Gallium nitride(GaN),as a third-generation semiconductor,is highly attractive due to its exceptional physical and chemical properties.Laser direct writing offers an efficient method for the precise processing of hard ...Gallium nitride(GaN),as a third-generation semiconductor,is highly attractive due to its exceptional physical and chemical properties.Laser direct writing offers an efficient method for the precise processing of hard and brittle materials.In this work,various types of surface microtexture were processed on GaN epilayers using a femtosecond laser with a wavelength of 1030 nm.The effects of the laser energy,singlepulse interval,number of pulses,and number of scan passes on groove machining were investigated with a view to achieving high-quality micromachining.The depth,width,surface morphology,and roughness of the grooves were analyzed using scanning electron microscopy,laser scanning confocal microscopy,and atomic force microscopy.Damage and stress were characterized at the microscale using Raman spectroscopy.High-quality precision machining of different types of periodic surface microtexture at 40 mW laser power was achieved by controlling the process parameters and laser trajectory.Finally,an initial exploration was conducted to examine vector-light-based microand nanostructure processing.The findings demonstrate the potential of femtosecond lasers for efficient micromachining of hard and brittle materials without the creation of heat-affected zones or microcracks.The high-quality textured structures achieved through this processing technique have broad and promising applications in optoelectronic devices and tribology.展开更多
The competition between dimensionality and ordering in multiferroic materials is of great interest for both fundamental physics and potential applications. Combining first-principles calculations with micromagnetic si...The competition between dimensionality and ordering in multiferroic materials is of great interest for both fundamental physics and potential applications. Combining first-principles calculations with micromagnetic simulations, we investigate recently synthesized ultrathin perovskite bismuth ferrite(BFO) films. Our numerical results reveal that, at the monolayer limit, the ferroelectricity of BFO is missing because the octahedral distortions are constrained. However, the monolayer bismuth ferrite is a topological antiferromagnetic metal with tunable bimeron magnetic structure. The dual topologically non-trivial characteristics make monolayer bismuth ferrite a multifunctional building block in future spintronic devices.展开更多
The recrystallization textures in 95%rolled aluminum sheets with different purities and initial textures were investigated.The effects of recovery levels and the dragging effects induced by impurities on the effective...The recrystallization textures in 95%rolled aluminum sheets with different purities and initial textures were investigated.The effects of recovery levels and the dragging effects induced by impurities on the effective driving force and corresponding behaviors of oriented nucleation and oriented growth during annealing were analyzed.The oriented nucleation is a common behavior in the initial stage of primary recrystallization if the effective driving force in deformed matrix is not too high to reduce the necessity of nucleation period.Oriented growth might appear if the temperature is not too high and the grains,of which the misorientation to matrix is about 40°〈111〉,have enough time and space to expand growth advantages,while certain reduction of effective driving force is also necessary.The recrystallization textures could be changed by controlling initial textures and effective driving forces which can be regulated by recovery levels and dragging effects.展开更多
The effect of concurrent precipitation on recrystallization textures in AA 3003 aluminum alloys was investigated using X-ray diffraction and electron backscattering diffraction（EBSD） analyses. A weak recrystallizati...The effect of concurrent precipitation on recrystallization textures in AA 3003 aluminum alloys was investigated using X-ray diffraction and electron backscattering diffraction（EBSD） analyses. A weak recrystallization texture was observed in the AA 3003 alloy annealed at 783 K due to the high annealing temperature. Under the same conditions, extremely high P {011 } （ 111 ） recrystallization textures were detected in the AA 3003 alloy added with 0. 39% Sc. Based on the EBSD results, no intensely preferential orientation nucleation of recrystallization grains was observed in the early stage of recrystallizafion for both alloys. However, concurrent precipitation strongly retarded the growth of recrystallization grains, except for P nucleation sites, thereby conferring an apparent initial growth advantage for P nucleation sites compared with other nucleation sites. Therefore, a sharp P {011 } 〈 111 〉 texture appeared in concurrently precipitated AA 3003 alloys.展开更多
The deformation and recrystallization textures of 6111 Al alloy with various precipitation states have been investigated by means of the orientation distribution functions (ODFs). It was found that the precipitation s...The deformation and recrystallization textures of 6111 Al alloy with various precipitation states have been investigated by means of the orientation distribution functions (ODFs). It was found that the precipitation state had significant effects on both rolling and recrystallization textures of Al alloy. For the alloy with no or little precipitate, the orientation intensities were distributed more homogeneously along the β-fiber. With increasing aging temperature, the orientation intensities along the β-fiber increased firstly and decreased then. Simultaneity, the orientation intensities along the β-fiber were distributed more and more inhomogeneously. On the other hand, with the precipitates increasing the recrystallization textures changed gradually from {001}<UVW> and very weak {011}<111> orientation to the strong {001}<311> and {011}<111> orientation.展开更多
