Heteroclitin D （H.D） was successfully isolated from Kadsurae Caulis by using flash chromatography and recrystalllzed by methanol, 10.2 mg of H.D was obtained from 4.86 g of crude extract, and the purity determined b...Heteroclitin D （H.D） was successfully isolated from Kadsurae Caulis by using flash chromatography and recrystalllzed by methanol, 10.2 mg of H.D was obtained from 4.86 g of crude extract, and the purity determined by HPLC was 99.4%. The structure was identified by UV, IR, MS, and NMR analysis. The fast, simple and efficient method can be applied to the preparation of reference substance of H. D.展开更多
In this study, a new parameter, S phase cell percentage （S fraction） normalized BrdU （SFN-BrdU） incorporation rate, was introduced to detect $ arrest. The results showed a positive linear correlation between the B...In this study, a new parameter, S phase cell percentage （S fraction） normalized BrdU （SFN-BrdU） incorporation rate, was introduced to detect $ arrest. The results showed a positive linear correlation between the BrdU incorporation rate and the S fraction in unperturbed 16HBE cells. Theoretical analysis indicated that only S arrest could result in a decrease in the SFN-BrdU incorporation rate. Additionally, the decrease in SFN-BrdU incorporation rate and the activation of DNA damage checkpoints further demonstrated that S arrest was induced by diethyl sulfate treatment of 16HBE cells. In conclusion, $FN-BrdU incorporation rate can be used to detecting S arrest.展开更多
Simultaneous quantification of Lamivudine and Zidovudine in tablets by HPTLC method was developed and validated.The chromatograms were developed using a mobile phase of toluene:ethyl acetate:methanol (4:4:2,v/v/v) on ...Simultaneous quantification of Lamivudine and Zidovudine in tablets by HPTLC method was developed and validated.The chromatograms were developed using a mobile phase of toluene:ethyl acetate:methanol (4:4:2,v/v/v) on pre-coated plate of silica gel GF aluminum TLC plate and quantified by densitometric absorbance mode at 276 nm.The R f values were 0.4170.03 and 0.6070.04 for Lamivudine and Zidovudine,respectively.The linearity of the method was found to be within the concentration range of 50 250 ng/spot for Lamivudine and for Zidovudine,it was 100 500 ng/spot.The lower limits of detection and quantification were 2.23 ng/spot and 7.90 ng/spot for Lamivudine and 2.90 ng/spot and 8.85 ng/spot for Zidovudine.The method was also validated for precision,specificity and recovery.This developed method was used to analyze fixed-dose tablets (Duovir,Cipla Ltd) samples of Lamivudine and Zidovudine.展开更多
Irregular phase-space orbits of the electrons are harmful to the electron-beam transport quality and hence deteriorate the performance of a free-electron laser （FEL）. In previous literature, it was demonstrated that...Irregular phase-space orbits of the electrons are harmful to the electron-beam transport quality and hence deteriorate the performance of a free-electron laser （FEL）. In previous literature, it was demonstrated that the irregularity of the electron phase-space orbits could be caused in several ways, such as varying the wiggler amplitude and inducing sidebands. Based on a Hamiltonian model with a set of self-consistent differential equations, it is shown in this paper that the electron- beam normalized plasma frequency functions not only couple the electron motion with the FEL wave, which results in the evolution of the FEL wave field and a possible power saturation at a large beam current, but also cause the irregularity of the electron phase-space orbits when the normalized plasma frequency has a sufficiently large value, even if the initial energy of the electron is equal to the synchronous energy or the FEL wave does not reach power saturation.展开更多
An attempt has been made to apply the wavelet methodology for the study of the results of the chaotic behavior of multiparticle production in relativistic heavy ion collisions. We reviewed the data that describes the ...An attempt has been made to apply the wavelet methodology for the study of the results of the chaotic behavior of multiparticle production in relativistic heavy ion collisions. We reviewed the data that describes the collisions of relativistic heavy ion for the case η-space in 1-D phase space of variable. We compared the experimental data and UrQMD data using wavelet coherency. We discussed the results of the comparison.展开更多
The interaction parameters for various phases in the Ti-W and Pd-W systems were calcula- ted using phase diagram information by means of a numerical procedure.The approach differs significantly from the trial and erro...The interaction parameters for various phases in the Ti-W and Pd-W systems were calcula- ted using phase diagram information by means of a numerical procedure.The approach differs significantly from the trial and error method and has the advantage of being very robust in the sense that one can make full use of the accurate experimental phase diagram data and deal with situations which are difficult or even impossible for the trial and error method. Using calculated parameters and lattice stability values for Ti,W and Pd given in literature, the diagrams of the above systems were recalcula- ted.The results are in good agreement with experimental information.展开更多
We applied the wavelet methodology for our earlier published research work of the chaotic behavior so called multiplicity fluctuations of secondary charged particles produced during the nucleus-nucleus (A-A) collision...We applied the wavelet methodology for our earlier published research work of the chaotic behavior so called multiplicity fluctuations of secondary charged particles produced during the nucleus-nucleus (A-A) collisions at an energy of the order of ≈ 409 GeV in a new fashion. We illustrated the wavelet coherency in a relation of chaotic behavior for above said data of secondary charged pions in different phase spaces of collisions such as: η-space, φ-space (in one dimension) and ηφ-space (in two dimensions) respectively. We have shown the changes in the wavelet coherence when there are different values of two parameters “q” and “p”. We discussed our new results for the comparison purpose and findings were in the good agreements.展开更多
