A salt-assistant stearic acid method (SAM) capable of forming ultrafine K4Ce2Nb10O30 products was described. XRD pattern re-vealed that tetragonal K4Ce2Nb10O30 products could be obtained by heat treatment at 900 ℃ ...A salt-assistant stearic acid method (SAM) capable of forming ultrafine K4Ce2Nb10O30 products was described. XRD pattern re-vealed that tetragonal K4Ce2Nb10O30 products could be obtained by heat treatment at 900 ℃ for 2 h. Transmission electron microscopy (TEM) observations indicated the introduction of KCl could lead to the formation of rod-like K4Ce2Nb10O30 products. The species of salts played a crucial role in fine tuning the shapes and sizes of K4Ce2Nb10O30 products. Furthermore, the K4Ce2Nb10O30 prepared by salt-assistant SAM had considerable activity under visible light irradiation.展开更多
基金supported by the National Natural Science Foundation of China (50902070)the Natural Science Foundation of Jiangsu province (BK2009391)+1 种基金the Research Fund for the Doctoral Program of Higher Education of China (20093219120011)NUST Research Funding (ZDJH07)
文摘A salt-assistant stearic acid method (SAM) capable of forming ultrafine K4Ce2Nb10O30 products was described. XRD pattern re-vealed that tetragonal K4Ce2Nb10O30 products could be obtained by heat treatment at 900 ℃ for 2 h. Transmission electron microscopy (TEM) observations indicated the introduction of KCl could lead to the formation of rod-like K4Ce2Nb10O30 products. The species of salts played a crucial role in fine tuning the shapes and sizes of K4Ce2Nb10O30 products. Furthermore, the K4Ce2Nb10O30 prepared by salt-assistant SAM had considerable activity under visible light irradiation.
基金National Natural Science Foundation of China(51572076,51508172,51378183)Science and Technology Bureau of Xiangyang,and the Foundation of Hubei Key Laboratory of Low Dimensional Optoelectronic Materials and Devices(14XKL1002)