The interaction of MgO-MgAl_(2)O_(4)-based and MgO-Cr_(2)O_(3)-based refractories with X70 molten steel was studied by immersion experiments at 1560℃.The effects of immersion time(30 and 60 min)on the contents of tot...The interaction of MgO-MgAl_(2)O_(4)-based and MgO-Cr_(2)O_(3)-based refractories with X70 molten steel was studied by immersion experiments at 1560℃.The effects of immersion time(30 and 60 min)on the contents of total oxygen(TO),Al,Nb,Si,Mn,and Cr as well as the composition,number density,and size distribution of inclusions in the molten steel were investigated.The influence of the penetration and erosion degree of the molten steel to the refractory on the steel-refractory interface layer was analyzed.The results show that,at 1560℃,the MgO-MgAl_(2)O_(4)-based refractory can better control the contents of TO and the composition of molten steel compared with the MgO-Cr_(2)O_(3)-based refractory.The TO content is only 16×10^(-4) wt.%in the molten steel after reacted with the Mg0-MgAl_(2)O_(4)-based refractory at the end point of refining,4 accounting for 11.5%of that reacted with the MgO-Cr_(2)O_(3)-based refractory(139×10^(-4) wt.%).The number density of inclusions is only 14 mm^(-2),and the average size ofinclusions is only 1.31μm,with thelargest proportion of inclusions in 1-2μm(70%).The Al_(2)O_(3)-MnS-CaO complex inclusions in the original steel changed to complex inclusions dominated by Cr-Nb-Mn-S-O and MgO.Al_(2)O_(3),corresponding to the MgO-Cr_(2)O_(3)-based and MgO-MgAl_(2)O_(4)-based refractories,respectively.The MgO.Al_(2)O_(3) layer was formed at the reaction interface between MgO-MgAl_(2)O_(4)-based refractory and molten steel,which is helpful to restrict the erosion of refractories and the pollution of molten steel.The damage mechanism of the MgO-Cr_(2)O_(3)-based refractory is mainly permeation and chemical reaction,while the damage of the MgO-MgAl_(2)O_(4)-based refractory is mainlyscouring erosion.展开更多
Slag movement on SiO2-based prism refractories in different slag systems was observed. The cross section shape evolution mechanism was discussed. Two types of shape evolution appear. For PbO-SiO2 slag whose surface te...Slag movement on SiO2-based prism refractories in different slag systems was observed. The cross section shape evolution mechanism was discussed. Two types of shape evolution appear. For PbO-SiO2 slag whose surface tension improves with SiO2 concentration, slag film flows up along four edges under axial Marangoni shear force and wettability. Then, it flows down along four lateral faces under gravity. Corrosion rate at edges is larger than that on lateral faces due to different SiO2 solubilities of ascending and descending flow. Prism cross section shape changes from square to round. For FetO-SiO2 slag whose surface tension reduces with the increase of SiO2 concentration, slag film flows up under the inflence of wettability. Then, it flows down under Marangoni shear force and gravity. Compared to four edges, slag is mainly up and down on four lateral faces due to larger surface tension and size. So, prism cross section shape keeps square.展开更多
The(Cu−10Sn)−Ni−MoS2 composites,prepared by powder metallurgy,were studied for the effects of Ni-coated MoS2 on the microstructure,mechanical properties and lubricating properties.The mechanism of effects of Ni and Mo...The(Cu−10Sn)−Ni−MoS2 composites,prepared by powder metallurgy,were studied for the effects of Ni-coated MoS2 on the microstructure,mechanical properties and lubricating properties.The mechanism of effects of Ni and MoS2 on the properties of composites was analyzed through a comparative experiment by adding Ni and MoS2 separately.The results show that the nickel wrapping around the MoS2 particles decreases the reaction rate of MoS2 with the copper matrix,and greatly improves the bonding of the matrix.The composites with 12 wt.%Ni-coated MoS2(C12)show the optimum performance including the mechanical properties and tribological behaviors.Under oil lubrication conditions,the friction coefficient is 0.0075 with a pressure of 8 MPa and a linear velocity of 0.25 m/s.The average dry friction coefficient,sliding against 40Cr steel disc,is measured to be 0.1769 when the linear velocity and pressure are 0.25 m/s and 4 MPa,respectively.展开更多
