To clarify the deformation behavior of MnS inclusions in a non-quenched and tempered steel at three different positions (edge, 1/2 radius and center) in the cross-section of the billet in the course of hot rolling, is...To clarify the deformation behavior of MnS inclusions in a non-quenched and tempered steel at three different positions (edge, 1/2 radius and center) in the cross-section of the billet in the course of hot rolling, isothermal compression experiments were performed under the deformation temperature range from 1073 to 1473 K, the reduction rates from 25% to 75% and the strain rates from 0.01 to 10 s^(−1). The variations of deformability features (i.e., aspect ratios, size distributions, and morphologies) of MnS inclusions with those isothermal compression parameters were revealed. The evaluation of the probable maximum aspect ratio of MnS inclusions at the three different positions in the cross-section of the billet after hot rolling was examined using the statistical analysis of extreme values. Results showed that the number densities of MnS inclusions at three different positions (edge, 1/2 radius and center) in the cross-section of the steel billet only fluctuated slightly when the deformation parameters varied in the isothermal compression, while the average inclusion aspect ratios in all cases generally have a negative correlation with the deformation temperature and positive correlations with the reduction ratio and the strain rate. Statistical analysis reveals that larger inclusions deform more easily during hot rolling. The effect of rolling temperature on the extreme value of the aspect ratio of inclusions is the smallest, while the effects of initial size, reduction ratio and strain rate are more significant.展开更多
The isothermal compression of M50 steel is carried out on a Gleeble-3500 thermo-mechanical simulator in temperature range of 1 223-1 423 K and strain rates range of 10-70 s^-1. The results show that the carbides play ...The isothermal compression of M50 steel is carried out on a Gleeble-3500 thermo-mechanical simulator in temperature range of 1 223-1 423 K and strain rates range of 10-70 s^-1. The results show that the carbides play a significant role in the flow behavior and microstructure evolution during isothermal compression of M50 steel. The average apparent activation energy for deformation in isothermal compression of M50 steel is （281.1±42.6） kJ·mol^-1 at the strains of 0.4-0.8. The dynamic recrystallization of austenite grains occurs in isothermal compression of M50 steel at 1 363 K and 1 393 K, enhancing with the increase of strain rate and/or strain. The volume fraction of the carbides decreases with the increase of deformation temperature during isothermal compression of M50 steel and the fine carbides inhibit the dynamic recrystallization of austenite grain. With the occurrence of dynamic recrystallization, the austenite grains are refined, leading to a minor increase in the flow stress and apparent activation energy for deformation in isothermal compression of M50 steel. The austenite grains begin to coarsen at 1 423 K and dynamic recrystallization is limited. Hot working of M50 steel should not be performed above 1 393 K in order to achieve good workability.展开更多
Isothermal compression of Ti-6Al-4V alloy was conducted in the deformation temperature range of 1093-1303 K, the strain rates of 0.001, 0.01, 0.1, 1.0, and 10.0 s-1, and the height reductions of 20%-60% with an interv...Isothermal compression of Ti-6Al-4V alloy was conducted in the deformation temperature range of 1093-1303 K, the strain rates of 0.001, 0.01, 0.1, 1.0, and 10.0 s-1, and the height reductions of 20%-60% with an interval of 10%. After compression, the effect of the processing parameters including deformation temperature, strain rate, and height reduction on the flow stress and the microstructure was investigated. The grain size of primary a phase was measured using an OLYMPUS PMG3 microscope with the quantitative metallography SISC IAS V8.0 image analysis software. A model of grain size in isothermal compression of Ti-6A1-4V alloy was developed using fuzzy neural net- work （FNN） with back-propagation （BP） learning algorithm. The maximum difference and the average difference between the predicted and the experimental grain sizes of primary a phase are 13.31% and 7.62% for the sampled data, and 16.48% and 6.97% for the non-sampled data, respectively. It can be concluded that the present model with high prediction precision can be used to predict the grain size in isothermal compression of Ti-6Al-4V alloy.展开更多
Isothermal compression of the Ti-6Al-4V alloy at the deformation temperatures of 950 and 980℃,height reductions of 30% and 60%,and strain rates of 0.001,0.010,0.100 and 1.000 s-1 was conducted,wherein the variations ...Isothermal compression of the Ti-6Al-4V alloy at the deformation temperatures of 950 and 980℃,height reductions of 30% and 60%,and strain rates of 0.001,0.010,0.100 and 1.000 s-1 was conducted,wherein the variations of microstructure with strain rate were investigated.The experimental results showed that the variation of the microstructure with the strain rate under one condition was significantly different from that under another condition,which meaned that the interaction between the processing parameters was great.The optimization of the strain rate under one condition was not suitable for another condition.Therefore,selecting the forging equipment and optimizing the strain rate should be based on simultaneously considering the deformation temperature and height reduction.展开更多
Isothermal compression of TC4 alloy was performed on a Thermecmaster-Z simulator at the deformation temperatures ranging from 1093 to 1243 K, the strain rates ranging from 0.001 to 10.000 s^-l and a maximum strain of ...Isothermal compression of TC4 alloy was performed on a Thermecmaster-Z simulator at the deformation temperatures ranging from 1093 to 1243 K, the strain rates ranging from 0.001 to 10.000 s^-l and a maximum strain of 0.8. The experimental results show that the flow stress increases with the decrease in the deformation temperature and the increase in the strain rate. The apparent activation energy for deformation is much lower at lower strain rates than that at higher strain rates. The flow stress model considering strain compensation was established. The average relative error between the calculated flow stress and experimental results is about 7.69%, indicating that the present model could be used to accurately predict the flow stress during high temperature in α＋β phase field of TC4 alloy.展开更多