The microstructure, texture characteristics and torsion ability of two kinds of steel wires were investigated. The eutectoid steel wires were produced by hot and cold drawing with severe deformation. The torsinability...The microstructure, texture characteristics and torsion ability of two kinds of steel wires were investigated. The eutectoid steel wires were produced by hot and cold drawing with severe deformation. The torsinability of steel wires was measured under two cases, i.e. there exists either fiber texture or circular texture. The results showed that the torsional behavior of the steel wires was affected by their textures and microstructures. The {110}<110> circular texture weakened the torsion ability of the wires. The torsion fracture behavior of {110}<110> texture wires is related to the fact that only two slip systems were activated under simple shear strain deformation.展开更多
In the gneisses from the drillhole ZK2304 of the Donghai area, there have been preserved high- and ultrahigh-pressure metamorphic mineral assemblages, a series of complicated retrogressive textures and relevant metamo...In the gneisses from the drillhole ZK2304 of the Donghai area, there have been preserved high- and ultrahigh-pressure metamorphic mineral assemblages, a series of complicated retrogressive textures and relevant metamorphic reactions. In addition to garnet, jadeititic-clinopyroxene and rutile, other peak stage (M2) minerals in some gneisses include phengite, aragonite and coesite or quartz pseudomorphs after coesite. The typical peak-stage mineral assemblages in gneisses are characterized by garnet + jadeitic-clinopyroxene + rutile + coesite, garnet + jadeitic-clinopyroxene + phengite + rutile ± coesite and garnet + jadeitic-clinopyroxene + aragonite + rutile ± coesite. The grossular content (Gro) in garnet is high and may reach 50. 1 mol%. The SiO2 content of phengite ranges from 54.37% to 54.84% with 3.54-3.57 p.f.u. Quartz pseudomorphs after coesite occur as inclusions in garnet.The gneisses of the Donghai area have been subjected to multistage recrystallization and exhibit a closewise P-T evolutional path characterized by the near-isothermal decompression. The inclusion assemblage (Hb+Ep+Bi+Pl+Qz) within garnet and other minerals has recorded a pre-peak stage (Mi) epidote amphibole fades metamorphic event. High- and ultrahigh-pressure peak metamorphism (M2) took place at T=750-860℃ and P>2.7 GPa. The symplectitic assemblages after garnet, jadeitic-clinopyroxene and rutile imply a near-isothermal decompression metamorphism (M3, M4) during the rapid exhumation. Several lines of evidence of petrography and metamorphic reactions indicate that both gneisses and eclogites have experienced ultrahigh-pressure metamorphism in the Donghai area. This research may be of great significance for an in-depth study of the metamorphism and tectonic evolution in the Su-Lu ultrahigh-pressure metamorphic belt.展开更多
The texture evolution in a high strength Ti-IF steel during the processing of hot rolling, cold rolling, and annealing is studied. For comparison, both ferrite rolling and austenite rolling are employed. It is found t...The texture evolution in a high strength Ti-IF steel during the processing of hot rolling, cold rolling, and annealing is studied. For comparison, both ferrite rolling and austenite rolling are employed. It is found that the texture type is the. same after ferrite rolling and austenite rolling, but the texture intensity is much higher in the ferrite rolled sample. Furthermore, texture characteristics at the surface are absolutely different from those at the mid sec tion in both ferrite rolled and austenite rolled samples, as well as under the cold rolled and annealed conditions. The shear texture { 110 } 〈001 〉 disappears and orientation rotates along { 110 } 〈001 〉→ { 554 } 〈 225 〉→ { 111 } 〈 112 〉→{111}〈110〉→{223}〈110〉 during cold rolling. Compared to the austenite rolled sample, the properties of the cold rolled and annealed sheet which is subjected to ferrite rolling are higher.展开更多
Channel die compression and initial textures are used to activate different deformation mechanisms in a fine-grained magnesium alloy AZ31. The σ-ε curves, microstructures and, particularly, textures are analyzed to ...Channel die compression and initial textures are used to activate different deformation mechanisms in a fine-grained magnesium alloy AZ31. The σ-ε curves, microstructures and, particularly, textures are analyzed to reveal different deformation mechanisms and to compare with those of coarse grained samples. Dominant double-prismatic slip, {1012} twinning and basal slip are detected in three types of samples, respectively, which is similar to those of coarse grained samples. The detrimental effect of shear band formation or {1011} twinning is limited in fine grained microstructure. In addition to the higher flow stress at low temperature an early decrease in flow stress at higher temperature is also found in fine-grained samples in comparison with their coarse-grained counterparts. This softening is ascribed to the early dynamic recrystallization or grain boundary glide.展开更多