Firm joins were obtained between Ti（C,N）-based cermet and steel with Ag-Cu-Zn-Ni filler metal by vacuum brazing. The effects of technological parameters such as brazing temperature, holding time, and filler thicknes...Firm joins were obtained between Ti（C,N）-based cermet and steel with Ag-Cu-Zn-Ni filler metal by vacuum brazing. The effects of technological parameters such as brazing temperature, holding time, and filler thickness on the shear strength of the joints were investigated. The microstructure of welded area and the reaction products of the filler metal were examined by scanning electron microscopy （SEM）, metallographic microscope （OM）, energy-dispersive X-ray analysis （EDS）, and X-ray diffraction （XRD）. The brazing temperature of 870℃, holding time of 15 min, and filler thickness of 0.4 mm are a set of optimum technological parameters, under which the maximum shear strength of the joints, 176.5 MPa, is achieved. The results of microstructure show that the wettability of the filler metal on Ti（C,N）-based cermet and steel is well. A mutual solution layer and a diffusion layer exist between the welding base materials and the filler metal.展开更多
In well stimulation treatments using hydrochloric acid,undesirable water-in-oil emulsion and acid sludge may produce and then cause operational problems in oil field development.The processes intensify in the presence...In well stimulation treatments using hydrochloric acid,undesirable water-in-oil emulsion and acid sludge may produce and then cause operational problems in oil field development.The processes intensify in the presence of Fe(Ⅲ),which are from the corroded surfaces of field equipment and/or iron-bearing minerals of the oil reservoir.In order to understand the reasons of the stability of acid emulsions,acid emulsions were prepared by mixing crude oil emulsion with 15% hydrochloric acid solutions with and without Fe(Ⅲ) and then separated into free and upper(water free) and intermediate(with water) layers.It is assumed that the oil phase of the free and upper layers contains the compounds which do not participate in the formation of acid emulsions,and the oil phase of the intermediate layers contains components involved in the formation of oil/acid interface.The composition of the oil phase of each layer of the emulsions was studied.It is found that the asphaltenes with a high content of sulfur,oxygen and metals as well the flocculated material of protonated non-polar oil components are concentrated at the oil/acid interface.In addition to the above,in the presence of Fe(Ⅲ) the Fe(Ⅲ)-based complexes with polar groups of asphaltenes are formed at the acid/oil interface,contributing to the formation of armor films which enhance the emulsion stability.展开更多
In order to solve the problem that traditional signature-based malware detection systems are inefficacious in detecting new malware,a practical malware detection system is constructed to find out new malware. Applicat...In order to solve the problem that traditional signature-based malware detection systems are inefficacious in detecting new malware,a practical malware detection system is constructed to find out new malware. Application programming interface( API) call sequence is introduced to capture activities of a program in this system. After that,based on variable-length n-gram,API call order can be extracted from API call sequence as the malicious behavior feature of a software. Compared with traditional methods,which use fixed-length n-gram,the solution can find more new malware. The experimental results show that the presented approach improves the accuracy of malware detection.展开更多
