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Real-Time Error Analysis of Multi-Channel Capacitive Voltage Transformer Using Co-Prediction Matrix
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作者 Jiusong Hu Ao Xiong +2 位作者 Yongqi Liu Guaxuan Xiao Yi Zhong 《Journal of Power and Energy Engineering》 2025年第1期1-17,共17页
Capacitive voltage transformers (CVTs) are essential in high-voltage systems. An accurate error assessment is crucial for precise energy metering. However, tracking real-time quantitative changes in capacitive voltage... Capacitive voltage transformers (CVTs) are essential in high-voltage systems. An accurate error assessment is crucial for precise energy metering. However, tracking real-time quantitative changes in capacitive voltage transformer errors, particularly minor variations in multi-channel setups, remains challenging. This paper proposes a method for online error tracking of multi-channel capacitive voltage transformers using a Co-Prediction Matrix. The approach leverages the strong correlation between in-phase channels, particularly the invariance of the signal proportions among them. By establishing a co-prediction matrix based on these proportional relationships, The influence of voltage changes on the primary measurements is mitigated. Analyzing the relationships between the co-prediction matrices over time allows for inferring true measurement errors. Experimental validation with real-world data confirms the effectiveness of the method, demonstrating its capability to continuously track capacitive voltage transformer measurement errors online with precision over extended durations. 展开更多
关键词 Capacitive Voltage Transformers Co-Prediction matrix high-VOLTAGE Measurement error
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Microstructure and mechanical properties of in situ(TiC+SiC)/FeCrCoNi high entropy alloy matrix composites 被引量:1
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作者 Yu-lu Li Yue Zhao +2 位作者 Lin Shen Hao Wu He-guo Zhu 《Journal of Iron and Steel Research International》 SCIE EI CAS CSCD 2021年第4期496-504,共9页
In situ(TiC+SiC)particles(5 vol.%and 10 vol.%,respectively)-reinforced FeCrCoNi high entropy alloy matrix composites were fabricated via vacuum inductive melting method,with equal volume fractions of TiC and SiC parti... In situ(TiC+SiC)particles(5 vol.%and 10 vol.%,respectively)-reinforced FeCrCoNi high entropy alloy matrix composites were fabricated via vacuum inductive melting method,with equal volume fractions of TiC and SiC particles.X-ray diffraction,scanning electron microscope and energy diffraction spectrum were employed to analyze the microstructure and composi-tion of the samples.The results manifested that the FeCrCoNi matrix is composed of FCC phase,and the in situ particles are homogeneously scattered in the matrix.The presence of reinforcements augmented the ultimate tensile strength from 452 to 783 MPa,and raised the yield strength from 162 to 466 MPa at room temperature,whereas the elongation to fracture was reduced from 70.6%to 28.6%.All the tensile fracture surfaces consisted of numerous tiny dimples,indicating that the composites exhibited ductile fracture.Furthermore,the enhancement of strength ascribes to a combination of thermal mis-match strengthening,load-bearing effect,grain refinement,Orowan strengthening and solid solution strengthening effect,which contribute about 58.0%,2.4%,12.3%,11.1%and 16.2%to the improvement of yield tensile strength,respectively. 展开更多
关键词 high entropy alloy matrix composite In situ reaction Microstructure Mechanical property Strengthening mechanism