Hot compression behavior of Ti-5 Al-5 Mo-5 V-1 Cr-1 Fe alloy with an equiaxed（α＋β） starting microstructure was investigated by isothermal compression test and optical microscopy. Based on the true strain-stress d...Hot compression behavior of Ti-5 Al-5 Mo-5 V-1 Cr-1 Fe alloy with an equiaxed（α＋β） starting microstructure was investigated by isothermal compression test and optical microscopy. Based on the true strain-stress data with temperature correction, constitutive models with a high accuracy were developed and processing maps were established. Strain inhomogeneity at different locations in the compressed sample is reduced by raising temperature, leading to a uniform distribution of α phases. For the temperature range of 800-840 ℃ with a strain rate of 10 s^-1, the transformed volume fraction of α phase increases and the average grain size of α phase decreases slightly with increasing the temperature, indicating co-existence of dynamic recovery and dynamic recrystallization. Flow localization and faint β grain boundaries are observed at the strain rate of 10 s^-1 in the temperature range of 860-900 ℃. The processing map analysis shows that hot working of Ti-5 Al-5 Mo-5 V-1 Cr-1 Fe alloy should be conducted with the strain rate lower than 0.01 s^-1 to extend its workability.展开更多
The compression tests were carried out by Gleeble-1500 thermo-mechanical simulator with samples of semi-solid ZCuSnl0 alloy prepared by strain-induced melt activation （SIMA） process. The original microstruc- ture an...The compression tests were carried out by Gleeble-1500 thermo-mechanical simulator with samples of semi-solid ZCuSnl0 alloy prepared by strain-induced melt activation （SIMA） process. The original microstruc- ture and the deformation temperature of semi-solid ZCuSnl0 alloy are different. The strain is 0.2, and the strain rate is 1 s-1 for the compression test. The results show that when the semi-solid ZCuSnl0 alloy was pre- pared by SIMA process, the liquid fraction of semi-solid microstructure increases, and the solid grain is smaller, more uniform and more inclined to be round as the roiling pre-deformation increasing. The results also indicate that the deformation resistance of ZCuSnl0 alloy in semi-solid state decreases with the deformation temperature increas- ing or the solid fraction of original microstructure de- creasing. The stress-strain curves of the isothermal compression can be divided into quasi-elastic deformation stage and plastic deformation stage, and there are three deformation zones in the samples after isothermal com- pression, namely the difficult deformation zone, the large deformation zone and the free deformation zone. In the three deformation zones, the main deformation mechanism is flow of liquid incorporating solid particles （FLS） mechanism, plastic deformation of solid particles （PDS） mechanism and liquid flow （LF） combining with FLS mechanism, respectively.展开更多
The molar volume isotherms of trans-decahydronaphthalene （C10H18） between 293 and 446 K and at pressures from 10 to 200 MPa have been determined. A modified Tait equation of state is used to fit each experimental mo...The molar volume isotherms of trans-decahydronaphthalene （C10H18） between 293 and 446 K and at pressures from 10 to 200 MPa have been determined. A modified Tait equation of state is used to fit each experimental molar volume isotherm with a maximum average deviation of 0.029%. The thermal expansivity （cubic expansion coefficient） α and isothermal compressibility κ were determined by fitting the slopes of the isobaric curves and isotherms, respectively. The coefficients in the equation Vm=C1＋C2T＋C3T^2-C4p-C5pT have been fitted with an average deviation of 1.03%.展开更多
The Tolman length δ 0 of a liquid with a plane surface has attracted increasing theoretical attention in recent years,but the expression of Tolman length in terms of observable quantities is still not very clear.In 2...The Tolman length δ 0 of a liquid with a plane surface has attracted increasing theoretical attention in recent years,but the expression of Tolman length in terms of observable quantities is still not very clear.In 2001,Bartell gave a simple expression of Tolman length δ 0 in terms of isothermal compressibility.However,this expression predicts that Tolman length is always negative,which is contrary to the results of molecular dynamics simulations（MDS） for simple liquids.In this paper,this contradiction is analyzed and the reason for the discrepancy in the sign is found.In addition,we introduce a new expression of Tolman length in terms of isothermal compressibility for simple fluids not near the critical points under some weak restrictions.The Tolman length of simple liquids calculated by using this formula is consistent with that obtained using MDS regarding the sign.展开更多
This paper concerns the global existence of strong solutions to the 3 D compressible isothermal Navier-Stokes equations with a vacuum at infinity.Based on the special structure of the Zlotnik inequality,the time unifo...This paper concerns the global existence of strong solutions to the 3 D compressible isothermal Navier-Stokes equations with a vacuum at infinity.Based on the special structure of the Zlotnik inequality,the time uniform upper bounds for density are established through some time-dependant a priori estimates under the assumption that the total mass is suitably small.展开更多
