimental method.For this purpose,a numerical study of the related flow field is performed using CFX.The shaft power and the head of the pump are taken as the evaluation indicators.Accordingly,the examined variables are the thickness(S),the blade cascade degree(t),the blade rim angle(β1),the blade hub angle(β2)and the hub length(L).The impact of each structural parameter on each evaluation index is examined and special attention is paid to the following combinations:S2 mm,t 2,β1235°,β2360°and L 140 mm(corresponding to a maximum head of 98.15 m);S 5 mm,t 1.6,β1252°,β2350°and L 140 mm(corresponding to a minimum shaft power of 63.06 KW).Moreover,using least squares and fish swarm algorithms,the pump shaft power and head are further optimized,yielding the following optimal combination:S 5 mm,t 1.9,β1252°,β2360°and L 145 mm(corresponding to the maximum head of 91.90 m,and a minimum shaft power of 64.83 KW).
基金Supported by the General Program of the NATIONAL NATURAL SCIENCE FOUNDATION OF CHINA(52374004)National Key Research and Development Program(2023YFF06141022023YFE0110900)。
文摘The method for optimizing the hydraulic fracturing parameters of the cube development infill well pad was proposed,aiming at the well pattern characteristic of“multi-layer and multi-period”of the infill wells in Sichuan Basin.The fracture propagation and inter-well interference model were established based on the evolution of 4D in-situ stress,and the evolution characteristics of stress and the mechanism of interference between wells were analyzed.The research shows that the increase in horizontal stress difference and the existence of natural fractures/faults are the main reasons for inter-well interference.Inter-well interference is likely to occur near the fracture zones and between the infill wells and parent wells that have been in production for a long time.When communication channels are formed between the infill wells and parent wells,it can increase the productivity of parent wells in the short term.However,it will have a delayed negative impact on the long-term sustained production of both infill wells and parent wells.The change trend of in-situ stress caused by parent well production is basically consistent with the decline trend of pore pressure.The lateral disturbance range of in-situ stress is initially the same as the fracture length and reaches 1.5 to 1.6 times that length after 2.5 years.The key to avoiding inter-well interference is to optimize the fracturing parameters.By adopting the M-shaped well pattern,the optimal well spacing for the infill wells is 300 m,the cluster spacing is 10 m,and the liquid volume per stage is 1800 m^(3).
基金supported by the Science and Technology Research Program of Chongqing Municipal Education Commission(KJQN202401501,KJZD-M202401501).
文摘This work proposes an optimization method for gas storage operation parameters under multi-factor coupled constraints to improve the peak-shaving capacity of gas storage reservoirs while ensuring operational safety.Previous research primarily focused on integrating reservoir,wellbore,and surface facility constraints,often resulting in broad constraint ranges and slow model convergence.To solve this problem,the present study introduces additional constraints on maximum withdrawal rates by combining binomial deliverability equations with material balance equations for closed gas reservoirs,while considering extreme peak-shaving demands.This approach effectively narrows the constraint range.Subsequently,a collaborative optimization model with maximum gas production as the objective function is established,and the model employs a joint solution strategy combining genetic algorithms and numerical simulation techniques.Finally,this methodology was applied to optimize operational parameters for Gas Storage T.The results demonstrate:(1)The convergence of the model was achieved after 6 iterations,which significantly improved the convergence speed of the model;(2)The maximum working gas volume reached 11.605×10^(8) m^(3),which increased by 13.78%compared with the traditional optimization method;(3)This method greatly improves the operation safety and the ultimate peak load balancing capability.The research provides important technical support for the intelligent decision of injection and production parameters of gas storage and improving peak load balancing ability.
基金the financial support provided by the National Key R&D Program of China(Grant No.2023YFC3903900)the Science and Technology Innovation Talent Program of Hubei Province(Grant No.2022EJD002)+1 种基金the Sichuan Science and Technology Program(Grant No.2025ZNSFSC0378)the Key Laboratory of Green Chemistry of Sichuan Institutes of Higher Education(Grant No.LZJ2303).
文摘Specialized vanadium(V)-iron(Fe)-based alloy additives utilized in the production of V-containing steels were investigated.Vanadium slag from the Panzhihua region of China was utilized as a raw material to optimize process parameters for the preparation of V-Fe-based alloy via silicon thermal reduction.Experiments were conducted to investigate the effects of reduction temperature,holding time,and slag composition on alloy-slag separation,alloy microstructure,and the oxide content of residual slag,with an emphasis on the recovery of valuable metal elements.The results indicated that the optimal process conditions for silicon thermal reduction were achieved at reduction temperature of 1823 K,holding time of 240 min,and slag composition of 45 wt.%SiO_(2),40 wt.%CaO,and 15 wt.%Al_(2)O_(3).The resulting V-Fe-based alloy predominantly consisted of Fe-based phases such as Fe,titanium(Ti),silicon(Si)and manganese(Mn),with Si,V,as well as chromium(Cr)concentrated in the intercrystalline phase of the Fe-based alloy.The recoveries of Fe,Mn,Cr,V,and Ti under the optimal conditions were 96.30%,91.96%,86.53%,80.29%,and 74.82%,respectively.The key components of the V-Fe-based alloy obtained were 41.96 wt.%Si,27.55 wt.%Fe,12.13 wt.%Mn,5.53 wt.%V,4.86 wt.%Cr,and 3.74 wt.%Ti,thereby enabling the comprehensive recovery of the valuable metal from vanadium slag.