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High Temperature Properties of Discontinuously Reinforced Titanium Matrix Composites:A Review 被引量:4
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作者 Lin Geng Lujun Huang 《Acta Metallurgica Sinica(English Letters)》 SCIE EI CAS CSCD 2014年第5期787-797,共11页
Further improvement on high temperature durability is one of the most important aims except for high specific strength, high specific stiffness, and excellent wear resistance, to design and fabricate discontinuously r... Further improvement on high temperature durability is one of the most important aims except for high specific strength, high specific stiffness, and excellent wear resistance, to design and fabricate discontinuously reinforced titanium matrix composites (DRTMCs). Their superior properties render them extensive application potential in aerospace and military industries due to the urgent demand for the materials with characteristics of lightweight, high strength, high stiffness and high temperature durability. With development on fabrication methods and room temperature properties, testing, characterizing, evaluating and further increasing high temperature properties of DRTMCs are becoming more and more important to promote their applications. This review provides insights and comprehensions on the high temperature tensile properties, superplastic tensile properties, creep behaviors, and high temperature oxidation behaviors of DRTMCs, 展开更多
关键词 Titanium matrix composites high temperature tensile properties Creep behaviors Oxidation behaviors SUPERPLASTICITY
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A High-Fe Aluminum Matrix Welding Filler Metal for Hardfacing Aluminum-Silicon Alloys
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作者 陈冰泉 《Journal of Wuhan University of Technology(Materials Science)》 SCIE EI CAS 2003年第1期25-28,共4页
A high Fe containing aluminum matrix filler metal for hardfacing aluminum silicon alloys has been developed by using iron,nickel,and silicon as the major strengthening elements,and by measuring mechanical properties... A high Fe containing aluminum matrix filler metal for hardfacing aluminum silicon alloys has been developed by using iron,nickel,and silicon as the major strengthening elements,and by measuring mechanical properties,room temperature and high temperature wear tests,and microstructural analysis.The filler metal,which contains 3.0%-5.0% Fe and 11.0%-13.0% Si,exhibits an excellent weldability.The as cast and as welded microstructures for the filler metal are of uniformly distribution and its dispersed network of hard phase is enriched with Al Si Fe Ni.The filler metal shows high mechanical properties and wear resistance at both room temperature and high temperatures.The deposited metal has a better resistance to impact wear at 220℃ than that of substrate Al Si Mg Cu piston alloy;at room temperature,the deposited metal has an equivalent resistance to slide wear with lubrication as that of a hyper eutectic aluminum silicon alloy with 27% Si and 1% Ni. 展开更多
关键词 aluminum silicon alloys high Fe aluminum matrix filler metal hardface
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Tool wear during high speed turning in situ TiC_p/TiB_w hybrid reinforced Ti-6Al-4V matrix composite 被引量:3
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作者 Ge Yingfei Xu Jiuhua Huan Haixiang 《Chinese Journal of Aeronautics》 SCIE EI CAS CSCD 2016年第5期1425-1435,共11页
