We report rigorous coupled-wave analysis(RCWA) method to non-destructively characterize the domain structure of periodically poled lithium niobate(PPLN) crystal. The strong light diffraction effect is achieved by appl...We report rigorous coupled-wave analysis(RCWA) method to non-destructively characterize the domain structure of periodically poled lithium niobate(PPLN) crystal. The strong light diffraction effect is achieved by applying a proper external voltage. We can observe reversed domain pattern and employ the detected diffraction intensity to optimally fit the result of RCWA based on least square method. Compared with conventional scalar diffraction theory, more accurate domain structure parameters with accuracies of 0.05 μm and 0.005 for the period and duty cycle are obtained respectively. It is proved that accurate, real-time and nondestructive characterization can be realized via this method.展开更多
To address the difficulty in testing and calibrating the stress gradient in the depth direction of mechanical components, a new technology of nondestructive testing and characterization of the residual stress gradient...To address the difficulty in testing and calibrating the stress gradient in the depth direction of mechanical components, a new technology of nondestructive testing and characterization of the residual stress gradient field by ultrasonic method is proposed based on acoustoelasticity theory. By carrying out theoretical analysis, the sensitivity coefficients of different types of ultrasonic are obtained by taking the low carbon steel(12%C) as a research object. By fixing the interval distance between sending and receiving transducers, the mathematical expressions of the change of stress and the variation of time are established. To design one sending-one receiving and oblique incidence ultrasonic detection probes, according to Snell law, the critically refracted longitudinal wave(LCR wave) is excited at a certain depth of the fixed distance of the tested components. Then, the relationship between the depth of LCR wave detection and the center frequency of the probe in Q235 steel is obtained through experimental study. To detect the stress gradient in the depth direction, a stress gradient LCR wave detection model is established, through which the stress gradient formula is derived by the relationship between center frequency and detecting depth. A C-shaped stress specimen of Q235 steel is designed to conduct stress loading tests, and the stress is measured with the five group probes at different center frequencies. The accuracy of ultrasonic testing is verified by X-ray stress analyzer. The stress value of each specific depth is calculated using the stress gradient formula. Accordingly, the ultrasonic characterization of residual stress field is realized. Characterization results show that the stress gradient distribution is consistent with the simulation in ANSYS. The new technology can be widely applied in the detection of the residual stress gradient field caused by mechanical processing, such as welding and shot peening.展开更多
At present,two-dimensional(2D)materials have shown great application potential in numerous fields based on their physical chemical and electronic properties.Raman spectroscopy and de-rivative techniques are effective ...At present,two-dimensional(2D)materials have shown great application potential in numerous fields based on their physical chemical and electronic properties.Raman spectroscopy and de-rivative techniques are effective tools for characterizing 2D materials.Raman spectroscopy conveys lots of knowledge on 2D materials,including layer number,doping type,strain and interlayer coupling.This review summarized advanced applications of Raman spectroscopy in 2D materials.The challenges and possible applied directions of Raman spectroscopy to 2D materials are discussed in detail.展开更多
基金supported by the National High Technology Research and Development Program of China(No.2013AA030501)
文摘We report rigorous coupled-wave analysis(RCWA) method to non-destructively characterize the domain structure of periodically poled lithium niobate(PPLN) crystal. The strong light diffraction effect is achieved by applying a proper external voltage. We can observe reversed domain pattern and employ the detected diffraction intensity to optimally fit the result of RCWA based on least square method. Compared with conventional scalar diffraction theory, more accurate domain structure parameters with accuracies of 0.05 μm and 0.005 for the period and duty cycle are obtained respectively. It is proved that accurate, real-time and nondestructive characterization can be realized via this method.
基金Supported by National Natural Science Foundation of China(Grant No.51275042)
文摘To address the difficulty in testing and calibrating the stress gradient in the depth direction of mechanical components, a new technology of nondestructive testing and characterization of the residual stress gradient field by ultrasonic method is proposed based on acoustoelasticity theory. By carrying out theoretical analysis, the sensitivity coefficients of different types of ultrasonic are obtained by taking the low carbon steel(12%C) as a research object. By fixing the interval distance between sending and receiving transducers, the mathematical expressions of the change of stress and the variation of time are established. To design one sending-one receiving and oblique incidence ultrasonic detection probes, according to Snell law, the critically refracted longitudinal wave(LCR wave) is excited at a certain depth of the fixed distance of the tested components. Then, the relationship between the depth of LCR wave detection and the center frequency of the probe in Q235 steel is obtained through experimental study. To detect the stress gradient in the depth direction, a stress gradient LCR wave detection model is established, through which the stress gradient formula is derived by the relationship between center frequency and detecting depth. A C-shaped stress specimen of Q235 steel is designed to conduct stress loading tests, and the stress is measured with the five group probes at different center frequencies. The accuracy of ultrasonic testing is verified by X-ray stress analyzer. The stress value of each specific depth is calculated using the stress gradient formula. Accordingly, the ultrasonic characterization of residual stress field is realized. Characterization results show that the stress gradient distribution is consistent with the simulation in ANSYS. The new technology can be widely applied in the detection of the residual stress gradient field caused by mechanical processing, such as welding and shot peening.
基金financial support from Natural Science Foundation of China(61605134)Basic Sichuan Applied Research Project(2019YJ0078)the Innovative Spark Project of Sichuan University(2018SCUH0043)
文摘At present,two-dimensional(2D)materials have shown great application potential in numerous fields based on their physical chemical and electronic properties.Raman spectroscopy and de-rivative techniques are effective tools for characterizing 2D materials.Raman spectroscopy conveys lots of knowledge on 2D materials,including layer number,doping type,strain and interlayer coupling.This review summarized advanced applications of Raman spectroscopy in 2D materials.The challenges and possible applied directions of Raman spectroscopy to 2D materials are discussed in detail.