The effects of initial microstructure on the flow stress, strain rate sensitivity （m）, strain hardening exponent （n）, apparent activation energy （Q） for deformation of Ti-5Al-2Sn-2Zr-4Mo-4Cr alloy were investiga...The effects of initial microstructure on the flow stress, strain rate sensitivity （m）, strain hardening exponent （n）, apparent activation energy （Q） for deformation of Ti-5Al-2Sn-2Zr-4Mo-4Cr alloy were investigated using isothermal compression tests. Results show that the alloy with Widmanst-tten alpha plates shows a higher peak stress and flow softening. Additionally, the alloy with equiaxed primary alpha exhibits an early yield drop at or above 810 ℃ and at strain rates of 0.1-5.0 s^-1. In the strain range of 0.5-0.7,m of the alloy with equiaxed primary alpha is found to be larger at 0.01 s^-1 and lower deformation temperatures. This phenomenon could be reasonably explained based on the microstructure evolution. The strain has a significant effect onn of the alloy with Widmanst-tten alpha plates, which is attributed to platelet bending/kinking and dynamic globularization ofα phase. In the strain range of 0.15-0.55,Q of the alloy with Widmanst-tten alpha plates is larger.展开更多
Isothermal hot compression tests were carried out on Mg-3.0Nd-0.2Zn-0.4Zr （mass fraction, %, NZ30K） alloy using a Gleeble-3500 thermo-simulation machine at temperatures ranging from 350 to 500 ℃and strain rates fro...Isothermal hot compression tests were carried out on Mg-3.0Nd-0.2Zn-0.4Zr （mass fraction, %, NZ30K） alloy using a Gleeble-3500 thermo-simulation machine at temperatures ranging from 350 to 500 ℃and strain rates from 0.001 to 1 s^-1. A correction of flow stress for deformation heating at a high strain rate was carried out. Based on the corrected data for deformation heating, a hyperbolic sine constitutive equation was established. The constants in the constitutive equation of the hyperbolic sine form were determined as a function of strain. The flow stresses predicted by the developed equation agree well with the experimental results, which confirms that the developed constitutive equations can be used to predict the flow stress of NZ30K alloy during hot deformation.展开更多
The flow behavior and microstructure evolution of 6A82 aluminum alloy (Al?Mg?Si?Cu) with high copper content were studied on a Gleeble?1500 system by isothermal hot compression test in the temperature range from 320 t...The flow behavior and microstructure evolution of 6A82 aluminum alloy (Al?Mg?Si?Cu) with high copper content were studied on a Gleeble?1500 system by isothermal hot compression test in the temperature range from 320 to 530 °C and the strain rate range from 0.001 to 10 s?1. The results reveal that the flow stress of the alloy exhibits a continuous flow softening behavior at low temperatures of 320?390 °C, whereas it reaches steady state at high temperatures (≥460°C), which are influenced greatly by the Zener?Hollomon parameter (Z) in the hyperbolic sine with the hot deformation activation energy of 325.12 kJ/mol. Microstructure characterizations show that prominent dynamic recrystallization and coarsening of dynamic precipitation may be responsible for the continuous flow softening behavior. Due to deformation heating at high strain rates (≥1 s?1), dynamic recrystallization is more prominent in the specimen deformed at 530 °C and 10 s?1 than in the specimen deformed at 460 °C and 0.1 s?1 even though they have very close lnZ values.展开更多
The hot deformation characteristics of Rene88DT superalloy with directionally solidified micro- structure produced by electroslag remelting continuous directionally solidification （ESR-CDS） were studied in the tempe...The hot deformation characteristics of Rene88DT superalloy with directionally solidified micro- structure produced by electroslag remelting continuous directionally solidification （ESR-CDS） were studied in the temperature range of 1,040-1,140 ℃ and strain rate range of 0.001-1.000 s-1 by hot compression tests. Flow curves for Rene88DT alloy with initial directionally solidified （DS） microstructure exhibit pronounced peak stresses at the early stage of deformation followed by the occurrence of dynamic softening phenomenon. Rene88DT alloy with DS micro- structure shows higher flow peak stresses compared with HIPed P/M superalloy FGH4096, but the disparities in peak stresses between ESR-CDSed Rene88DT and HIPed P/M superalloy FGH4096 reduce as temperature increases. The improvement of hot workability of DS alloy with columnar grains avoiding the maximum shear stress comes true. A hot deformation constitutive equation as a function of strain that describes the dependence of flow stress on strain rate and temperature is established. Hot deformation apparent acti- vation energy （Q） varies not only with the strain rate and temperature but also with strain. The strain rate sensitivity exponent （m） map is established at the strain of 0.8, which reveals that global dynamic recrystallization （DRX） shows a relatively high m value in a large strain compression. Optimum parameters are predicted in two regions： T = 1,100-1,130 ℃, ε = 0.100-1.000 s-1 and T = 1,080- 1,100 ℃, ε = 0.010-100 s-1, which is based on pro- cessing maps and deformation microstructure observations.展开更多
As an advanced solid state bonding process,plastic deformation bonding(PDB)is a highly reliable metallurgical joining method that produces significant plastic deformation at the bonding interface of welded joints thro...As an advanced solid state bonding process,plastic deformation bonding(PDB)is a highly reliable metallurgical joining method that produces significant plastic deformation at the bonding interface of welded joints through thermo-mechanical coupling.In this study,PDB behavior of IN718 superalloy was systematically investigated by performing a series of isothermal compression tests at various processing conditions.It was revealed that new grains evolved in the bonding area through discontinuous dynamic recrystallization(DDRX)at 1000–1150℃.Electron backscattered diffraction(EBSD)and transmission electron microscopy(TEM)results revealed that the bonding of joints is related with interfacial grain boundary(IGB)bulging process,which is considered as a nucleation process of DRXed grain under different deformation environments.During recrystallization process,the bonded interface moved due to strain-induced boundary migration(SIBM)process.Stored energy difference(caused by accumulation of dislocations at the bonding interface)was the dominant factor for SIBM during DRX.The mechanical properties of the bonded joints were dependent upon the recrystallized microstructure and SIBM ensued during PDB.展开更多