在万物互联的云时代,云应用程序编程接口(API)是数字经济建设和服务化软件开发的关键数字基础设施。然而,云API数量的持续增长给用户决策和推广带来挑战,设计有效的推荐方法成为亟待解决的重要问题。现有研究多利用调用偏好、搜索关键...在万物互联的云时代,云应用程序编程接口(API)是数字经济建设和服务化软件开发的关键数字基础设施。然而,云API数量的持续增长给用户决策和推广带来挑战,设计有效的推荐方法成为亟待解决的重要问题。现有研究多利用调用偏好、搜索关键词或二者结合进行建模,主要解决为给定Mashup推荐合适云API的问题,未考虑开发者对个性化高阶互补云API的实际需求。该文提出一种基于个性化张量分解的高阶互补云API推荐方法(Personalized Tensor Decomposition based High-order Complementary cloud API Recommendation,PTDHCR)。首先,将Mashup与云API之间的调用关系,以及云API与云API之间的互补关系建模为三维张量,并利用RECAL张量分解技术对这两种关系进行共同学习,以挖掘云API之间的个性化非对称互补关系。然后,考虑到不同互补关系对推荐结果的影响程度不同,构建个性化高阶互补感知网络,充分利用Mashup、查询云API以及候选云API的多模态特征,动态计算Mashup对不同查询和候选云API之间互补关系的关注程度。在此基础上,将个性化互补关系拓展到高阶,得到候选云API与查询云API集合的整体个性化互补性。最后,利用两个真实云API数据集进行实验,结果表明,相较于传统方法,PTDHCR在挖掘个性化互补关系和推荐方面具有较大的优势。展开更多
Ransomware,particularly crypto-ransomware,remains a significant cybersecurity challenge,encrypting victim data and demanding a ransom,often leaving the data irretrievable even if payment is made.This study proposes an...Ransomware,particularly crypto-ransomware,remains a significant cybersecurity challenge,encrypting victim data and demanding a ransom,often leaving the data irretrievable even if payment is made.This study proposes an early detection approach to mitigate such threats by identifying ransomware activity before the encryption process begins.The approach employs a two-tiered approach:a signature-based method using hashing techniques to match known threats and a dynamic behavior-based analysis leveraging Cuckoo Sandbox and machine learning algorithms.A critical feature is the integration of the most effective Application Programming Interface call monitoring,which analyzes system-level interactions such as file encryption,key generation,and registry modifications.This enables the detection of both known and zero-day ransomware variants,overcoming limitations of traditional methods.The proposed technique was evaluated using classifiers such as Random Forest,Support Vector Machine,and K-Nearest Neighbors,achieving a detection accuracy of 98%based on 26 key ransomware attributes with an 80:20 training-to-testing ratio and 10-fold cross-validation.By combining minimal feature sets with robust behavioral analysis,the proposed method outperforms existing solutions and addresses current challenges in ransomware detection,thereby enhancing cybersecurity resilience.展开更多
基金support from the National Natural Science Foundation of China(Grant Nos.U1860205 and 52204352)Youth Project of Hubei Natural Science Foundation(Grant No.2022CFB593)+1 种基金Key R&D Project of Hubei Province(Grant No.2022BAA021)Guiding Project of Scientific Research Plan of Hubei Provincial Department of Education(Grant No.B2022019).
文摘The interaction of MgO-MgAl_(2)O_(4)-based and MgO-Cr_(2)O_(3)-based refractories with X70 molten steel was studied by immersion experiments at 1560℃.The effects of immersion time(30 and 60 min)on the contents of total oxygen(TO),Al,Nb,Si,Mn,and Cr as well as the composition,number density,and size distribution of inclusions in the molten steel were investigated.The influence of the penetration and erosion degree of the molten steel to the refractory on the steel-refractory interface layer was analyzed.The results show that,at 1560℃,the MgO-MgAl_(2)O_(4)-based refractory can better control the contents of TO and the composition of molten steel compared with the MgO-Cr_(2)O_(3)-based refractory.The TO content is only 16×10^(-4) wt.%in the molten steel after reacted with the Mg0-MgAl_(2)O_(4)-based refractory at the end point of refining,4 accounting for 11.5%of that reacted with the MgO-Cr_(2)O_(3)-based refractory(139×10^(-4) wt.%).The number density of inclusions is only 14 mm^(-2),and the average size ofinclusions is only 1.31μm,with thelargest proportion of inclusions in 1-2μm(70%).The Al_(2)O_(3)-MnS-CaO complex inclusions in the original steel changed to complex inclusions dominated by Cr-Nb-Mn-S-O and MgO.Al_(2)O_(3),corresponding to the MgO-Cr_(2)O_(3)-based and MgO-MgAl_(2)O_(4)-based refractories,respectively.The MgO.Al_(2)O_(3) layer was formed at the reaction interface between MgO-MgAl_(2)O_(4)-based refractory and molten steel,which is helpful to restrict the erosion of refractories and the pollution of molten steel.The damage mechanism of the MgO-Cr_(2)O_(3)-based refractory is mainly permeation and chemical reaction,while the damage of the MgO-MgAl_(2)O_(4)-based refractory is mainlyscouring erosion.