基金supported in part by the National Natural Science Foundation of China(62373089).
文摘It is a challenging issue to obtain the minimum amplitude control for linear systems subject to amplitudebounded disturbances.The difficulty is how to accurately give the quantitative relationship between the system H∞norm and control parameters.An optimal-Lyapunov-function-based controller design concept is proposed,and a minimum amplitude control scheme is presented under amplitude-bounded disturbances.Firstly,the optimal Lyapunov function is proposed by analyzing the geometric characteristics of the system H∞norm,and the necessary and sufficient condition of the optimal Lyapunov function parameter matrix is given.Secondly,the optimal Lyapunov function parameter matrix is constructed in the parameterized matrix equation,and the accurate quantitative relationship between the system H∞norm and control parameters is given.Finally,the control parameter optimization method is proposed according to the quantitative relationship between the system H∞norm and control parameters.Unlike robust optimization control methods,the presented minimum amplitude control scheme avoids the improper selection of the Lyapunov function in the controller design,and provides a novel way to design the minimum amplitude control under the given control accuracy.A buck converter example is given to illustrate the effectiveness and practicability of the presented scheme.
基金supported by the National Key R&D Program of China(No.2022YFA1005204l)。
文摘Silicone material extrusion(MEX)is widely used for processing liquids and pastes.Owing to the uneven linewidth and elastic extrusion deformation caused by material accumulation,products may exhibit geometric errors and performance defects,leading to a decline in product quality and affecting its service life.This study proposes a process parameter optimization method that considers the mechanical properties of printed specimens and production costs.To improve the quality of silicone printing samples and reduce production costs,three machine learning models,kernel extreme learning machine(KELM),support vector regression(SVR),and random forest(RF),were developed to predict these three factors.Training data were obtained through a complete factorial experiment.A new dataset is obtained using the Euclidean distance method,which assigns the elimination factor.It is trained with Bayesian optimization algorithms for parameter optimization,the new dataset is input into the improved double Gaussian extreme learning machine,and finally obtains the improved KELM model.The results showed improved prediction accuracy over SVR and RF.Furthermore,a multi-objective optimization framework was proposed by combining genetic algorithm technology with the improved KELM model.The effectiveness and reasonableness of the model algorithm were verified by comparing the optimized results with the experimental results.
基金Project (51005112) supported by the National Natural Science Foundation of ChinaProject (2010ZF56019) supported by the Aviation Science Foundation of China+1 种基金Project (GJJ11156) supported by the Education Commission of Jiangxi Province, ChinaProject(GF200901008) supported by the Open Fund of National Defense Key Disciplines Laboratory of Light Alloy Processing Science and Technology, China
文摘The high temperature deformation behaviors of α＋β type titanium alloy TC11 （Ti-6.5Al-3.5Mo-1.5Zr-0.3Si） with coarse lamellar starting microstructure were investigated based on the hot compression tests in the temperature range of 950-1100 ℃ and the strain rate range of 0.001-10 s-1. The processing maps at different strains were then constructed based on the dynamic materials model, and the hot compression process parameters and deformation mechanism were optimized and analyzed, respectively. The results show that the processing maps exhibit two domains with a high efficiency of power dissipation and a flow instability domain with a less efficiency of power dissipation. The types of domains were characterized by convergence and divergence of the efficiency of power dissipation, respectively. The convergent domain in a＋fl phase field is at the temperature of 950-990 ℃ and the strain rate of 0.001-0.01 s^-1, which correspond to a better hot compression process window of α＋β phase field. The peak of efficiency of power dissipation in α＋β phase field is at 950 ℃ and 0.001 s 1, which correspond to the best hot compression process parameters of α＋β phase field. The convergent domain in β phase field is at the temperature of 1020-1080 ℃ and the strain rate of 0.001-0.1 s^-l, which correspond to a better hot compression process window of β phase field. The peak of efficiency of power dissipation in ℃ phase field occurs at 1050 ℃ over the strain rates from 0.001 s^-1 to 0.01 s^-1, which correspond to the best hot compression process parameters of ,8 phase field. The divergence domain occurs at the strain rates above 0.5 s^-1 and in all the tested temperature range, which correspond to flow instability that is manifested as flow localization and indicated by the flow softening phenomenon in stress-- strain curves. The deformation mechanisms of the optimized hot compression process windows in a＋β and β phase fields are identified to be spheroidizing and dynamic recrystallizing controlled by self-diffusion mechanism, respectively. The microstructure observation of the deformed specimens in different domains matches very well with the optimized results.
