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Macro-micro tests of cohesive soil under varied normal and shear stresses subjected to drying-wetting cycles 被引量:1
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作者 Fangyue Luo Ga Zhang Yangping Yao 《Journal of Rock Mechanics and Geotechnical Engineering》 2025年第9期5893-5905,共13页
The mechanical behavior of cohesive soil is sensitized to drying-wetting cycles under confinements.However,the hydromechanical coupling effect has not been considered in current constitutive models.A macro-micro analy... The mechanical behavior of cohesive soil is sensitized to drying-wetting cycles under confinements.However,the hydromechanical coupling effect has not been considered in current constitutive models.A macro-micro analysis scheme is proposed in this paper to investigate the soil deformation behavior under the coupling of stress and drying-wetting cycles.A new device is developed based on CT(computerized tomography)workstation to apply certain normal and shear stresses on a soil specimen during drying-wetting cycles.A series of tests are conducted on a type of loess with various coupling of stress paths and drying-wetting cycles.At macroscopic level,stress sensor and laser sensor are used to acquire stress and strain,respectively.The shear and volumetric strain increase during the first few drying-wetting cycles and then become stable.The increase of the shear stress level or confining pressure would cause higher increase rate and the value of shear strain in the process of drying-wetting cycles.At microscopic level,the grayscale value(GSV)of CT scanning image is characterized as the proportion of soil particles to voids.A fabric state parameter is proposed to characterize soil microstructures under the influence of stress and drying-wetting cycle.Test results indicate that the macroand micro-responses show high consistence and relevance.The stress and drying-wetting cycles would both induce collapse of the soil microstructure,which dominants degradation of the soil mechanical properties.The evolution of the macro-mechanical property of soil exhibits a positive linear relationship with the micro-evolution of the fabric state parameter. 展开更多
关键词 Cohesive soil Drying-wetting cycle Coupled loading Macro and micro test FABRIC
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基于原位动态Micro CT的针刺预制体结构表征及工艺改进
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作者 张文奇 任志鹏 +4 位作者 邹艳玲 耿巍麟 陈伟 王孝锋 蒋云 《棉纺织技术》 2026年第3期42-47,共6页
采用原位动态Micro CT技术对某梯度密度针刺预制体进行无损检测与分析,通过高分辨率扫描和三维重构技术,实现了材料内部三维组织结构的精确表征,并定量统计了针刺纤维束的长度、直径等参数。结果表明:原工艺加工的产品均匀性存在缺陷;... 采用原位动态Micro CT技术对某梯度密度针刺预制体进行无损检测与分析,通过高分辨率扫描和三维重构技术,实现了材料内部三维组织结构的精确表征,并定量统计了针刺纤维束的长度、直径等参数。结果表明:原工艺加工的产品均匀性存在缺陷;结合统计数据,对织物层间及面内针刺工艺参数优化后,针刺纤维束平均直径提升约36%,表明纤维间的结合更加紧密;针刺纤维束长度下降约6%,说明纤维分布更加均匀。认为:通过原位动态Micro CT技术优化针刺工艺,可实现从结构表征到工艺改进的闭环优化,具有重要的工程应用价值。 展开更多
关键词 原位动态micro CT 预制体 无损检测 三维结构 针刺均匀性 针刺纤维束
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ISOLATION DESIGN AND SIMULATIONAL EXPERIMENT OF NANOMETER MICRO MOVEMENT TEST-BED
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作者 吴晓琳 刘平成 +1 位作者 杨圣 杨晓红 《Transactions of Nanjing University of Aeronautics and Astronautics》 EI 2001年第2期200-205,共6页