Chipping, adhesive wear, abrasive wear and crater wear are prevalent for both the polycrystalline diamond (PCD) and the carbide tools during high speed turning of TiCp/TiBw hybrid reinforced Ti-6Al-4V (TC4) matrix... Chipping, adhesive wear, abrasive wear and crater wear are prevalent for both the polycrystalline diamond (PCD) and the carbide tools during high speed turning of TiCp/TiBw hybrid reinforced Ti-6Al-4V (TC4) matrix composite (TMCs). The combined effects of abrasive wear and diffusion wear caused the big crater on PCD and carbide tool rake face. Compared to the PCD, bigger size of crater was found on the carbide tool due to much higher cutting temperature and the violent chemical reaction between the Ti element in the workpiece and the WC in the tool. However, the marks of the abrasive wear looked much slighter or even could not be observed on the carbide tool especially when low levels of cutting parameters were used, which attributes to much lower hardness and smaller size of WC combined with more significant chemical degradation of carbide. When cutting TC4 using PCD tool, notch wear was the most significant wear pattern which was not found when cutting the TMCs. However, chipping, adhesive wear and crater wear were much milder when compared to the cutting of titanium matrix composite. Due to the absence of abrasive wear when cutting TC4, the generated titanium carbide on the PCD protected the tool from fast wear, which caused that the tool life for TC4 was 6-10 times longer than that for TMCs. 展开更多
关键词 Carbide tool high speed cutting PCD tool Titanium matrix composite Tool wear TURNING
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Microstructure evolution of SiC_w/AZ91 magnesium matrix composite during high temperature compression
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作者 李淑波 甘为民 +1 位作者 郑明毅 吴昆 《中国有色金属学会会刊:英文版》 CSCD 2005年第S2期245-250,共6页
The compressive behavior of the squeeze cast SiC_w/AZ91 composite was investigated at 400℃ and strain rate of 0.01s -1 by Gleeble-1500 thermal mechanical simulator. The microstructure evolution of the composite d... The compressive behavior of the squeeze cast SiC_w/AZ91 composite was investigated at 400℃ and strain rate of 0.01s -1 by Gleeble-1500 thermal mechanical simulator. The microstructure evolution of the composite during compression was observed by scanning electron microscope(SEM) and transmission electron microscope (TEM). The results indicate that the microstructure evolutions involve the movement of SiC whiskers and the changes of the matrix. The rotation and the broken of SiC whiskers tend to be obvious with the increasing strain. At the initial stage of compression (ε=1%), high density of dislocations was observed in the matrix. And at further strain (ε=10%), a number of twins are formed in the matrix. In this case, some twins intercept with each other and are broken with the increasing strain, and dynamic recrystallization (DRX) grains are nucleated at twin boundaries and twin intersections. 展开更多
关键词 MAGNESIUM matrix composite high temperature compression WHISKER TWIN
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Self-propagating high temperature synthesis of MoSi_2 matrix composites 被引量:3
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作者 Akhtar Farid S.H. Islam 《Rare Metals》 SCIE EI CAS CSCD 2006年第3期225-230,共6页