文摘Aim To obtain an optimizing range of the main configuration parameters of double swirls combustion system (DSCS) Methods To analyze the influence of DS combustion cham-ber configuration parameters on fuel spray and mixing by means of the fuel jet developmentperiphery charts obtained by the high speed photography with a modeling test device deve-loped by authors,and to examine it by the tests on a single cylinder diesel engine.Resultsand Conclusion The mixing process can be divided into four phases.The optimizing range of the ration of the inner chamber diameter to the cylinder bore,d2/D,is 0.4-0.7; and the outerchamber diameter,d1 the height of the circular ridge to the piston top face,h1,the radius of outer/inner chamber circle,R1,R2 ,the max depth of outer/inner chamber bowl,H1,H2,etc. are also important
文摘Most previous land-surface model calibration studies have defined globalranges for their parameters to search for optimal parameter sets. Little work has been conducted tostudy the impacts of realistic versus global ranges as well as model complexities on the calibrationand uncertainty estimates. The primary purpose of this paper is to investigate these impacts byemploying Bayesian Stochastic Inversion (BSI) to the Chameleon Surface Model (CHASM). The CHASM wasdesigned to explore the general aspects of land-surface energy balance representation within acommon modeling framework that can be run from a simple energy balance formulation to a complexmosaic type structure. The BSI is an uncertainty estimation technique based on Bayes theorem,importance sampling, and very fast simulated annealing. The model forcing data and surface flux datawere collected at seven sites representing a wide range of climate and vegetation conditions. Foreach site, four experiments were performed with simple and complex CHASM formulations as well asrealistic and global parameter ranges. Twenty eight experiments were conducted and 50 000 parametersets were used for each run. The results show that the use of global and realistic ranges givessimilar simulations for both modes for most sites, but the global ranges tend to produce someunreasonable optimal parameter values. Comparison of simple and complex modes shows that the simplemode has more parameters with unreasonable optimal values. Use of parameter ranges and modelcomplexities have significant impacts on frequency distribution of parameters, marginal posteriorprobability density functions, and estimates of uncertainty of simulated sensible and latent heatfluxes. Comparison between model complexity and parameter ranges shows that the former has moresignificant impacts on parameter and uncertainty estimations.
基金Project (192450/I30) supported by the Norwegian Research Council under the Strategic University Program
文摘With the help of FESEM, high resolution electron backscatter diffraction can investigate the grains/subgrains as small as a few tens of nanometers with a good angular resolution （~0.5°）. Fast development of EBSD speed （up to 1100 patterns per second） contributes that the number of published articles related to EBSD has been increasing sharply year by year. This paper reviews the sample preparation, parameters optimization and analysis of EBSD technique, emphasizing on the investigation of ultrafine grained and nanostructured materials processed by severe plastic deformation （SPD）. Detailed and practical parameters of the electropolishing, silica polishing and ion milling have been summarized. It is shown that ion milling is a real universal and promising polishing method for EBSD preparation of almost all materials. There exists a maximum value of indexed points as a function of step size. The optimum step size depends on the magnification and the board resolution/electronic step size. Grains/subgrains and texture, and grain boundary structure are readily obtained by EBSD. Strain and stored energy may be analyzed by EBSD.
基金Shanxi Province Science and Technology Research Project(No.20140321008-03)
文摘The paper analyzes the factors influencing machine tool selection. By using fuzzy mathematics theory, we establish a theorietical model for optimal machine tool selection considering geometric features, clamping size, machining range, machining precision and surface roughness. By means of fuzzy comprehensive evaluation method, the membership degree of machine tool selection and the largest comprehensive evaluation index are determined. Then the reasonably automatic selection of machine tool is realized in the generative computer aided process planning （CAPP） system. Finally, the finite element model based on ABAQUS is established and the cutting process of machine tool is simulated. According to the theoretical and empirical cutting parameters and the curve of surface residual stress, the optimal cutting parameters can be determined.
基金funded by the National Key R&D Program of China,China(No.2024YFF0507903)the National Key Research and Development Program of China(Grant No.2024YFF0507904)the National Natural Science Foundation of China,China(Grant No.52379114).These supports are gratefully acknowledged.