The relation of mass, stiffness and rate of damping is obtained by using the mechanical analysis of the obstructive vibration system of two dimensions for the design of the obstructive vibration system of more freedom... The relation of mass, stiffness and rate of damping is obtained by using the mechanical analysis of the obstructive vibration system of two dimensions for the design of the obstructive vibration system of more freedom and the micro vibration test bed. The result of stimulational experiment indicates that the isolation of vibration of this system is satisfactory. The design method of vibration can be used as the reference to ultra precision machine tool, super micro orientation machanism and so on. 展开更多
关键词 nanometer (NM) micro vibration test bed isolation of vibration simulation transmission quotiety
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Measurement of Ca^(2+) Flow in Cochlear Cells Using Non-Invasive Micro-Test Technique 被引量:1
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作者 CHEN Shi-qin YU Ning +2 位作者 YE Sheng-nan YANG Shi-ming ZHAI Suo-qiang 《Journal of Otology》 2010年第2期90-96,共7页
Objective To test Calcium ion(Ca2+) flow at the head and end of outer hair cells(OHCs) in resting state and in response to Nimodipine treatment.Methods Non-invasive micro-test techniques were used to study Ca2+ in iso... Objective To test Calcium ion(Ca2+) flow at the head and end of outer hair cells(OHCs) in resting state and in response to Nimodipine treatment.Methods Non-invasive micro-test techniques were used to study Ca2+ in isolated OHCs in adult guinea pigs.Results Four types of Ca2+ transport were identified in OHCs on basilar membrane tissue fragments:influx at the head of with efflux at the bottom(type 1):efflux at the head of OHCs with influx at the bottom(type 2);influx at the both head and bottom(type 3);and efflux at the both head and bottom(type 4).However,only type 1 and type 3 of Ca2+ ion transport were detected in the cochlea.We propose that Ca2+ ion transport exists in adult guinea pig cochlear OHCs in resting state and is variable.Ca2 + flow in OHC can be inhibited by Nimodipine in resting state. 展开更多
关键词 Guinea pig outer hair cells Ca2+ ion non-invasive micro-test technique nimodipine.
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Comparison of mechanical properties in welded joint for CO_2 arc welding by using the micro-shear test and impact test
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作者 Zhou Lixia Wang Shiyuan and Shi Yaowu (Xi’an Jiaotong University)L. Dorn(Technical University of Berlin) 《China Welding》 EI CAS 1995年第1期57-64,共8页
A micro shear testing method which can suit to measure the mechanical properties of heterogeneous materials is introduced, and the properties in each zone of welded joint for CO2 arc welding can be evaluated by using ... A micro shear testing method which can suit to measure the mechanical properties of heterogeneous materials is introduced, and the properties in each zone of welded joint for CO2 arc welding can be evaluated by using this method in this paper. Moreover, these results are compared with those results of Charpy V-notch impact test and their correlation is discussed. 展开更多
关键词 mechanical properties micro shear test CO_2 arc welding WELDED