Texture evolution in nickel, copper and α-brass that are representative of face-centered-cubic （fcc） materials with different stacking fault energy （SFE） during cold rolling was systematically investigated. X-ray...Texture evolution in nickel, copper and α-brass that are representative of face-centered-cubic （fcc） materials with different stacking fault energy （SFE） during cold rolling was systematically investigated. X-ray diffraction, scanning electron microscopy and electron backscatter diffraction techniques were employed to characterize microstructures and local orientation distributions of specimens at different thickness reductions. Besides, Taylor and Schmid factors of the {111} 〈110〉 slip systems and {111} 〈112〉 twin systems for some typical orientations were utilized to explore the relationship between texture evolution and deformation microstructures. It was found that in fcc metals with low SFE at large deformations, the copper-oriented grains rotated around the 〈110〉 crystallographic axis through the brass-R orientation to the Goss orientation, and finally toward the brass orientation. The initiation of shear banding was the dominant mechanism for the above-mentioned texture transition.展开更多
Study of dolomite texture can contribute to understanding the process of dolomitization.This research reports textures and homogenization temperatures of dolomites from the Permian-Triassic strata in the Sichuan Basin...Study of dolomite texture can contribute to understanding the process of dolomitization.This research reports textures and homogenization temperatures of dolomites from the Permian-Triassic strata in the Sichuan Basin and the Lower Paleozoic strata in the Tarim Basin,which provided insights into relationships between dolomite textures and their formation temperatures.Our results are summarized as follows：1） dolomites with well-preserved texture indicate low dolomitization temperature.However,in certain diagenetic environments,the hydrothermal dolomitization may completely or partially preserve the original texture of dolomites.2） The formation temperatures of non-planar dolomites are always higher than those of planar dolomites.3） The formation temperatures of dolomite cements are generally higher than those of replacive dolomites.4） Although the formation temperatures of saddle dolomite cements have a wide range,they show higher values than those of the planar subhedral to euhedral dolomite cements.Thus,saddle dolomites could generally be an indicator of high precipitation temperature.5） The fluid Mg/Ca ratio is another element controlling dolomite morphology.Micritic dolomites,which precipitate from hypersaline fluids with a high Mg/Ca ratio in a subaerial environment could also have features of non-planar anhedral crystal shape because of rapid nucleation and crystallization during dolomitization.展开更多
Textures of high-strength and low-expansion Fe-Ni alloy wires during cold-drawing processes were investigated using X-ray diffraction （XRD） and electron back scatter diffraction （EBSD） techniques. The experimental...Textures of high-strength and low-expansion Fe-Ni alloy wires during cold-drawing processes were investigated using X-ray diffraction （XRD） and electron back scatter diffraction （EBSD） techniques. The experimental results show that the 〈111〉 and 〈100〉 fibre textures are the main texture components, and crystalline grains in the surface are more fine and uniform than those in the center of Fe-Ni alloy wires during cold-drawing processes. It is found that the volume fraction of the 〈111〉 fibre texture component determined by quantitative regression calculation of the Gaussian distribution function reaches more than 60% and the strong 〈111〉 fibre texture component favors the torsional property of Fe-Ni alloy wires.展开更多
Ingot metallurgy (IM) aluminum has long been the subject and attracted the attention of many metallurgists and textural researchers of materials. Due to the introduction of large amounts of ex situ interfaces, however...Ingot metallurgy (IM) aluminum has long been the subject and attracted the attention of many metallurgists and textural researchers of materials. Due to the introduction of large amounts of ex situ interfaces, however, the textures in powder metallurgy (PM) processed aluminum has been rarely reported. In this article, a pure aluminum plate was prepared via PM route. The starting billet was first produced with uni-axially cold compaction and flat hot-extrusion and then followed by cold rolling processes. The hot-extruded and cold rolling deformation textures of the pure PM aluminum at 50%, 80% and 90% cold rolling reductions were studied by orientation distribution functions (ODFs) analysis. The finite element polycrystal model (FEPM) was finally utilized to simulate the cold rolling textural evolution at various stages of cold rolling. In FEPM simulation, the initial hot-extruded textures were taken into account as inputs. The results showed that typical β-fiber texture formed in pure PM aluminum with the cold rolling reduction increased till 80%, and there was not much change after excessive cold rolling deformation. Homogeneous slip is not the only deformation mode in PM processed pure aluminum plate at over 80% cold rolling reduction. The experimental results were qualitatively in good agreement with the simulated ones.展开更多
The influence of torsion deformation on textures of cold drawing pearlific steel wires was investigated by twisting the wires to different number of revolutions. Macro-texture （over the entire wire cross section） as...The influence of torsion deformation on textures of cold drawing pearlific steel wires was investigated by twisting the wires to different number of revolutions. Macro-texture （over the entire wire cross section） associated with torsion deformation was investigated by X-ray diffraction, while micro-texture （near the wire surface） was characterized by EBSD. The results show that the （110） macro-texture increases at the beginning of torsion and then decreases with increasing of torsion strain, while the （110） micro-texture decreases linearly with increasing of torsion strain. The relationships between the （110） fiber texture and the microhardness of the wires are also discussed.展开更多