文摘In-situ enlargement of super-large-span tunnels can intensify excavation-induced unloading in the surrounding rock,increasing deformation demand and failure risk during construction.This study combines laboratory model tests with FLAC3D simulations to evaluate the stabilizing role of prestressed anchor cables and to establish an energy-balance framework for support optimization.Comparative model tests of existing and enlarged tunnel sections,with and without anchors,show that reinforcement increases load-carrying capacity,reduces displacement,and confines damage to more localized zones.The numerical simulations reproduce displacement fields,shear-strain localization,and plastic-zone evolution with good agreement against the experimental observations.The energy framework is implemented in the in-situ simulations by quantifying unloading-related energy release in the rock mass and reinforcement work contributed by the anchors,and by introducing an energy release–reinforcement ratio as a stability indicator.Parametric analyses indicate that anchor length,spacing,and prestress influence stability in a nonlinear manner,with diminishing returns once reinforcement extends beyond the mechanically dominant deformation zone.An efficient parameter window is identified that improves deformation and yielding control while avoiding unnecessary reinforcement.The results provide an energy-consistent and design-oriented basis for prestressed anchorage selection in large-span tunnel expansion.
基金Projects(E2024203001,E2024203049,E2024203071)supported by the Hebei Natural Science Foundation of ChinaProject(236Z1805G)supported by the S&T Program of Hebei,China。
文摘Laser welding is a highly promising joining method for Al alloys.However,certain limitations such as elevated thermal input and keyhole instability are associated with its application in medium-thickness aluminium alloy plates.To address these issues,circular oscillating laser welding combined with post-weld heat treatment was employed to improve the formation quality and mechanical properties of the welds.The effects of the frequency of circular oscillating laser on the forming quality,microstructure,and properties of the welds were analyzed.At an oscillation frequency of 200 Hz,the grain size in the weld zone was reduced compared to single laser welding,and the maximum tensile strength of the weld was observed to reach(264.96±1.33)MPa,representing approximately 61.19%of the base metal.Following the post-weld heat treatment of"solid solution and artificial aging",the grain boundary segregation was diminished.Nanoscale precipitated phases are present in the weld zone.Furthermore,the tensile strength was augmented to(386.35±5.65)MPa,representing approximately 89.23%of the strength of the base metal.The results of this study can provide a theoretical basis and technological reference for the circular oscillating laser welding of medium-thickness 2219-T 6 aluminium alloy plates.
基金funded by the National Natural Science Foundation of China(Grand No.52325904)National Key Research and Development Program of China(Grant No.2023YFB2390200)the National Natural Science Foundation of China(Grant No.52309134).
文摘Laser-assisted drilling combined with full-size polycrystalline diamond compact(PDC)bit is considered a feasible solution to enhance the drilling performance of engineering machinery.In this method,determining the optimal collaborative control parameters that support rapid drilling is crucial for improving the combined performance.This study used average drilling speed,average torque,and total specificenergy for quantitative analysis to characterize the efficiencyand economy of combined rock breaking.Given the advantage of the response surface methodology in providing high-precision predictions with limited experimental data,regression models of the average drilling speed,average torque,and total specificenergy were established.The results showed that as the laser power and irradiation time increased,the average drilling speed firstincreased rapidly and then leveled off,while the average torque decreased sharply before decelerating.The total specificenergy initially decreased and then increased,with the combined drilling outperforming conventional mechanical drilling within specific parameter ranges.As the weight on bit increased,both the average torque and total specificenergy first decreased and then increased.With rising rotating speed,the average torque exhibited a trend of initial increase,then decrease,and finalincrease,whereas the total specificenergy increased slowly at firstand then sharply.Both parameters exhibited optimal values at which the average torque and total specific energy remained at minimal levels.For granite combined drilling,the optimal performance was achieved at a laser power of 3000 W,irradiation time of 31 s,the weight on bit of 2.4 kN,and the rotating speed of 97 r/min.
基金Project(9140A12060110BQ03)supported by the National Key Laboratory of Science and Technology on Materials under Shock and Impact,China
文摘Electroless copper plating on diamond particles precoated with 1%Cr was carried out to evaluate the effects of various experimental parameters on coating quality and deposition rate to obtain the optimized reaction parameters. The formulated samples under optimized parameters were characterized by X-ray diffraction, scanning electron microscopy, energy dispersive spectroscopy, X-ray photoelectron spectra and optical microscopy. The best parameters, where uniform and maximum coating thickness was achieved, are etching with 20%NaOH for 30 min, sensitization and activation with SnCl2 and PdCl2 for 5 and 20 min, respectively. The composition of the copper solution bath was 16 g/L CuSO4＆#183;5H2O, 35 mL/L formaldehyde （HCHO）, 23 g/L KNaC4H4O6 at 60 ℃, pH=13 and stirring at （350±15） r/min under ultrasonication.