Isothermal compression tests were conducted to predict the hot deformational flow stress behaviour of 2024AI-T3 alloy with respect to a wide range of strain rates （0.001-100 s l）, strains （0.1-0.5） and temperatur...Isothermal compression tests were conducted to predict the hot deformational flow stress behaviour of 2024AI-T3 alloy with respect to a wide range of strain rates （0.001-100 s l）, strains （0.1-0.5） and temperatures （573-773 K）. The prediction capabilities of various constitutive models for 2024A1 alloys and a recently developed constitutive model were evaluated using statistical parameters such as the average absolute relative error （AARE） and the correlation coefficient （R）. Models recorded the lowest AARE （4.6%） and the highest correlation coefficient （R=0.99） were developed compared with the other models. Hence, this model can track the deformational behaviour of 2027Al-T3 alloy more accurately compared with other models throughout the entire processing domain investigated.展开更多
The two-pass isothermal hot compression method was used to study the effect of different thermal deformation conditions on static recrystallization behavior in Ni-Cr-Mo series SA508Gr.4N low alloy steel with interval ...The two-pass isothermal hot compression method was used to study the effect of different thermal deformation conditions on static recrystallization behavior in Ni-Cr-Mo series SA508Gr.4N low alloy steel with interval holding time ranging from 1 to 300 s,temperature ranging from 950 to 1150℃,strain rate ranging from 0.01 to 1 s^(-1),true strains ranging from 0.1 to 0.2,and initial austenite grain size ranging from 175 to 552μm.It can be concluded that the static recrystallization volume fraction gradually increases with the increase in the deformation temperature,strain rate,strain and pass interval,and the decrease in the initial grain size,which is mainly due to the increase in the deformation energy storage and dislocations.Moreover,strain-induced grain boundary migration is the nucleation mechanism for static recrystallization of SA508Gr.4N low alloy steel.Based on the stress-strain curve,the predicted value obtained from the established static recrystallization kinetics model is in good consistence with the experimental value,and the static recrystallization thermal activation energy of SA508Gr.4N steel was calculated as 264,225.99 J/mol.展开更多
Isothermal compression of TC11 alloy at the deformation temperatures ranging from 1023 to 1323 K with an interval of 20 K, the strain rates of 0.001, 0.1, 1.0, and 10.0 s-1, and the height reductions of 50% and 70% wa...Isothermal compression of TC11 alloy at the deformation temperatures ranging from 1023 to 1323 K with an interval of 20 K, the strain rates of 0.001, 0.1, 1.0, and 10.0 s-1, and the height reductions of 50% and 70% was conducted on a Gleeble-1500D thermomechanical simulator. According to the experimental results, the isothermal compression and the processing maps of TC11 alloy at different strains were drawn by using the dynamic material model （DMM）. Based on the processing maps, the proper forging parameters, including a combination of defor-mation temperature and strain rate, vary with the strain in different phases of TC11 alloy.展开更多
Isothermal compression of a Ti-5.6Al-4.8Sn-2.0Zr alloy was conducted on a Thermecmaster-Z simulator at the deformation temperatures ranging from 960 to 1060℃, the strain rates ranging from 0.001 to 10.0 s^-1, and the...Isothermal compression of a Ti-5.6Al-4.8Sn-2.0Zr alloy was conducted on a Thermecmaster-Z simulator at the deformation temperatures ranging from 960 to 1060℃, the strain rates ranging from 0.001 to 10.0 s^-1, and the maximum height reduction of 70.0%. In the two-phase region of the Ti-5.6Al-4.8Sn-2.0Zr alloy, the volume fraction of α phase decreases with an increase in deformation temperature, but the grain size has a slight variation with deformation temperature. The strain rate affects both morphologies and grain size of the α phase in the isothermal compression of the Ti-5.6Al-4.8Sn-2.0Zr alloy. The optimal height reduction also contributes to the small and well-distributed α phase in the isothermal compression of Ti-5.6Al-4.8Sn-2.0Zr alloy.展开更多
With a strain rate range of 0.01–10 s^(−1) and a deformation temperature range of 1110–1200℃,the isothermal compression test was performed on one powder metallurgy superalloy which is macroscopic segregation free.U...With a strain rate range of 0.01–10 s^(−1) and a deformation temperature range of 1110–1200℃,the isothermal compression test was performed on one powder metallurgy superalloy which is macroscopic segregation free.Using electron backscatter diffraction,the effect of strain rate and deformation temperature on grain shape and grain size of superalloys during thermal deformation was studied.The results established that exquisite and equiaxed dynamic recrystallization(DRX)grains are procured at supernal deformation temperature and high strain rate because of the high dislocation density.At the same time,the interaction between high DRX nucleation rate and low grain growth rate at high strain rate is favorable in making finer DRX grains.The equivalent medial grain size expanded with lowering strain rate and elevating proof temperature.Moreover,the grain shape was researched by the effective method of aspect ratio.Most aspect ratio of original grains is 0.61,and the aspect ratio has important implications for DRX and grain growth process.The average aspect ratio increases slightly when deformation temperature rises from 1110 to 1140℃,while the average aspect ratio increases memorably as the deformation temperature is higher than 1140℃.展开更多
基金supported by the National Natural Science Foundation of China(Grant Nos.52074198,52374342 and U21A20113)also supported by the Department of Science and Technology of Hubei Province(Grant No.2023AFB603 and No.2023DJC140).