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Elastic modulus of claystone evaluated by nano-/micro-indentation tests and meso-compression tests 被引量:5
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作者 Christophe Auvray Noémie Lafrance Danièle Bartier 《Journal of Rock Mechanics and Geotechnical Engineering》 SCIE CSCD 2017年第1期84-91,共8页
Toarcian claystone such as that of the Callovo-Oxfordian is a qualified multiphase material. The claystone samples tested in this study are composed of four main mineral phases: silicates(clay minerals, quartz,feldspa... Toarcian claystone such as that of the Callovo-Oxfordian is a qualified multiphase material. The claystone samples tested in this study are composed of four main mineral phases: silicates(clay minerals, quartz,feldspars, micas)(z86%), sulphides(pyrite)(z3%), carbonates(calcite, dolomite)(z10%) and organic kerogen(z1%). Three sets of measurements of the modulus of deformability were compared as determined in(i) nanoindentation tests with a constant indentation depth of 2 mm,(ii) micro-indentation tests with a constant indentation depth of 20 mm, and(iii) meso-compression tests with a constant displacement of 200 mm. These three experimental methods have already been validated in earlier studies. The main objective of this study is to demonstrate the influence of the scaling effect on the modulus of deformability of the material. Different frequency distributions of the modulus of deformability were obtained at the different sample scales:(i) in nano-indentation tests, the distribution was spread between 15 GPa and 90 GPa and contained one peak at34 GPa and another at 51 GPa;(ii) in the micro-indentation tests, the distribution was spread between 25 GPa and 60 GPa and displayed peaks at 26 GPa and 37 GPa; and(iii) in the meso-compression tests, a narrow frequency distribution was obtained, ranging from 25 GPa to 50 GPa and with a maximum at around 35 GPa. 展开更多
关键词 Claystone Elastic modulus Scaling effect Nano-and micro-indentation Meso-compression tests Multi-scale mechanical tests
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Vibration test of micro machined gyroscope based on high speed photography and SURF 被引量:1
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作者 姚峰林 高世桥 +1 位作者 赵婕 高崇仁 《Journal of Beijing Institute of Technology》 EI CAS 2012年第2期179-184,共6页
Based on three kinds of dynamic test of MEMS, a dynamic system for the vibration test of micro machined gyroscope based on high speed photography is introduced. Firstly, the architecture of the system hardware is intr... Based on three kinds of dynamic test of MEMS, a dynamic system for the vibration test of micro machined gyroscope based on high speed photography is introduced. Firstly, the architecture of the system hardware is introduced. Secondly, the image tracking performance is compared by the test using the template matching algorithm, the mean shift algorithm and the SURF algorithm. The vibration curve shows that high speed photograph combined with SURF algorithm is faster, more ac- curate, and more suitable for the vibration test of micro machined gyroscope. After the frequency a- nalysis and related interpolation, more characteristics of micro gyroscope can be obtained. 展开更多