A unidirectional carbon/carbon composite (1D-C/C) of low bulk density with textures of poruns granular and isotropic carbons sharply manifests brittle fracture and does not display high pseudoplasticity as expected. ...A unidirectional carbon/carbon composite (1D-C/C) of low bulk density with textures of poruns granular and isotropic carbons sharply manifests brittle fracture and does not display high pseudoplasticity as expected. The results of transmisson electron microscopy (TEM) studies show that the strong interface of fiber-matrix should determine its fracture mode.展开更多
Ultrafine-grained commercial-purity aluminum（AA1070） sheets produced by four cycles of accumulative roll-bonding（ARB） without lubrication are subjected to annealing treatments in the temperature range from 250℃ t...Ultrafine-grained commercial-purity aluminum（AA1070） sheets produced by four cycles of accumulative roll-bonding（ARB） without lubrication are subjected to annealing treatments in the temperature range from 250℃ to 400℃.Microstructures and microtextures in the surface and center regions of the ARBed and annealed sheets are measured by electron backscatter diffraction.The results show that annealing treatments at 325℃ or above lead to a reduction in the microstructure gradient but a significant through-thickness texture gradient different from that in the as-deformed state.The center region is featured by the development of a strong cube texture at the expense of rolling components.In the surface region,shear-type components are either enhanced or largely retained,showing a high persistency upon annealing.While the grain structures are restored predominantly by continuous recrystallization in the surface region,a mixture of continuous and discontinuous recrystallization is envisaged for the center region.展开更多
Surface textures had long been recognized as primary factors to provide the skid resistance on pavements; however, no measurement of skid resistance on pervious concrete pavement with various surface texture parameter...Surface textures had long been recognized as primary factors to provide the skid resistance on pavements; however, no measurement of skid resistance on pervious concrete pavement with various surface texture parameters had been made. Fractal geometry was introduced in the present work to accurately simulate transect contour curves of pervious concrete specimens through fractal interpolation. It is proved that its fractal dimension (D) can be adopted to measure the skid resistance on pervious concrete pavement, overcoming the shortcomings of both macrotexture depth (DT ) and British portable pendulum number (NBP). Combined with Fujikawa-Koike tire/road contact model, the optimization method of all surface textures was recommended for designing and constructing excellently skid-resistant and noise-absorptive pervious concrete pavement. In addition, evaluating of the abrasion process and attenuation of the surface textures on concrete pavement slabs was also the focus of this work based on accelerated abrasion test. Results show that the surface textures on pervious concrete pavement slabs is extremely durable, compared to those on conventional grooved or exposed aggregate concrete pavement slabs.展开更多
Electric-field control of topological magnetic states in thinfilm heterostructures is promising for applications in nextgeneration memory or logic devices with ultrahigh density and low-power consumption.Multiferroic ...Electric-field control of topological magnetic states in thinfilm heterostructures is promising for applications in nextgeneration memory or logic devices with ultrahigh density and low-power consumption.Multiferroic materials,where spin and polar degrees of freedom coexist,provide a versatile playground to manipulate magnetism(converse magnetoelectric effect).Here,we report that the topological spin textures can be controlled by electric field in rhombohedral BiFeO_(3)/monoclinic La_(0.67)Sr_(0.33)MnO_(3)thin-film heterostructure at room temperature.展开更多
The effect of cooling rate on the microstructure and transformation textures of high strength hot-rolled steels was investigated.Heat treated samples subjected to different cooling conditions were characterized by opt...The effect of cooling rate on the microstructure and transformation textures of high strength hot-rolled steels was investigated.Heat treated samples subjected to different cooling conditions were characterized by optical and scanning electron microscopes using orientation imaging microscopy（OIM）.The experimental results demonstrate that there is a significant effect of cooling rate on microstructures and textures resulting from phase transformation.Slow cooling rates lead to the appearance of the cube（001）[010],rotated cube（001）[110]/（001）[110],Goss（110）[001]and rotated Goss（110）[110]components.In contrast,textures developed at rapid cooling rates are preferably of Cu（112）[111],Br（110）[112],transformed Cu（113）[110]and transformed Br（332）[113]/（112）[131].These texture changes are attributed to the selective character of the phase transformation.The OIM technique was used to have a better understanding of the formation of phases and their relationship between microstructure and processing conditions.The volume fraction of micro-constituents resulting from phase transformation such as bainite,martensite and different types of ferrite,can be measured satisfactorily by this technique correlating image quality of EBSD patterns to specific phases.展开更多
基金supported by the Henan Key Laboratory of Intelligent Manufacturing Equipment Integration for Superhard Materials(Grant No.JDKJ2022-01)the National Natural Science Foundation of China(Grant Nos.52035009 and 51761135106)+1 种基金the 2020 Mobility Programme of the Sino-German Center for Research Promotion(Grant No.M-0396)the“111”project by the State Administration of Foreign Experts Affairs and the Ministry of Education of China(Grant No.B07014).