The phase dependence and independence of the response of a trichromatieally driven two-level medium to an arbitrarily intense probe field have been studied. The sum of the relative phases of the sideband components of...The phase dependence and independence of the response of a trichromatieally driven two-level medium to an arbitrarily intense probe field have been studied. The sum of the relative phases of the sideband components of the trichromatic field compared to the central component plays a crucial role in the response of the medium. For a weak probe field, as the sum of the relative phases changes from 0 to π, multiple switching can be achieved, in which switching from normal to anomalous dispersion occurs in multiple separate frequency regimes. The remarkable dependence on the sum phase is also shown for a strong probe field. On the other hand, when the sum of the two relative phases is fixed, the changes in the respective phases have no influence on the response of the medium.展开更多
The effects of rotation and gravity on an electro-magneto-thermoelastic medium with diffusion and voids in a generalized thermoplastic half-space are studied by using the Lord-Shulman (L-S) model and the dual-phase-la...The effects of rotation and gravity on an electro-magneto-thermoelastic medium with diffusion and voids in a generalized thermoplastic half-space are studied by using the Lord-Shulman (L-S) model and the dual-phase-lag (DPL) model. The analytical solutions for the displacements, stresses, temperature, diffusion concentration, and volume fraction field with different values of the magnetic field, the rotation, the gravity, and the initial stress are obtained and portrayed graphically. The results indicate that the effects of gravity, rotation, voids, diffusion, initial stress, and electromagnetic field are very pronounced on the physical properties of the material.展开更多
Dynamical quantum phase transitions(DQPTs),characterized by non-analytic behavior in rate function and abrupt changes in dynamic topological order parameters(DTOPs)over time,have garnered enormous attention in recent ...Dynamical quantum phase transitions(DQPTs),characterized by non-analytic behavior in rate function and abrupt changes in dynamic topological order parameters(DTOPs)over time,have garnered enormous attention in recent decades.However,in non-Hermitian systems,the special biorthogonality of the bases makes the definition of DQPTs complex.In this work,we delve into the comprehensive investigation of self-normal DQPTs(originally used in Hermitian systems)to compare them with their biorthogonal counterpart,within the context of non-Hermitian quantum walks(QWs).We present a detailed analysis of the behaviors of Loschmidt rate functions and DTOPs under these two distinct theoretical approaches.While both self-normal and biorthogonal methods can be used to detect DQPTs in quench dynamics between different topological phases,we theoretically present their differences in the definition of critical momenta and critical times by analyzing the Fisher zeros and fixed points.Finally,we present an experiment that observes both types of DQPTs using one-dimensional discrete-time QWs with single photons.展开更多
基金supported by the International Scientific and Technological Cooperation Program of China(No:2009DFA31230)the Industry-University-Research Cooperation Program from Science and Technology Department of Qingyuang City(No:2012D021211001)
文摘Heteroclitin D （H.D） was successfully isolated from Kadsurae Caulis by using flash chromatography and recrystalllzed by methanol, 10.2 mg of H.D was obtained from 4.86 g of crude extract, and the purity determined by HPLC was 99.4%. The structure was identified by UV, IR, MS, and NMR analysis. The fast, simple and efficient method can be applied to the preparation of reference substance of H. D.
基金supported by the National Nature Science Foundation of China(Nos.81370079 and 81001253)the Beijing Natural Science Foundation(No.7132122)
文摘In this study, a new parameter, S phase cell percentage （S fraction） normalized BrdU （SFN-BrdU） incorporation rate, was introduced to detect $ arrest. The results showed a positive linear correlation between the BrdU incorporation rate and the S fraction in unperturbed 16HBE cells. Theoretical analysis indicated that only S arrest could result in a decrease in the SFN-BrdU incorporation rate. Additionally, the decrease in SFN-BrdU incorporation rate and the activation of DNA damage checkpoints further demonstrated that S arrest was induced by diethyl sulfate treatment of 16HBE cells. In conclusion, $FN-BrdU incorporation rate can be used to detecting S arrest.
文摘Simultaneous quantification of Lamivudine and Zidovudine in tablets by HPTLC method was developed and validated.The chromatograms were developed using a mobile phase of toluene:ethyl acetate:methanol (4:4:2,v/v/v) on pre-coated plate of silica gel GF aluminum TLC plate and quantified by densitometric absorbance mode at 276 nm.The R f values were 0.4170.03 and 0.6070.04 for Lamivudine and Zidovudine,respectively.The linearity of the method was found to be within the concentration range of 50 250 ng/spot for Lamivudine and for Zidovudine,it was 100 500 ng/spot.The lower limits of detection and quantification were 2.23 ng/spot and 7.90 ng/spot for Lamivudine and 2.90 ng/spot and 8.85 ng/spot for Zidovudine.The method was also validated for precision,specificity and recovery.This developed method was used to analyze fixed-dose tablets (Duovir,Cipla Ltd) samples of Lamivudine and Zidovudine.