关键词 high speed photograph SURF micro machined gyroscope dynamic test VIBRATION IMAGE
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Micro-Doppler effect testing technique for attitude of projectile in space flight
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作者 张万君 吴晓颖 +2 位作者 张晓炜 牛敏杰 冷雪冰 《Journal of Beijing Institute of Technology》 EI CAS 2013年第3期350-353,共4页
To measure projectile attitude in space flight, based on continuous wave (CW) radar, a new micro-Doppler effect testing technique is developed in this paper. It also establishes radar testing model for attitude of f... To measure projectile attitude in space flight, based on continuous wave (CW) radar, a new micro-Doppler effect testing technique is developed in this paper. It also establishes radar testing model for attitude of flying projectile and resolve micro-Doppler effect of projectile motion attitude. By distinguishing and geting attitude parameters such as micro-motion period, this technique can in- tuitively estimate the flight stability of projectile, and the validity of this technique is proved accord- ing to flight tests. 展开更多
关键词 attitude of projectile micro-DOPPLER radar testing target micro-motion
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China,America Have Coo[erated in Micro Biological Production Test
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作者 Hou Fu 《China Oil & Gas》 CAS 1996年第3期189-189,共1页
China,AmericaHaveCooperatedinMicrobiologicalProductionTestHouFuThemicrobiologicalproductiontechnologyhasbeen... China,AmericaHaveCooperatedinMicrobiologicalProductionTestHouFuThemicrobiologicalproductiontechnologyhasbeenintroducedfromthe... 展开更多
关键词 China America Have Coo[erated in micro Biological Production test
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Salt spray corrosion test of micro-plasma oxidation ceramic coatings on Ti alloy 被引量:3
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作者 HAO Guodong YAO Zhongping JIANG Zhaohua 《Rare Metals》 SCIE EI CAS CSCD 2007年第6期560-564,共5页
Ceramic coatings were prepared on Ti-6Al-4V alloy in NaAlO2 solution by micro-plasma oxidation (MPO). The salt spray tests of the coated samples and the substrates were carded out in a salt spray test machine. The p... Ceramic coatings were prepared on Ti-6Al-4V alloy in NaAlO2 solution by micro-plasma oxidation (MPO). The salt spray tests of the coated samples and the substrates were carded out in a salt spray test machine. The phase composition and surface morphology of the coatings were investigated by XRD and SEAM. Severe corrosion occurred on the substrate surface, while there were no obvious corrosion phenomena on the coated samples. The coatings were composed of Al2TiO5 and a little α-Al2O3 and mille TiO2, and the salt spray test did not change the composition of the coatings. The weight loss rate of the coatings decreased with increasing MPO time because of the increase in density and thickness of the coatings. The surface morphology of the coatings was influenced by salt spray corrosion test. Among the coated samples, the coating prepared for 2 h has the best corrosion resistance under salt spray test. 展开更多
关键词 micro-plasma oxidation ceramic coating salt spray corrosion test Ti alloy