文摘Gallium nitride(GaN),as a third-generation semiconductor,is highly attractive due to its exceptional physical and chemical properties.Laser direct writing offers an efficient method for the precise processing of hard and brittle materials.In this work,various types of surface microtexture were processed on GaN epilayers using a femtosecond laser with a wavelength of 1030 nm.The effects of the laser energy,singlepulse interval,number of pulses,and number of scan passes on groove machining were investigated with a view to achieving high-quality micromachining.The depth,width,surface morphology,and roughness of the grooves were analyzed using scanning electron microscopy,laser scanning confocal microscopy,and atomic force microscopy.Damage and stress were characterized at the microscale using Raman spectroscopy.High-quality precision machining of different types of periodic surface microtexture at 40 mW laser power was achieved by controlling the process parameters and laser trajectory.Finally,an initial exploration was conducted to examine vector-light-based microand nanostructure processing.The findings demonstrate the potential of femtosecond lasers for efficient micromachining of hard and brittle materials without the creation of heat-affected zones or microcracks.The high-quality textured structures achieved through this processing technique have broad and promising applications in optoelectronic devices and tribology.
基金supported by the National Natural Science Foundation of China (Grant No. 12174382)the Strategic Priority Research Program of the Chinese Academy of Sciences (Grant Nos. XDB0460000 and XDB28000000)the Innovation Program for Quantum Science and Technology (Grant Nos. 2024ZD0300104 and 2021ZD0302600)。
文摘The competition between dimensionality and ordering in multiferroic materials is of great interest for both fundamental physics and potential applications. Combining first-principles calculations with micromagnetic simulations, we investigate recently synthesized ultrathin perovskite bismuth ferrite(BFO) films. Our numerical results reveal that, at the monolayer limit, the ferroelectricity of BFO is missing because the octahedral distortions are constrained. However, the monolayer bismuth ferrite is a topological antiferromagnetic metal with tunable bimeron magnetic structure. The dual topologically non-trivial characteristics make monolayer bismuth ferrite a multifunctional building block in future spintronic devices.
文摘The recrystallization textures in 95%rolled aluminum sheets with different purities and initial textures were investigated.The effects of recovery levels and the dragging effects induced by impurities on the effective driving force and corresponding behaviors of oriented nucleation and oriented growth during annealing were analyzed.The oriented nucleation is a common behavior in the initial stage of primary recrystallization if the effective driving force in deformed matrix is not too high to reduce the necessity of nucleation period.Oriented growth might appear if the temperature is not too high and the grains,of which the misorientation to matrix is about 40°〈111〉,have enough time and space to expand growth advantages,while certain reduction of effective driving force is also necessary.The recrystallization textures could be changed by controlling initial textures and effective driving forces which can be regulated by recovery levels and dragging effects.
基金The National Natural Science Foundation of China(No.51201031)the Natural Science Foundation of Jiangsu Province(No.BK2011615)the Transformation Program of Science and Technology Achievements of Jiangsu Province(No.BA2011024)
文摘The effect of concurrent precipitation on recrystallization textures in AA 3003 aluminum alloys was investigated using X-ray diffraction and electron backscattering diffraction（EBSD） analyses. A weak recrystallization texture was observed in the AA 3003 alloy annealed at 783 K due to the high annealing temperature. Under the same conditions, extremely high P {011 } （ 111 ） recrystallization textures were detected in the AA 3003 alloy added with 0. 39% Sc. Based on the EBSD results, no intensely preferential orientation nucleation of recrystallization grains was observed in the early stage of recrystallizafion for both alloys. However, concurrent precipitation strongly retarded the growth of recrystallization grains, except for P nucleation sites, thereby conferring an apparent initial growth advantage for P nucleation sites compared with other nucleation sites. Therefore, a sharp P {011 } 〈 111 〉 texture appeared in concurrently precipitated AA 3003 alloys.