文摘To clarify the deformation behavior of MnS inclusions in a non-quenched and tempered steel at three different positions (edge, 1/2 radius and center) in the cross-section of the billet in the course of hot rolling, isothermal compression experiments were performed under the deformation temperature range from 1073 to 1473 K, the reduction rates from 25% to 75% and the strain rates from 0.01 to 10 s^(−1). The variations of deformability features (i.e., aspect ratios, size distributions, and morphologies) of MnS inclusions with those isothermal compression parameters were revealed. The evaluation of the probable maximum aspect ratio of MnS inclusions at the three different positions in the cross-section of the billet after hot rolling was examined using the statistical analysis of extreme values. Results showed that the number densities of MnS inclusions at three different positions (edge, 1/2 radius and center) in the cross-section of the steel billet only fluctuated slightly when the deformation parameters varied in the isothermal compression, while the average inclusion aspect ratios in all cases generally have a negative correlation with the deformation temperature and positive correlations with the reduction ratio and the strain rate. Statistical analysis reveals that larger inclusions deform more easily during hot rolling. The effect of rolling temperature on the extreme value of the aspect ratio of inclusions is the smallest, while the effects of initial size, reduction ratio and strain rate are more significant.
文摘The isothermal compression of M50 steel is carried out on a Gleeble-3500 thermo-mechanical simulator in temperature range of 1 223-1 423 K and strain rates range of 10-70 s^-1. The results show that the carbides play a significant role in the flow behavior and microstructure evolution during isothermal compression of M50 steel. The average apparent activation energy for deformation in isothermal compression of M50 steel is （281.1±42.6） kJ·mol^-1 at the strains of 0.4-0.8. The dynamic recrystallization of austenite grains occurs in isothermal compression of M50 steel at 1 363 K and 1 393 K, enhancing with the increase of strain rate and/or strain. The volume fraction of the carbides decreases with the increase of deformation temperature during isothermal compression of M50 steel and the fine carbides inhibit the dynamic recrystallization of austenite grain. With the occurrence of dynamic recrystallization, the austenite grains are refined, leading to a minor increase in the flow stress and apparent activation energy for deformation in isothermal compression of M50 steel. The austenite grains begin to coarsen at 1 423 K and dynamic recrystallization is limited. Hot working of M50 steel should not be performed above 1 393 K in order to achieve good workability.
基金financially supported by the National Natural Science Foundation of China (No.50975234)
文摘Isothermal compression of Ti-6Al-4V alloy was conducted in the deformation temperature range of 1093-1303 K, the strain rates of 0.001, 0.01, 0.1, 1.0, and 10.0 s-1, and the height reductions of 20%-60% with an interval of 10%. After compression, the effect of the processing parameters including deformation temperature, strain rate, and height reduction on the flow stress and the microstructure was investigated. The grain size of primary a phase was measured using an OLYMPUS PMG3 microscope with the quantitative metallography SISC IAS V8.0 image analysis software. A model of grain size in isothermal compression of Ti-6A1-4V alloy was developed using fuzzy neural net- work （FNN） with back-propagation （BP） learning algorithm. The maximum difference and the average difference between the predicted and the experimental grain sizes of primary a phase are 13.31% and 7.62% for the sampled data, and 16.48% and 6.97% for the non-sampled data, respectively. It can be concluded that the present model with high prediction precision can be used to predict the grain size in isothermal compression of Ti-6Al-4V alloy.
基金financially supported by the National Natural Science Foundation of China (No.50975234)
文摘Isothermal compression of the Ti-6Al-4V alloy at the deformation temperatures of 950 and 980℃,height reductions of 30% and 60%,and strain rates of 0.001,0.010,0.100 and 1.000 s-1 was conducted,wherein the variations of microstructure with strain rate were investigated.The experimental results showed that the variation of the microstructure with the strain rate under one condition was significantly different from that under another condition,which meaned that the interaction between the processing parameters was great.The optimization of the strain rate under one condition was not suitable for another condition.Therefore,selecting the forging equipment and optimizing the strain rate should be based on simultaneously considering the deformation temperature and height reduction.
基金financially supported by China Postdoctoral Science Foundation (No. 2017M610649)Fundamental Research Funds for the Central Universities (No. 3102017zy001)
文摘Isothermal compression of TC4 alloy was performed on a Thermecmaster-Z simulator at the deformation temperatures ranging from 1093 to 1243 K, the strain rates ranging from 0.001 to 10.000 s^-l and a maximum strain of 0.8. The experimental results show that the flow stress increases with the decrease in the deformation temperature and the increase in the strain rate. The apparent activation energy for deformation is much lower at lower strain rates than that at higher strain rates. The flow stress model considering strain compensation was established. The average relative error between the calculated flow stress and experimental results is about 7.69%, indicating that the present model could be used to accurately predict the flow stress during high temperature in α＋β phase field of TC4 alloy.