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Experimental Tests on a Pre-Heated Combustion Chamber for Ultra Micro Gas Turbine Device: Air/Fuel Ratio Evaluation
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作者 Roberto Capata Kliton Kylykbashi +1 位作者 Alfonso Calabria Mario Di Veroli 《Engineering(科研)》 2016年第11期789-805,共17页
Current portable power generators are mainly based on internal combustion engine since they present higher values of efficiency comparing to other engines;the main reason why internal combustion engine is not convenie... Current portable power generators are mainly based on internal combustion engine since they present higher values of efficiency comparing to other engines;the main reason why internal combustion engine is not convenient for micro power generation (5 - 30 kW) is because of their heaviness. Micro and ultra micro gas turbine devices, based on a micro compressor and a micro turbine installed on the same shaft, are more suitable for this scope for several reasons. Micro turbine systems have many advantages over reciprocating engine generators, such as higher power density (with respect to size and weight), extremely low emissions and few, or just one, moving part. Those designed with foil bearings and air-cooling operate without oil, coolants or other hazardous materials. Micro turbines also have the advantage of having the majority of their waste heat contained in their relatively high temperature exhaust. Micro turbines offer several potential advantages compared to other technologies for small-scale power generation, including: a small number of moving parts, compact size, lightweight, greater efficiency, lower emissions, lower electricity costs, and opportunities to utilize waste fuels. The object of this study is the experimental tests on a stand-alone gas turbine device with a pre-heated combustion chamber (CC), to validate the fuel consumption reduction, compared to an actual and commercial device, used on air models. 展开更多
关键词 Experimental tests Combustion Chamber Ultra micro Gas Turbine Fuel Consumption
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表皮生长因子受体变异体Ⅲ型促进胶质瘤细胞钙离子外流
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作者 介子元 崔中亮 +4 位作者 徐孟辉 李冠璋 闫旭 张伟 师忠芳 《中国微侵袭神经外科杂志》 2026年第2期109-114,共6页
目的探讨表皮生长因子受体变异体Ⅲ型(epidermal growth factor receptor variantⅢ,EGFRvⅢ)对胶质瘤细胞Ca^(2+)跨膜流动的影响,及其与替莫唑胺(temozolomide,TMZ)耐药的关系。方法构建稳定转染EGFRvⅢ的U87和LN229胶质瘤细胞株,分别... 目的探讨表皮生长因子受体变异体Ⅲ型(epidermal growth factor receptor variantⅢ,EGFRvⅢ)对胶质瘤细胞Ca^(2+)跨膜流动的影响,及其与替莫唑胺(temozolomide,TMZ)耐药的关系。方法构建稳定转染EGFRvⅢ的U87和LN229胶质瘤细胞株,分别采用免疫荧光染色、实时荧光定量PCR(qRT-PCR)及Western blotting验证EGFRvⅢ蛋白和mRNA表达情况。运用非损伤微测技术(non-invasive micro-test technique,NMT)检测细胞Ca^(2+)跨膜流动特征。结果与未转染EGFRvⅢ组相比,转染EGFRvⅢ的U87及LN229细胞中EGFRvⅢ呈显著阳性免疫荧光信号,且qRT-PCR及Western blotting检测显示其mRNA及蛋白水平均明显升高(均P<0.001),提示转染成功。NMT检测结果显示:未转染EGFRvⅢ组U87及LN229细胞主要表现为Ca^(2+)内流;而转染EGFRvⅢ组细胞Ca^(2+)跨膜流动方向由内流转变为外排。结论EGFRvⅢ表达可显著改变胶质瘤细胞Ca^(2+)跨膜流动模式(由内流转为外排),提示EGFRvⅢ可能通过促进细胞Ca^(2+)离子外流参与胶质瘤TMZ耐药。 展开更多
关键词 神经胶质瘤 表皮生长因子受体变异体Ⅲ型 非损伤微测技术 钙离子
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CO_(2)-工业废渣协同固化渣土多尺度试验研究
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作者 朱剑锋 汪正清 +3 位作者 陶燕丽 龚晓南 夏亚宁 李挺 《工程科学学报》 北大核心 2026年第3期504-516,共13页