基金Projects(U1738101,51804023)supported by the National Natural Science Foundation of ChinaProjects(FRF-TP-18-007A1,FRF-MP-18-007)supported by Fundamental Research Funds for the Central Universities,ChinaProject(2019M650489)supported by China Postdoctoral Science Foundation
文摘Slag movement on SiO2-based prism refractories in different slag systems was observed. The cross section shape evolution mechanism was discussed. Two types of shape evolution appear. For PbO-SiO2 slag whose surface tension improves with SiO2 concentration, slag film flows up along four edges under axial Marangoni shear force and wettability. Then, it flows down along four lateral faces under gravity. Corrosion rate at edges is larger than that on lateral faces due to different SiO2 solubilities of ascending and descending flow. Prism cross section shape changes from square to round. For FetO-SiO2 slag whose surface tension reduces with the increase of SiO2 concentration, slag film flows up under the inflence of wettability. Then, it flows down under Marangoni shear force and gravity. Compared to four edges, slag is mainly up and down on four lateral faces due to larger surface tension and size. So, prism cross section shape keeps square.
基金Projects(51371099,51501091)supported by the National Natural Science Foundation of China。
文摘The(Cu−10Sn)−Ni−MoS2 composites,prepared by powder metallurgy,were studied for the effects of Ni-coated MoS2 on the microstructure,mechanical properties and lubricating properties.The mechanism of effects of Ni and MoS2 on the properties of composites was analyzed through a comparative experiment by adding Ni and MoS2 separately.The results show that the nickel wrapping around the MoS2 particles decreases the reaction rate of MoS2 with the copper matrix,and greatly improves the bonding of the matrix.The composites with 12 wt.%Ni-coated MoS2(C12)show the optimum performance including the mechanical properties and tribological behaviors.Under oil lubrication conditions,the friction coefficient is 0.0075 with a pressure of 8 MPa and a linear velocity of 0.25 m/s.The average dry friction coefficient,sliding against 40Cr steel disc,is measured to be 0.1769 when the linear velocity and pressure are 0.25 m/s and 4 MPa,respectively.
基金supported by the National Natural Science Foundation of China (No. 50074014)
文摘Firm joins were obtained between Ti（C,N）-based cermet and steel with Ag-Cu-Zn-Ni filler metal by vacuum brazing. The effects of technological parameters such as brazing temperature, holding time, and filler thickness on the shear strength of the joints were investigated. The microstructure of welded area and the reaction products of the filler metal were examined by scanning electron microscopy （SEM）, metallographic microscope （OM）, energy-dispersive X-ray analysis （EDS）, and X-ray diffraction （XRD）. The brazing temperature of 870℃, holding time of 15 min, and filler thickness of 0.4 mm are a set of optimum technological parameters, under which the maximum shear strength of the joints, 176.5 MPa, is achieved. The results of microstructure show that the wettability of the filler metal on Ti（C,N）-based cermet and steel is well. A mutual solution layer and a diffusion layer exist between the welding base materials and the filler metal.