基金Project(BS2013CL034)supported by the Promotive Research Fund for Excellent Young and Middle-aged Scientists of Shandong Province,ChinaProject(51401115)supported by the National Natural Science Foundation of ChinaProject(GN2013001)supported by Independent Innovation Foundation of Shandong University,China
文摘Hot compression behavior of Ti-5 Al-5 Mo-5 V-1 Cr-1 Fe alloy with an equiaxed（α＋β） starting microstructure was investigated by isothermal compression test and optical microscopy. Based on the true strain-stress data with temperature correction, constitutive models with a high accuracy were developed and processing maps were established. Strain inhomogeneity at different locations in the compressed sample is reduced by raising temperature, leading to a uniform distribution of α phases. For the temperature range of 800-840 ℃ with a strain rate of 10 s^-1, the transformed volume fraction of α phase increases and the average grain size of α phase decreases slightly with increasing the temperature, indicating co-existence of dynamic recovery and dynamic recrystallization. Flow localization and faint β grain boundaries are observed at the strain rate of 10 s^-1 in the temperature range of 860-900 ℃. The processing map analysis shows that hot working of Ti-5 Al-5 Mo-5 V-1 Cr-1 Fe alloy should be conducted with the strain rate lower than 0.01 s^-1 to extend its workability.
基金financially supported by the Applied Basic Research Key Project of Yunnan Province in China(No.2011FA007)the Specialized Research Fund for Doctoral Program of Higher Education(No.20125314120013)+1 种基金the Applied Basic Research General Program of Yunnan Province in China(No.2014FB131)the Development Research Fund from Sichuan University of Science and Engineering(No.2013PY05)
文摘The compression tests were carried out by Gleeble-1500 thermo-mechanical simulator with samples of semi-solid ZCuSnl0 alloy prepared by strain-induced melt activation （SIMA） process. The original microstruc- ture and the deformation temperature of semi-solid ZCuSnl0 alloy are different. The strain is 0.2, and the strain rate is 1 s-1 for the compression test. The results show that when the semi-solid ZCuSnl0 alloy was pre- pared by SIMA process, the liquid fraction of semi-solid microstructure increases, and the solid grain is smaller, more uniform and more inclined to be round as the roiling pre-deformation increasing. The results also indicate that the deformation resistance of ZCuSnl0 alloy in semi-solid state decreases with the deformation temperature increas- ing or the solid fraction of original microstructure de- creasing. The stress-strain curves of the isothermal compression can be divided into quasi-elastic deformation stage and plastic deformation stage, and there are three deformation zones in the samples after isothermal com- pression, namely the difficult deformation zone, the large deformation zone and the free deformation zone. In the three deformation zones, the main deformation mechanism is flow of liquid incorporating solid particles （FLS） mechanism, plastic deformation of solid particles （PDS） mechanism and liquid flow （LF） combining with FLS mechanism, respectively.
文摘The molar volume isotherms of trans-decahydronaphthalene （C10H18） between 293 and 446 K and at pressures from 10 to 200 MPa have been determined. A modified Tait equation of state is used to fit each experimental molar volume isotherm with a maximum average deviation of 0.029%. The thermal expansivity （cubic expansion coefficient） α and isothermal compressibility κ were determined by fitting the slopes of the isobaric curves and isotherms, respectively. The coefficients in the equation Vm=C1＋C2T＋C3T^2-C4p-C5pT have been fitted with an average deviation of 1.03%.
基金Project supported by the National Natural Science Foundation of China (Grant No. 11072242)
文摘The Tolman length δ 0 of a liquid with a plane surface has attracted increasing theoretical attention in recent years,but the expression of Tolman length in terms of observable quantities is still not very clear.In 2001,Bartell gave a simple expression of Tolman length δ 0 in terms of isothermal compressibility.However,this expression predicts that Tolman length is always negative,which is contrary to the results of molecular dynamics simulations（MDS） for simple liquids.In this paper,this contradiction is analyzed and the reason for the discrepancy in the sign is found.In addition,we introduce a new expression of Tolman length in terms of isothermal compressibility for simple fluids not near the critical points under some weak restrictions.The Tolman length of simple liquids calculated by using this formula is consistent with that obtained using MDS regarding the sign.
基金partially supported by the National Natural Science Foundation of China(11701192)。
文摘This paper concerns the global existence of strong solutions to the 3 D compressible isothermal Navier-Stokes equations with a vacuum at infinity.Based on the special structure of the Zlotnik inequality,the time uniform upper bounds for density are established through some time-dependant a priori estimates under the assumption that the total mass is suitably small.