为实现工程渣土的高效固化并资源化利用,以纯工业废渣—WZ01为主固化剂,电石渣(CCR)为碱性激发剂,结合CO_(2)碳化技术,采用微观-单元体-模型多尺度试验研究CO_(2)-CCR-WZ01协同固化渣土的可行性,通过开展无侧限抗压强度试验与CO_(2)吸... 为实现工程渣土的高效固化并资源化利用,以纯工业废渣—WZ01为主固化剂,电石渣(CCR)为碱性激发剂,结合CO_(2)碳化技术,采用微观-单元体-模型多尺度试验研究CO_(2)-CCR-WZ01协同固化渣土的可行性,通过开展无侧限抗压强度试验与CO_(2)吸收率测定试验来分析通碳时间(T_(c))、碳化温度(K_(c))、通碳压强(P_(c))、CO_(2)浓度(W_(c))四种因素对碳化效果的影响规律,并结合微观与模型试验探究CO_(2)-WZ01-CCR固化土的微观演变规律,从多尺度角度评价CO_(2)-CCR-WZ01协同固化技术的固化效果.结果表明:在T_(c)=6 h、K_(c)=60℃,、P_(c)=600 kPa、W_(c)=50%时,渣土的碳化效果最佳;在碳化-固化反应的内外协同作用下,生成的方解石、C-A-H、C-S-H等产物可以有效填充孔隙,提高渣土强度;CO_(2)-CCR-WZ01协同作用下碳化土的贯入指数最低,承载力达到700 kPa,土体物理力学性质得到显著提升.CO_(2)-CCR-WZ01协同固化技术具有高效、低碳、环保等特征,可在渣土资源化利用中得到广泛引用. 展开更多
关键词 渣土 碳化 无侧限抗压强度 碳吸附率 微观结构 模型试验
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某复杂地层遗址保护防渗墙渗漏的检测和加固
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作者 刘晓燕 马永华 +2 位作者 李瑛 童星 刘兴旺 《地基处理》 2026年第1期67-73,共7页
为防止地下水侵蚀遗址本体或改变遗址保护区环境的湿度,通常需要在遗址本体周围设置封闭的防渗墙来切断遗址层与外围地层的水力联系。现有防渗墙技术往往难以达到零渗漏的理想效果,因此对防渗墙进行及时有效的检测和加固十分必要。结合... 为防止地下水侵蚀遗址本体或改变遗址保护区环境的湿度,通常需要在遗址本体周围设置封闭的防渗墙来切断遗址层与外围地层的水力联系。现有防渗墙技术往往难以达到零渗漏的理想效果,因此对防渗墙进行及时有效的检测和加固十分必要。结合某复杂地层遗址展示工程防渗墙的设计、施工、检测、加固以及运营期监测,分析了在复杂地层防渗墙渗漏的可能路径,对比了抽水试验和微电流场无损检测技术对渗漏的探测效果,介绍了用于防渗墙加固的全方位高压喷射系统(MJS),并得出以下结论:微电流场无损检测技术可高效准确地指出渗漏的平面位置和深度;全方位高压喷射系统加固防渗墙效果好,扰动小;遗址层底部的隔水层性质是影响整体防渗效果的重要因素,有条件时应通过土体加固形成水平隔水层。 展开更多
关键词 防渗墙 渗漏 无损检测 遗址保护 微电流场
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高速铁路隧道音爆机理及其抑控技术研究进展
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作者 韩嘉强 马伟斌 +4 位作者 叶阳升 安哲立 田经纬 郭小雄 李卓明 《中国铁道科学》 北大核心 2026年第1期145-159,共15页
针对高速铁路隧道音爆问题,在系统梳理国内外相关研究的基础上,结合已开展的大量实车试验数据,重点分析音爆的产生过程、噪声时频域特性及其峰值传播规律,讨论音爆与微气压波的关联关系,揭示动车组、隧道和环境因素对音爆关键参数的影... 针对高速铁路隧道音爆问题,在系统梳理国内外相关研究的基础上,结合已开展的大量实车试验数据,重点分析音爆的产生过程、噪声时频域特性及其峰值传播规律,讨论音爆与微气压波的关联关系,揭示动车组、隧道和环境因素对音爆关键参数的影响机制,并分析改变隧道洞口缓冲结构、增设隧道内辅助坑道、敷设吸声轨道板和增设道床石砟等措施对音爆和微气压波的缓解效果,为高速铁路隧道音爆问题的深化研究提出研究思路和建议。结果表明:压缩波在隧道内激化形成弱激波是诱发音爆的直接原因;音爆为中低频噪声,具有突发性强、持续时间短的特点;音爆发生时,其A计权声压级噪声峰值通常大于60 dB(A),随着传播距离的增大,噪声峰值表现为先增后减的变化趋势;随着动车组速度增大,发生音爆的隧道临界长度不断减小,隧道内音爆噪声影响范围扩大;减小车体截面积或优化头部流线型设计参数可在一定程度上降低初始压缩波激化强度,从而提升触发音爆的临界速度,减小音爆噪声峰值;相同动车组条件下,隧道长度越长,音爆风险越高;隧道环境温度升高、压力下降、洞口空间立体角增大可有效减缓洞口微气压波峰值;通过改变隧道洞口缓冲结构型式、增设隧道内辅助坑道、敷设吸声轨道板和增设道床石砟等措施可有效减小压力梯度峰值,缓解压缩波的激化现象,减小音爆风险。 展开更多
关键词 音爆 产生机理 实车试验 微气压波 噪声特性 抑控技术
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基于人工神经网络的超微量液滴分配参数配置规律与体积预测方法研究
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作者 迟成涛 刘慧芳 +3 位作者 王文国 刘小江 许哲名 赵丁睿 《传感技术学报》 北大核心 2026年第2期295-301,共7页
微纳尺度的超微量胶液分配技术是高性能微纳封装、连接及装配制造领域迫切需求的核心技术之一,然而明确工艺参数对微液滴分配结果的作用规律,并实现对微滴尺寸与体积的准确预测,是精准调控工作参数以完成对微液滴分配体积准确控制的关... 微纳尺度的超微量胶液分配技术是高性能微纳封装、连接及装配制造领域迫切需求的核心技术之一,然而明确工艺参数对微液滴分配结果的作用规律,并实现对微滴尺寸与体积的准确预测,是精准调控工作参数以完成对微液滴分配体积准确控制的关键。本文针对课题组所研发的针转移式微量液滴分配系统,提出了一种基于人工神经网络分析点胶性能的方法。运用数值仿真方法分析移液针尖端直径、点胶距离、接触距离等加工参数对胶滴尺寸及表面质量的影响规律。并且,建立了微量液滴分配过程的神经网络预测模型,分析出实验参数对胶斑直径的相关性影响,进一步形成了工艺参数匹配方法。通过单变量实验,验证了由神经网络模型和数值仿真得到的工作参数影响规律理论结果,并通过正交实验进一步验证微量点胶神经网络经验模型的有效性和可靠性、以及工艺参数配置方法的可行性。 展开更多
关键词 微量点胶 点胶分析 人工神经网络 正交试验
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基于细菌内毒素检查法的醋酸氯己定冲洗剂的干扰消除及方法建立
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作者 蔺红伟 武雪宾 +3 位作者 唐蕾 李静娴 梁凤英 朴淑娟 《海军军医大学学报》 北大核心 2026年第2期274-278,共5页