MoSi2 is presently regarded as the most important material for electrical heating and as one with huge potential for high temperature structural uses. MoSi2 and MoSi2 matrix composites were prepared by self-propagatin... MoSi2 is presently regarded as the most important material for electrical heating and as one with huge potential for high temperature structural uses. MoSi2 and MoSi2 matrix composites were prepared by self-propagating high temperature synthesis (SHS). Pure MoSi2 was obtained and a compound of MoSi2 and WSi2was synthesized in the form of predominant solid solution (Mo,W)Si2. By adding aluminum of 5.5 at.% to Mo-Si, the crystal structure of MoSi2 changed into a mixture of tetragonal Cllb MoSi2and hexagonal C40 Mo(Si,Al)2. The (Mo,W)Si2-Mo(Si,Al)2-W(Si,Al)2 composite materials were synthesized by adding aluminum of 5.5 at.% to Mo-W-Si. However, if the amount of the added aluminum was not larger than 2.5 at.%, it did not have any significant effect. SHS is an effective technology for synthesis of MoSi2 and MoSi2 matrix composites. 展开更多
关键词 powder metallurgy MoSi2 matrix composites self-propagating high temperature synthesis molybdenumtungsten disilicide molybdenum aluminosilicide
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Optimal Estimation of High-Dimensional Covariance Matrices with Missing and Noisy Data
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作者 Meiyin Wang Wanzhou Ye 《Advances in Pure Mathematics》 2024年第4期214-227,共14页
The estimation of covariance matrices is very important in many fields, such as statistics. In real applications, data are frequently influenced by high dimensions and noise. However, most relevant studies are based o... The estimation of covariance matrices is very important in many fields, such as statistics. In real applications, data are frequently influenced by high dimensions and noise. However, most relevant studies are based on complete data. This paper studies the optimal estimation of high-dimensional covariance matrices based on missing and noisy sample under the norm. First, the model with sub-Gaussian additive noise is presented. The generalized sample covariance is then modified to define a hard thresholding estimator , and the minimax upper bound is derived. After that, the minimax lower bound is derived, and it is concluded that the estimator presented in this article is rate-optimal. Finally, numerical simulation analysis is performed. The result shows that for missing samples with sub-Gaussian noise, if the true covariance matrix is sparse, the hard thresholding estimator outperforms the traditional estimate method. 展开更多
关键词 high-Dimensional Covariance matrix Missing Data Sub-Gaussian Noise Optimal Estimation
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基于高基质进样-电感耦合等离子体质谱对尿碘测定的研究
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作者 柳华春 周洪伟 +3 位作者 程焰芳 潘心红 彭荣飞 谢进 《医学动物防制》 2025年第1期82-85,共4页
目的建立尿碘的高基质进样-电感耦合等离子体质谱(high matrix introduction-inductively coupled plasma mass spectrometry,HMI-ICP-MS)分析方法,并应用于临床尿碘检测,以了解2019年广州市儿童尿碘的摄入情况,为制定碘缺乏病防制措施... 目的建立尿碘的高基质进样-电感耦合等离子体质谱(high matrix introduction-inductively coupled plasma mass spectrometry,HMI-ICP-MS)分析方法,并应用于临床尿碘检测,以了解2019年广州市儿童尿碘的摄入情况,为制定碘缺乏病防制措施提供科学依据。方法通过调节雾化气、稀释气和反应气流量获得最佳HMI条件,通过对检出限、精密度、准确度进行测定,评估HMI-ICP-MS对尿碘的测定方法,对广州市儿童尿碘进行非参数秩和检验统计分析。结果当雾化气流量为0.4ml/min,稀释气流量为0.7ml/min,碰撞气流量为4.4ml/min时,HMI可以获得最佳工作条件。尿碘浓度在1.0~40.0μg/L时,该方法线性良好,相关系数为0.9999~1.0000;以3倍[信噪比(signal-to-noise ratio,S/N)=3]确定的检出限为0.088μg/L,尿碘加标回收率为71.3%~101.3%,相对标准偏差为1.2%~2.4%。2019年广州市577名8~10岁男童的尿碘中位数为203.4μg/L,566名女童的尿碘中位数为197.0μg/L,不同性别儿童尿碘水平差异无统计学意义(Z=20.703,P=0.931)。结论高基质进样-电感耦合等离子体质谱法方法准确度高,精密度好,满足方法要求,该方法具有更高的耐受大量高盐样品检测的能力。性别本身对尿碘水平影响不大。 展开更多
关键词 高基质进样 碘缺乏病 电感耦合等离子体质谱法 尿碘 儿童
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基于纳米压痕的B_(4)C/7075Al复合材料界面本构方程反演分析
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作者 薛克敏 王可成 +3 位作者 代良伟 田辙环 石文超 李萍 《塑性工程学报》 北大核心 2025年第4期131-140,共10页
为研究热处理后高压扭转B_(4)C/7075Al复合材料界面的介观尺度力学性能,利用纳米压痕实验获取复合材料界面的载荷-位移曲线,提出了一种结合量纲法和有限元反演分析法来确定复合材料界面弹塑性本构关系的逆向分析方法。并基于获得的弹塑... 为研究热处理后高压扭转B_(4)C/7075Al复合材料界面的介观尺度力学性能,利用纳米压痕实验获取复合材料界面的载荷-位移曲线,提出了一种结合量纲法和有限元反演分析法来确定复合材料界面弹塑性本构关系的逆向分析方法。并基于获得的弹塑性本构关系开展有限元模拟,将模拟结果与实验结果进行对比。结果表明:热处理后高压扭转B_(4)C/7075Al复合材料界面的弹性模量、应变硬化指数和屈服强度分别为117.44 GPa、0.296和978 MPa。模拟得到的弹性模量和纳米硬度与实验值的相对误差分别为5.8%和2.9%,证实了基于纳米压痕反演分析B_(4)C/7075Al复合材料界面本构方程的可行性。 展开更多