基金Projects(5120531851275416)supported by the National Natural Science Foundation of ChinaProject(2012KJ02002)supported by the Innovation Fund of Science and Technology in Northwestern Polytechnical University,China
文摘The effects of initial microstructure on the flow stress, strain rate sensitivity （m）, strain hardening exponent （n）, apparent activation energy （Q） for deformation of Ti-5Al-2Sn-2Zr-4Mo-4Cr alloy were investigated using isothermal compression tests. Results show that the alloy with Widmanst-tten alpha plates shows a higher peak stress and flow softening. Additionally, the alloy with equiaxed primary alpha exhibits an early yield drop at or above 810 ℃ and at strain rates of 0.1-5.0 s^-1. In the strain range of 0.5-0.7,m of the alloy with equiaxed primary alpha is found to be larger at 0.01 s^-1 and lower deformation temperatures. This phenomenon could be reasonably explained based on the microstructure evolution. The strain has a significant effect onn of the alloy with Widmanst-tten alpha plates, which is attributed to platelet bending/kinking and dynamic globularization ofα phase. In the strain range of 0.15-0.55,Q of the alloy with Widmanst-tten alpha plates is larger.
基金Project (2009AA033501) supported by High-tech Research and Development Program of ChinaProject (08DZ1150302) supported by the Science and Technology Commission Foundation Program of Shanghai Municipality, ChinaProject (0911) supported by Shanghai Automotive Industry Science and Technology Development Foundation, China
文摘Isothermal hot compression tests were carried out on Mg-3.0Nd-0.2Zn-0.4Zr （mass fraction, %, NZ30K） alloy using a Gleeble-3500 thermo-simulation machine at temperatures ranging from 350 to 500 ℃and strain rates from 0.001 to 1 s^-1. A correction of flow stress for deformation heating at a high strain rate was carried out. Based on the corrected data for deformation heating, a hyperbolic sine constitutive equation was established. The constants in the constitutive equation of the hyperbolic sine form were determined as a function of strain. The flow stresses predicted by the developed equation agree well with the experimental results, which confirms that the developed constitutive equations can be used to predict the flow stress of NZ30K alloy during hot deformation.
基金Project(2014DFA51270)supported by the International Science and Technology Cooperation Program of ChinaProject(CDJRC10130008)supported by the Fundamental Research Funds for the Central Universities,ChinaProject(51421001)supported by the National Natural Science Foundation of China
文摘The flow behavior and microstructure evolution of 6A82 aluminum alloy (Al?Mg?Si?Cu) with high copper content were studied on a Gleeble?1500 system by isothermal hot compression test in the temperature range from 320 to 530 °C and the strain rate range from 0.001 to 10 s?1. The results reveal that the flow stress of the alloy exhibits a continuous flow softening behavior at low temperatures of 320?390 °C, whereas it reaches steady state at high temperatures (≥460°C), which are influenced greatly by the Zener?Hollomon parameter (Z) in the hyperbolic sine with the hot deformation activation energy of 325.12 kJ/mol. Microstructure characterizations show that prominent dynamic recrystallization and coarsening of dynamic precipitation may be responsible for the continuous flow softening behavior. Due to deformation heating at high strain rates (≥1 s?1), dynamic recrystallization is more prominent in the specimen deformed at 530 °C and 10 s?1 than in the specimen deformed at 460 °C and 0.1 s?1 even though they have very close lnZ values.
基金financially supported by the Military Supporting Project (No. JPPT125GJGG11)
文摘The hot deformation characteristics of Rene88DT superalloy with directionally solidified micro- structure produced by electroslag remelting continuous directionally solidification （ESR-CDS） were studied in the temperature range of 1,040-1,140 ℃ and strain rate range of 0.001-1.000 s-1 by hot compression tests. Flow curves for Rene88DT alloy with initial directionally solidified （DS） microstructure exhibit pronounced peak stresses at the early stage of deformation followed by the occurrence of dynamic softening phenomenon. Rene88DT alloy with DS micro- structure shows higher flow peak stresses compared with HIPed P/M superalloy FGH4096, but the disparities in peak stresses between ESR-CDSed Rene88DT and HIPed P/M superalloy FGH4096 reduce as temperature increases. The improvement of hot workability of DS alloy with columnar grains avoiding the maximum shear stress comes true. A hot deformation constitutive equation as a function of strain that describes the dependence of flow stress on strain rate and temperature is established. Hot deformation apparent acti- vation energy （Q） varies not only with the strain rate and temperature but also with strain. The strain rate sensitivity exponent （m） map is established at the strain of 0.8, which reveals that global dynamic recrystallization （DRX） shows a relatively high m value in a large strain compression. Optimum parameters are predicted in two regions： T = 1,100-1,130 ℃, ε = 0.100-1.000 s-1 and T = 1,080- 1,100 ℃, ε = 0.010-100 s-1, which is based on pro- cessing maps and deformation microstructure observations.
基金the National Key Research and Development Program[grant number 2018YFA0702900]the National Natural Science Foundation of China[grant numbers U1508215,51774265]+2 种基金the National Science and Technology Major Project of China[Grant No.2019ZX06004010]the Key Program of the Chinese Academy of Sciences[Grant No.ZDRW-CN-2017-1]the CAS Interdisciplinary Innovation Team。
文摘As an advanced solid state bonding process,plastic deformation bonding(PDB)is a highly reliable metallurgical joining method that produces significant plastic deformation at the bonding interface of welded joints through thermo-mechanical coupling.In this study,PDB behavior of IN718 superalloy was systematically investigated by performing a series of isothermal compression tests at various processing conditions.It was revealed that new grains evolved in the bonding area through discontinuous dynamic recrystallization(DDRX)at 1000–1150℃.Electron backscattered diffraction(EBSD)and transmission electron microscopy(TEM)results revealed that the bonding of joints is related with interfacial grain boundary(IGB)bulging process,which is considered as a nucleation process of DRXed grain under different deformation environments.During recrystallization process,the bonded interface moved due to strain-induced boundary migration(SIBM)process.Stored energy difference(caused by accumulation of dislocations at the bonding interface)was the dominant factor for SIBM during DRX.The mechanical properties of the bonded joints were dependent upon the recrystallized microstructure and SIBM ensued during PDB.