目的建立微量鲎试剂凝胶检查法检查醋酸氯己定冲洗剂细菌内毒素限度的方法。方法依照《中国药典》2020年版四部1143细菌内毒素检查法和9251细菌内毒素检查法应用指导原则,找到消除醋酸氯己定冲洗剂凝胶法干扰因素的方法,并建立细菌内毒... 目的建立微量鲎试剂凝胶检查法检查醋酸氯己定冲洗剂细菌内毒素限度的方法。方法依照《中国药典》2020年版四部1143细菌内毒素检查法和9251细菌内毒素检查法应用指导原则,找到消除醋酸氯己定冲洗剂凝胶法干扰因素的方法,并建立细菌内毒素的微量鲎试剂凝胶检查法。结果确认用镁离子缓冲液对醋酸氯己定冲洗剂稀释2倍,再用细菌内毒素检查用水稀释至8倍,可消除其对鲎试剂凝集反应的干扰,细菌内毒素限值为0.5 EU/mL,用λ0.06 EU/mL的鲎试剂进行检测。结论本实验建立的微量鲎试剂凝胶检查法操作简单、准确性高、重复性好,适用于醋酸氯己定冲洗剂的细菌内毒素限度的检查,可以作为醋酸氯己定冲洗剂生物检查法部分的质量控制方法。 展开更多
关键词 内毒素 微量鲎试剂凝胶检查法 镁离子缓冲液 醋酸氯己定冲洗剂 干扰
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微量动态显色法检测盐酸乌拉地尔注射液细菌内毒素含量
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作者 李逢春 杨海燕 +2 位作者 王健 郭强 周继春 《中国药业》 2026年第4期101-105,共5页
目的探讨应用微量动态显色法对盐酸乌拉地尔注射液进行细菌内毒素定量检测的可行性。方法使用微量动态显色法鲎试剂,进行细菌内毒素标准曲线可靠性检测,通过干扰试验确定不干扰浓度,对6批盐酸乌拉地尔注射液进行细菌内毒素检测,并与凝... 目的探讨应用微量动态显色法对盐酸乌拉地尔注射液进行细菌内毒素定量检测的可行性。方法使用微量动态显色法鲎试剂,进行细菌内毒素标准曲线可靠性检测,通过干扰试验确定不干扰浓度,对6批盐酸乌拉地尔注射液进行细菌内毒素检测,并与凝胶法的结果比较。结果标准曲线可靠性检测范围为0.05~5.0 EU/mL,两个厂家的微量动态显色法鲎试剂回归方程分别为lgT_(1)=2.9230-0.2832 lgC_(1);lgT_(2)=2.9866-0.2229 lgC_(2),相关系数分别为-0.9996及-0.9999。使用微量动态显色法鲎试剂对盐酸乌拉地尔注射液进行细菌内毒素检测,盐酸乌拉地尔注射液稀释至0.15625 mg/mL及以下浓度时对微量动态显色法鲎试剂与细菌内毒素的凝集反应无干扰作用,回收率在50%~200%之间。6批供试品的细菌内毒素检测结果与凝胶法一致,均符合规定。结论微量动态显色法可用于盐酸乌拉地尔注射液细菌内毒素的定量检测,结果准确且灵敏度高。 展开更多
关键词 盐酸乌拉地尔注射液 微量动态显色法 定量检测 干扰试验 细菌内毒素
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水泥基渗透结晶型防水剂与微膨胀剂对混凝土抗渗透性能的提升研究
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作者 江腾寿 吴超 姜昊 《中国建筑防水》 2026年第1期10-14,共5页
为探讨防水剂与外加剂在混凝土抗渗透性能提升中的作用,设计开展掺量分级与复配方式控制下的试验对比研究,选用水泥基渗透结晶型防水剂与微膨胀剂复配,配制5组试件,分别进行抗渗压力与电通量试验。结果显示,掺量提升与复配设计有助于削... 为探讨防水剂与外加剂在混凝土抗渗透性能提升中的作用,设计开展掺量分级与复配方式控制下的试验对比研究,选用水泥基渗透结晶型防水剂与微膨胀剂复配,配制5组试件,分别进行抗渗压力与电通量试验。结果显示,掺量提升与复配设计有助于削弱混凝土内部孔隙连通性与离子渗透通道,显著增强其抗渗透性能。 展开更多
关键词 抗渗透性能 水泥基渗透结晶型防水剂 微膨胀剂 抗渗压力试验 电通量试验
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Fractal characteristics of cracks and fragments generated in unloading rockburst tests 被引量:12
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作者 Li Dejian Zhao Fei Zheng Maojiong 《International Journal of Mining Science and Technology》 SCIE EI 2014年第6期819-823,共5页
True triaxial rockburst experiments with four different unloading rates were performed on four prism specimens of granite sampled from Beishan, China. The damage evolution in the rockburst test was investigated from t... True triaxial rockburst experiments with four different unloading rates were performed on four prism specimens of granite sampled from Beishan, China. The damage evolution in the rockburst test was investigated from two aspects including fracture surface crack and fragment characteristics. The scanning electron microscopy was used to observe the micro crack information on fragment surface. Combing binarization and box counting dimensions, the fractal dimensions of cracks were obtained. Meanwhile,the fragments were collected and a sieving experiment was conducted. We weighed the fragments qualities, counted the amount of fragments and measured the fragments length, width and thickness.Utilizing four methods to calculate damage fractal dimensions of fragments, the trend of fractal value changing with unloading rates can be roughly described. It can be concluded from these experiments that the fractal dimension either for crack or for fragment holds a decreasing trend with the decreasing unloading rate, indicating a reduction of damage level. 展开更多
关键词 Unloading rockburst test Fragments Grain distribution micro crack Fractal dimension
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