文摘The deformation and recrystallization textures of 6111 Al alloy with various precipitation states have been investigated by means of the orientation distribution functions (ODFs). It was found that the precipitation state had significant effects on both rolling and recrystallization textures of Al alloy. For the alloy with no or little precipitate, the orientation intensities were distributed more homogeneously along the β-fiber. With increasing aging temperature, the orientation intensities along the β-fiber increased firstly and decreased then. Simultaneity, the orientation intensities along the β-fiber were distributed more and more inhomogeneously. On the other hand, with the precipitates increasing the recrystallization textures changed gradually from {001}<UVW> and very weak {011}<111> orientation to the strong {001}<311> and {011}<111> orientation.
基金This work is supported by key project of the National Nat-ural Science Foundation of China(Grant No.50231030)the National High Technology Research and Development Pro-gram of China(Grant No.2003AA331030)the Teaching and Research Award Program for Outstanding Young Teach-ers in Higher Education Institutions.
文摘The microstructure, texture characteristics and torsion ability of two kinds of steel wires were investigated. The eutectoid steel wires were produced by hot and cold drawing with severe deformation. The torsinability of steel wires was measured under two cases, i.e. there exists either fiber texture or circular texture. The results showed that the torsional behavior of the steel wires was affected by their textures and microstructures. The {110}<110> circular texture weakened the torsion ability of the wires. The torsion fracture behavior of {110}<110> texture wires is related to the fact that only two slip systems were activated under simple shear strain deformation.
文摘In the gneisses from the drillhole ZK2304 of the Donghai area, there have been preserved high- and ultrahigh-pressure metamorphic mineral assemblages, a series of complicated retrogressive textures and relevant metamorphic reactions. In addition to garnet, jadeititic-clinopyroxene and rutile, other peak stage (M2) minerals in some gneisses include phengite, aragonite and coesite or quartz pseudomorphs after coesite. The typical peak-stage mineral assemblages in gneisses are characterized by garnet + jadeitic-clinopyroxene + rutile + coesite, garnet + jadeitic-clinopyroxene + phengite + rutile ± coesite and garnet + jadeitic-clinopyroxene + aragonite + rutile ± coesite. The grossular content (Gro) in garnet is high and may reach 50. 1 mol%. The SiO2 content of phengite ranges from 54.37% to 54.84% with 3.54-3.57 p.f.u. Quartz pseudomorphs after coesite occur as inclusions in garnet.The gneisses of the Donghai area have been subjected to multistage recrystallization and exhibit a closewise P-T evolutional path characterized by the near-isothermal decompression. The inclusion assemblage (Hb+Ep+Bi+Pl+Qz) within garnet and other minerals has recorded a pre-peak stage (Mi) epidote amphibole fades metamorphic event. High- and ultrahigh-pressure peak metamorphism (M2) took place at T=750-860℃ and P>2.7 GPa. The symplectitic assemblages after garnet, jadeitic-clinopyroxene and rutile imply a near-isothermal decompression metamorphism (M3, M4) during the rapid exhumation. Several lines of evidence of petrography and metamorphic reactions indicate that both gneisses and eclogites have experienced ultrahigh-pressure metamorphism in the Donghai area. This research may be of great significance for an in-depth study of the metamorphism and tectonic evolution in the Su-Lu ultrahigh-pressure metamorphic belt.
基金National Natural Science Foundation of China (50104004)
文摘The texture evolution in a high strength Ti-IF steel during the processing of hot rolling, cold rolling, and annealing is studied. For comparison, both ferrite rolling and austenite rolling are employed. It is found that the texture type is the. same after ferrite rolling and austenite rolling, but the texture intensity is much higher in the ferrite rolled sample. Furthermore, texture characteristics at the surface are absolutely different from those at the mid sec tion in both ferrite rolled and austenite rolled samples, as well as under the cold rolled and annealed conditions. The shear texture { 110 } 〈001 〉 disappears and orientation rotates along { 110 } 〈001 〉→ { 554 } 〈 225 〉→ { 111 } 〈 112 〉→{111}〈110〉→{223}〈110〉 during cold rolling. Compared to the austenite rolled sample, the properties of the cold rolled and annealed sheet which is subjected to ferrite rolling are higher.
基金This work was supported by the National Natural Sci-ence Foundation of China under grant No.50171009the National 863 Program of China(No.2002A A305501)Part work was performed at IMM RWTH A achen,Germany.