文摘Isothermal compression tests were conducted to predict the hot deformational flow stress behaviour of 2024AI-T3 alloy with respect to a wide range of strain rates （0.001-100 s l）, strains （0.1-0.5） and temperatures （573-773 K）. The prediction capabilities of various constitutive models for 2024A1 alloys and a recently developed constitutive model were evaluated using statistical parameters such as the average absolute relative error （AARE） and the correlation coefficient （R）. Models recorded the lowest AARE （4.6%） and the highest correlation coefficient （R=0.99） were developed compared with the other models. Hence, this model can track the deformational behaviour of 2027Al-T3 alloy more accurately compared with other models throughout the entire processing domain investigated.
基金This work was financially supported by the National Energy Application Technology Research and Engineering Demonstrative Project of China(NY201501)the National High Technology Research and Development Program of China(863 program.No.2012AA03A501)the National Key Research and Development Program of China(2016YFB0300203).
文摘The two-pass isothermal hot compression method was used to study the effect of different thermal deformation conditions on static recrystallization behavior in Ni-Cr-Mo series SA508Gr.4N low alloy steel with interval holding time ranging from 1 to 300 s,temperature ranging from 950 to 1150℃,strain rate ranging from 0.01 to 1 s^(-1),true strains ranging from 0.1 to 0.2,and initial austenite grain size ranging from 175 to 552μm.It can be concluded that the static recrystallization volume fraction gradually increases with the increase in the deformation temperature,strain rate,strain and pass interval,and the decrease in the initial grain size,which is mainly due to the increase in the deformation energy storage and dislocations.Moreover,strain-induced grain boundary migration is the nucleation mechanism for static recrystallization of SA508Gr.4N low alloy steel.Based on the stress-strain curve,the predicted value obtained from the established static recrystallization kinetics model is in good consistence with the experimental value,and the static recrystallization thermal activation energy of SA508Gr.4N steel was calculated as 264,225.99 J/mol.
基金supported by the National Natural Science Foundation of China (No. 50975234)
文摘Isothermal compression of TC11 alloy at the deformation temperatures ranging from 1023 to 1323 K with an interval of 20 K, the strain rates of 0.001, 0.1, 1.0, and 10.0 s-1, and the height reductions of 50% and 70% was conducted on a Gleeble-1500D thermomechanical simulator. According to the experimental results, the isothermal compression and the processing maps of TC11 alloy at different strains were drawn by using the dynamic material model （DMM）. Based on the processing maps, the proper forging parameters, including a combination of defor-mation temperature and strain rate, vary with the strain in different phases of TC11 alloy.
基金supported by the National Natural Science Foundation of China(No.50975234)the State Key of Laboratory of Solidification Processing in Northwestern Polytechnical University(No.KP200905)
文摘Isothermal compression of a Ti-5.6Al-4.8Sn-2.0Zr alloy was conducted on a Thermecmaster-Z simulator at the deformation temperatures ranging from 960 to 1060℃, the strain rates ranging from 0.001 to 10.0 s^-1, and the maximum height reduction of 70.0%. In the two-phase region of the Ti-5.6Al-4.8Sn-2.0Zr alloy, the volume fraction of α phase decreases with an increase in deformation temperature, but the grain size has a slight variation with deformation temperature. The strain rate affects both morphologies and grain size of the α phase in the isothermal compression of the Ti-5.6Al-4.8Sn-2.0Zr alloy. The optimal height reduction also contributes to the small and well-distributed α phase in the isothermal compression of Ti-5.6Al-4.8Sn-2.0Zr alloy.
基金This work received financial support of the National Natural Science Foundation of China(Grant No.51805308)the China Postdoctoral Science Foundation(Grant No.2018M631189)+1 种基金the Natural Science Foundation of Shaanxi Province(No.2019JQ-303)the Wenzhou Municipal Science and Technology Foundation(No.G20180032).
文摘With a strain rate range of 0.01–10 s^(−1) and a deformation temperature range of 1110–1200℃,the isothermal compression test was performed on one powder metallurgy superalloy which is macroscopic segregation free.Using electron backscatter diffraction,the effect of strain rate and deformation temperature on grain shape and grain size of superalloys during thermal deformation was studied.The results established that exquisite and equiaxed dynamic recrystallization(DRX)grains are procured at supernal deformation temperature and high strain rate because of the high dislocation density.At the same time,the interaction between high DRX nucleation rate and low grain growth rate at high strain rate is favorable in making finer DRX grains.The equivalent medial grain size expanded with lowering strain rate and elevating proof temperature.Moreover,the grain shape was researched by the effective method of aspect ratio.Most aspect ratio of original grains is 0.61,and the aspect ratio has important implications for DRX and grain growth process.The average aspect ratio increases slightly when deformation temperature rises from 1110 to 1140℃,while the average aspect ratio increases memorably as the deformation temperature is higher than 1140℃.