文摘In well stimulation treatments using hydrochloric acid,undesirable water-in-oil emulsion and acid sludge may produce and then cause operational problems in oil field development.The processes intensify in the presence of Fe(Ⅲ),which are from the corroded surfaces of field equipment and/or iron-bearing minerals of the oil reservoir.In order to understand the reasons of the stability of acid emulsions,acid emulsions were prepared by mixing crude oil emulsion with 15% hydrochloric acid solutions with and without Fe(Ⅲ) and then separated into free and upper(water free) and intermediate(with water) layers.It is assumed that the oil phase of the free and upper layers contains the compounds which do not participate in the formation of acid emulsions,and the oil phase of the intermediate layers contains components involved in the formation of oil/acid interface.The composition of the oil phase of each layer of the emulsions was studied.It is found that the asphaltenes with a high content of sulfur,oxygen and metals as well the flocculated material of protonated non-polar oil components are concentrated at the oil/acid interface.In addition to the above,in the presence of Fe(Ⅲ) the Fe(Ⅲ)-based complexes with polar groups of asphaltenes are formed at the acid/oil interface,contributing to the formation of armor films which enhance the emulsion stability.
基金Supported by the National High Technology Research and Development Programme of China(No.2013AA014702)the Fundamental Research Funds for the Central University(No.2014PTB-00-04)the China Next Generation Internet Project(No.CNGI-12-02-027)
文摘In order to solve the problem that traditional signature-based malware detection systems are inefficacious in detecting new malware,a practical malware detection system is constructed to find out new malware. Application programming interface( API) call sequence is introduced to capture activities of a program in this system. After that,based on variable-length n-gram,API call order can be extracted from API call sequence as the malicious behavior feature of a software. Compared with traditional methods,which use fixed-length n-gram,the solution can find more new malware. The experimental results show that the presented approach improves the accuracy of malware detection.
文摘在万物互联的云时代,云应用程序编程接口(API)是数字经济建设和服务化软件开发的关键数字基础设施。然而,云API数量的持续增长给用户决策和推广带来挑战,设计有效的推荐方法成为亟待解决的重要问题。现有研究多利用调用偏好、搜索关键词或二者结合进行建模,主要解决为给定Mashup推荐合适云API的问题,未考虑开发者对个性化高阶互补云API的实际需求。该文提出一种基于个性化张量分解的高阶互补云API推荐方法(Personalized Tensor Decomposition based High-order Complementary cloud API Recommendation,PTDHCR)。首先,将Mashup与云API之间的调用关系,以及云API与云API之间的互补关系建模为三维张量,并利用RECAL张量分解技术对这两种关系进行共同学习,以挖掘云API之间的个性化非对称互补关系。然后,考虑到不同互补关系对推荐结果的影响程度不同,构建个性化高阶互补感知网络,充分利用Mashup、查询云API以及候选云API的多模态特征,动态计算Mashup对不同查询和候选云API之间互补关系的关注程度。在此基础上,将个性化互补关系拓展到高阶,得到候选云API与查询云API集合的整体个性化互补性。最后,利用两个真实云API数据集进行实验,结果表明,相较于传统方法,PTDHCR在挖掘个性化互补关系和推荐方面具有较大的优势。
基金funded by the National University of Sciences and Technology(NUST)supported by the Basic Science Research Program through the National Research Foundation of Korea(NRF),funded by the Ministry of Education(2021R1IIA3049788).
文摘Ransomware,particularly crypto-ransomware,remains a significant cybersecurity challenge,encrypting victim data and demanding a ransom,often leaving the data irretrievable even if payment is made.This study proposes an early detection approach to mitigate such threats by identifying ransomware activity before the encryption process begins.The approach employs a two-tiered approach:a signature-based method using hashing techniques to match known threats and a dynamic behavior-based analysis leveraging Cuckoo Sandbox and machine learning algorithms.A critical feature is the integration of the most effective Application Programming Interface call monitoring,which analyzes system-level interactions such as file encryption,key generation,and registry modifications.This enables the detection of both known and zero-day ransomware variants,overcoming limitations of traditional methods.The proposed technique was evaluated using classifiers such as Random Forest,Support Vector Machine,and K-Nearest Neighbors,achieving a detection accuracy of 98%based on 26 key ransomware attributes with an 80:20 training-to-testing ratio and 10-fold cross-validation.By combining minimal feature sets with robust behavioral analysis,the proposed method outperforms existing solutions and addresses current challenges in ransomware detection,thereby enhancing cybersecurity resilience.