文摘Channel die compression and initial textures are used to activate different deformation mechanisms in a fine-grained magnesium alloy AZ31. The σ-ε curves, microstructures and, particularly, textures are analyzed to reveal different deformation mechanisms and to compare with those of coarse grained samples. Dominant double-prismatic slip, {1012} twinning and basal slip are detected in three types of samples, respectively, which is similar to those of coarse grained samples. The detrimental effect of shear band formation or {1011} twinning is limited in fine grained microstructure. In addition to the higher flow stress at low temperature an early decrease in flow stress at higher temperature is also found in fine-grained samples in comparison with their coarse-grained counterparts. This softening is ascribed to the early dynamic recrystallization or grain boundary glide.
基金the financial support of the National Natural Science Foundation of China(Grant No.51101030)the Fundamental Research Funds for the Central Universities(Grant No.N100702001)
文摘Texture evolution in nickel, copper and α-brass that are representative of face-centered-cubic （fcc） materials with different stacking fault energy （SFE） during cold rolling was systematically investigated. X-ray diffraction, scanning electron microscopy and electron backscatter diffraction techniques were employed to characterize microstructures and local orientation distributions of specimens at different thickness reductions. Besides, Taylor and Schmid factors of the {111} 〈110〉 slip systems and {111} 〈112〉 twin systems for some typical orientations were utilized to explore the relationship between texture evolution and deformation microstructures. It was found that in fcc metals with low SFE at large deformations, the copper-oriented grains rotated around the 〈110〉 crystallographic axis through the brass-R orientation to the Goss orientation, and finally toward the brass orientation. The initiation of shear banding was the dominant mechanism for the above-mentioned texture transition.
基金supported by the National Natural Science Foundation(Nos.41172099,41272130)
文摘Study of dolomite texture can contribute to understanding the process of dolomitization.This research reports textures and homogenization temperatures of dolomites from the Permian-Triassic strata in the Sichuan Basin and the Lower Paleozoic strata in the Tarim Basin,which provided insights into relationships between dolomite textures and their formation temperatures.Our results are summarized as follows：1） dolomites with well-preserved texture indicate low dolomitization temperature.However,in certain diagenetic environments,the hydrothermal dolomitization may completely or partially preserve the original texture of dolomites.2） The formation temperatures of non-planar dolomites are always higher than those of planar dolomites.3） The formation temperatures of dolomite cements are generally higher than those of replacive dolomites.4） Although the formation temperatures of saddle dolomite cements have a wide range,they show higher values than those of the planar subhedral to euhedral dolomite cements.Thus,saddle dolomites could generally be an indicator of high precipitation temperature.5） The fluid Mg/Ca ratio is another element controlling dolomite morphology.Micritic dolomites,which precipitate from hypersaline fluids with a high Mg/Ca ratio in a subaerial environment could also have features of non-planar anhedral crystal shape because of rapid nucleation and crystallization during dolomitization.
文摘Textures of high-strength and low-expansion Fe-Ni alloy wires during cold-drawing processes were investigated using X-ray diffraction （XRD） and electron back scatter diffraction （EBSD） techniques. The experimental results show that the 〈111〉 and 〈100〉 fibre textures are the main texture components, and crystalline grains in the surface are more fine and uniform than those in the center of Fe-Ni alloy wires during cold-drawing processes. It is found that the volume fraction of the 〈111〉 fibre texture component determined by quantitative regression calculation of the Gaussian distribution function reaches more than 60% and the strong 〈111〉 fibre texture component favors the torsional property of Fe-Ni alloy wires.
文摘Ingot metallurgy (IM) aluminum has long been the subject and attracted the attention of many metallurgists and textural researchers of materials. Due to the introduction of large amounts of ex situ interfaces, however, the textures in powder metallurgy (PM) processed aluminum has been rarely reported. In this article, a pure aluminum plate was prepared via PM route. The starting billet was first produced with uni-axially cold compaction and flat hot-extrusion and then followed by cold rolling processes. The hot-extruded and cold rolling deformation textures of the pure PM aluminum at 50%, 80% and 90% cold rolling reductions were studied by orientation distribution functions (ODFs) analysis. The finite element polycrystal model (FEPM) was finally utilized to simulate the cold rolling textural evolution at various stages of cold rolling. In FEPM simulation, the initial hot-extruded textures were taken into account as inputs. The results showed that typical β-fiber texture formed in pure PM aluminum with the cold rolling reduction increased till 80%, and there was not much change after excessive cold rolling deformation. Homogeneous slip is not the only deformation mode in PM processed pure aluminum plate at over 80% cold rolling reduction. The experimental results were qualitatively in good agreement with the simulated ones.