基金Project supported by the Science Foundation of Department of Education of Sichuan Province,China (Grant No.12233454)the Youth Foundation of Department of Education of Sichuan Province,China (Grant No.10ZB080)the Xihua University Foundation,China (Grant No.Z0913306)
文摘Irregular phase-space orbits of the electrons are harmful to the electron-beam transport quality and hence deteriorate the performance of a free-electron laser （FEL）. In previous literature, it was demonstrated that the irregularity of the electron phase-space orbits could be caused in several ways, such as varying the wiggler amplitude and inducing sidebands. Based on a Hamiltonian model with a set of self-consistent differential equations, it is shown in this paper that the electron- beam normalized plasma frequency functions not only couple the electron motion with the FEL wave, which results in the evolution of the FEL wave field and a possible power saturation at a large beam current, but also cause the irregularity of the electron phase-space orbits when the normalized plasma frequency has a sufficiently large value, even if the initial energy of the electron is equal to the synchronous energy or the FEL wave does not reach power saturation.
文摘An attempt has been made to apply the wavelet methodology for the study of the results of the chaotic behavior of multiparticle production in relativistic heavy ion collisions. We reviewed the data that describes the collisions of relativistic heavy ion for the case η-space in 1-D phase space of variable. We compared the experimental data and UrQMD data using wavelet coherency. We discussed the results of the comparison.
文摘The interaction parameters for various phases in the Ti-W and Pd-W systems were calcula- ted using phase diagram information by means of a numerical procedure.The approach differs significantly from the trial and error method and has the advantage of being very robust in the sense that one can make full use of the accurate experimental phase diagram data and deal with situations which are difficult or even impossible for the trial and error method. Using calculated parameters and lattice stability values for Ti,W and Pd given in literature, the diagrams of the above systems were recalcula- ted.The results are in good agreement with experimental information.
文摘We applied the wavelet methodology for our earlier published research work of the chaotic behavior so called multiplicity fluctuations of secondary charged particles produced during the nucleus-nucleus (A-A) collisions at an energy of the order of ≈ 409 GeV in a new fashion. We illustrated the wavelet coherency in a relation of chaotic behavior for above said data of secondary charged pions in different phase spaces of collisions such as: η-space, φ-space (in one dimension) and ηφ-space (in two dimensions) respectively. We have shown the changes in the wavelet coherence when there are different values of two parameters “q” and “p”. We discussed our new results for the comparison purpose and findings were in the good agreements.
基金Project supported by the National Natural Science Foundation of China （Grant No 60378008）.
文摘The phase dependence and independence of the response of a trichromatieally driven two-level medium to an arbitrarily intense probe field have been studied. The sum of the relative phases of the sideband components of the trichromatic field compared to the central component plays a crucial role in the response of the medium. For a weak probe field, as the sum of the relative phases changes from 0 to π, multiple switching can be achieved, in which switching from normal to anomalous dispersion occurs in multiple separate frequency regimes. The remarkable dependence on the sum phase is also shown for a strong probe field. On the other hand, when the sum of the two relative phases is fixed, the changes in the respective phases have no influence on the response of the medium.
文摘The effects of rotation and gravity on an electro-magneto-thermoelastic medium with diffusion and voids in a generalized thermoplastic half-space are studied by using the Lord-Shulman (L-S) model and the dual-phase-lag (DPL) model. The analytical solutions for the displacements, stresses, temperature, diffusion concentration, and volume fraction field with different values of the magnetic field, the rotation, the gravity, and the initial stress are obtained and portrayed graphically. The results indicate that the effects of gravity, rotation, voids, diffusion, initial stress, and electromagnetic field are very pronounced on the physical properties of the material.
基金supported by the National Key R&D Program of China(Grant No.2023YFA1406701)National Natural Science Foundation of China(Grants No.12025401,92265209,12474352,92476106,and 12088101)Kunkun Wang and Lei Xiao acknowledge support from Beijing National Laboratory for Condensed Matter Physics(No.2024BNLCMPKF010).
文摘Dynamical quantum phase transitions(DQPTs),characterized by non-analytic behavior in rate function and abrupt changes in dynamic topological order parameters(DTOPs)over time,have garnered enormous attention in recent decades.However,in non-Hermitian systems,the special biorthogonality of the bases makes the definition of DQPTs complex.In this work,we delve into the comprehensive investigation of self-normal DQPTs(originally used in Hermitian systems)to compare them with their biorthogonal counterpart,within the context of non-Hermitian quantum walks(QWs).We present a detailed analysis of the behaviors of Loschmidt rate functions and DTOPs under these two distinct theoretical approaches.While both self-normal and biorthogonal methods can be used to detect DQPTs in quench dynamics between different topological phases,we theoretically present their differences in the definition of critical momenta and critical times by analyzing the Fisher zeros and fixed points.Finally,we present an experiment that observes both types of DQPTs using one-dimensional discrete-time QWs with single photons.