基金financially supported by the National Natural Science Foundation of China (No. 50890170)the National Key Technology R&D Program of China (No. 2007BAE15B01)the Fundamental Research Funds for the Central Universities of China (No. XDJK2013C088)
文摘The influence of torsion deformation on textures of cold drawing pearlific steel wires was investigated by twisting the wires to different number of revolutions. Macro-texture （over the entire wire cross section） associated with torsion deformation was investigated by X-ray diffraction, while micro-texture （near the wire surface） was characterized by EBSD. The results show that the （110） macro-texture increases at the beginning of torsion and then decreases with increasing of torsion strain, while the （110） micro-texture decreases linearly with increasing of torsion strain. The relationships between the （110） fiber texture and the microhardness of the wires are also discussed.
文摘A unidirectional carbon/carbon composite (1D-C/C) of low bulk density with textures of poruns granular and isotropic carbons sharply manifests brittle fracture and does not display high pseudoplasticity as expected. The results of transmisson electron microscopy (TEM) studies show that the strong interface of fiber-matrix should determine its fracture mode.
基金supported by the National Natural Science Foundation of China (Nos.51571213 and 51271204)the Hunan Provincial Innovation Foundation for Postgraduate (No.CX2016B040)
文摘Ultrafine-grained commercial-purity aluminum（AA1070） sheets produced by four cycles of accumulative roll-bonding（ARB） without lubrication are subjected to annealing treatments in the temperature range from 250℃ to 400℃.Microstructures and microtextures in the surface and center regions of the ARBed and annealed sheets are measured by electron backscatter diffraction.The results show that annealing treatments at 325℃ or above lead to a reduction in the microstructure gradient but a significant through-thickness texture gradient different from that in the as-deformed state.The center region is featured by the development of a strong cube texture at the expense of rolling components.In the surface region,shear-type components are either enhanced or largely retained,showing a high persistency upon annealing.While the grain structures are restored predominantly by continuous recrystallization in the surface region,a mixture of continuous and discontinuous recrystallization is envisaged for the center region.
基金Project(kfj080205) supported by Key Laboratory of Road Structure and Material of Ministry of Transport of Changsha, China
文摘Surface textures had long been recognized as primary factors to provide the skid resistance on pavements; however, no measurement of skid resistance on pervious concrete pavement with various surface texture parameters had been made. Fractal geometry was introduced in the present work to accurately simulate transect contour curves of pervious concrete specimens through fractal interpolation. It is proved that its fractal dimension (D) can be adopted to measure the skid resistance on pervious concrete pavement, overcoming the shortcomings of both macrotexture depth (DT ) and British portable pendulum number (NBP). Combined with Fujikawa-Koike tire/road contact model, the optimization method of all surface textures was recommended for designing and constructing excellently skid-resistant and noise-absorptive pervious concrete pavement. In addition, evaluating of the abrasion process and attenuation of the surface textures on concrete pavement slabs was also the focus of this work based on accelerated abrasion test. Results show that the surface textures on pervious concrete pavement slabs is extremely durable, compared to those on conventional grooved or exposed aggregate concrete pavement slabs.
基金financially supported by the Basic Science Center Program of National Natural Science Foundation of China(No.51788104)the National Natural Science Foundation of China(Nos.11974052,12074365)the National Key R&D Program of China(No.2021YFA0718700)。
文摘Electric-field control of topological magnetic states in thinfilm heterostructures is promising for applications in nextgeneration memory or logic devices with ultrahigh density and low-power consumption.Multiferroic materials,where spin and polar degrees of freedom coexist,provide a versatile playground to manipulate magnetism(converse magnetoelectric effect).Here,we report that the topological spin textures can be controlled by electric field in rhombohedral BiFeO_(3)/monoclinic La_(0.67)Sr_(0.33)MnO_(3)thin-film heterostructure at room temperature.
文摘The effect of cooling rate on the microstructure and transformation textures of high strength hot-rolled steels was investigated.Heat treated samples subjected to different cooling conditions were characterized by optical and scanning electron microscopes using orientation imaging microscopy（OIM）.The experimental results demonstrate that there is a significant effect of cooling rate on microstructures and textures resulting from phase transformation.Slow cooling rates lead to the appearance of the cube（001）[010],rotated cube（001）[110]/（001）[110],Goss（110）[001]and rotated Goss（110）[110]components.In contrast,textures developed at rapid cooling rates are preferably of Cu（112）[111],Br（110）[112],transformed Cu（113）[110]and transformed Br（332）[113]/（112）[131].These texture changes are attributed to the selective character of the phase transformation.The OIM technique was used to have a better understanding of the formation of phases and their relationship between microstructure and processing conditions.The volume fraction of micro-constituents resulting from phase transformation such as bainite,martensite and different types of ferrite,can be measured satisfactorily by this technique correlating image quality of EBSD patterns to specific phases.