关键词 金属基复合材料 高压扭转 纳米压痕 反演分析
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Unified parametric approaches for high-order integral observer design for matrix second-order linear systems
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作者 Guangren DUAN Yunli WU 《控制理论与应用(英文版)》 EI 2006年第2期133-139,共7页
A type of high-order integral observers for matrix second-order linear systems is proposed on the basis of generalized eigenstructure assignment via unified parametric approaches. Through establishing two general para... A type of high-order integral observers for matrix second-order linear systems is proposed on the basis of generalized eigenstructure assignment via unified parametric approaches. Through establishing two general parametric solutions to this type of generalized matrix second-order Sylvester matrix equations, two unified complete parametric methods for the proposed observer design problem are presented. Both methods give simple complete parametric expressions for the observer gain matrices. The first one mainly depends on a series of singular value decompositions, and is thus numerically simple and reliable; the second one utilizes the fight factorization of the system, and allows eigenvalues of the error system to be set undetermined and sought via certain optimization procedures. A spring-mass-dashpot system is utilized to illustrate the design procedure and show the effect of the proposed approach. 展开更多
关键词 matrix second-order linear systems high-order integral observer Generalized eigenstructure assignment Singular value decomposition Right factorization
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陀螺效应对高速旋转轮对弯曲模态的影响 被引量:1
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作者 关庆华 王文波 +1 位作者 张丰英 温泽峰 《铁道学报》 北大核心 2025年第3期54-63,共10页
基于转子动力学理论,以Timoshenko连续转轴模拟轮轴,以旋转圆盘模拟车轮,建立旋转轮对动力学模型。利用Riccati传递矩阵计算不同速度下弹性悬挂轮对的涡动模态。通过Timoshenko梁连续转轴模型的色散特性曲线,揭示陀螺效应对旋转体正反... 基于转子动力学理论,以Timoshenko连续转轴模拟轮轴,以旋转圆盘模拟车轮,建立旋转轮对动力学模型。利用Riccati传递矩阵计算不同速度下弹性悬挂轮对的涡动模态。通过Timoshenko梁连续转轴模型的色散特性曲线,揭示陀螺效应对旋转体正反涡动频率的影响机理。与有限元模型计算结果对比表明,基于Timoshenko梁连续转轴模型的弹性轮对能够满足前4阶弯曲模态计算需求,Euler梁模型无法考虑转轴旋转陀螺效应,仅适用于前2阶弯曲响应分析。研究结果表明:陀螺效应使轮对弯曲模态出现正反涡动,随转速提高,正涡动模态频率增大,反涡动模态频率减小;陀螺效应对轮对1、2阶弯曲涡动频率变化影响显著,对3、4阶弯曲涡动模态频率变化影响不大,速度每提高100 km/h,前4阶弯曲模态正涡动频率分别增加9.31、9.62、2.09、0.57 Hz,前4阶弯曲模态反涡动频率分别下降4.97、5.83、1.27、0.50 Hz。 展开更多
关键词 高速轮对 陀螺效应 旋转动力学 传递矩阵 涡动模态
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超声调控技术在碳纤维内部注浆工艺中的应用与价值分析
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作者 王晓强 郭泓飞 《沈阳航空航天大学学报》 2025年第3期10-18,共9页
针对传统连续碳纤维增韧超高温陶瓷基复合材料(C_(f)/UHTCs)制备方式周期长、成本高等问题,提出一种基于超声调控技术的碳纤维内部注浆工艺,实现陶瓷粉体在碳纤维编织体中的均匀分布,并在此基础上分析制备复合材料的力学性能。研究结果... 针对传统连续碳纤维增韧超高温陶瓷基复合材料(C_(f)/UHTCs)制备方式周期长、成本高等问题,提出一种基于超声调控技术的碳纤维内部注浆工艺,实现陶瓷粉体在碳纤维编织体中的均匀分布,并在此基础上分析制备复合材料的力学性能。研究结果表明,通过超声调控技术辅助碳纤维内部注浆,可有效提升复合材料的力学性能,在连续碳纤维增韧超高温陶瓷基复合材料的制备中具有显著效果,可在提升材料制备效率的同时,改善材料性能,对于推动复合材料制备技术的创新有着十分重要的作用。 展开更多
关键词 超声调控 碳纤维内部注浆 超高温陶瓷基复合材料 连续碳纤维 力学性能
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基于编码和错位叠加的高速压缩成像
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作者 程涛 涂鑫 李晓妮 《探测与控制学报》 北大核心 2025年第4期182-187,共6页
尽管高速相机和条纹相机的帧速率很高,但是依然无法满足工业和科研日益增长的需求。提出使用毛玻璃对目标图像逐帧编码,然后通过硬件或软件将编码后的图像帧错位叠加,从而极大提高数据压缩比和帧速率。基于逐帧编码和错位叠加后的图像... 尽管高速相机和条纹相机的帧速率很高,但是依然无法满足工业和科研日益增长的需求。提出使用毛玻璃对目标图像逐帧编码,然后通过硬件或软件将编码后的图像帧错位叠加,从而极大提高数据压缩比和帧速率。基于逐帧编码和错位叠加后的图像分别构建错位循环子块矩阵、分块对角矩阵和压缩感知模型。在不改变数据采集模式的基础上,通过优化处理分块对角矩阵和测量数据,进一步改善了解码重构效果。实验结果表明:优化后,即使压缩比为3.33时,也可实现0.54的SSIM和13.98 dB的SNR;当压缩比为2时,就可获得很好的重构效果。SNR不能完全反映图像质量的改善,SSIM是比SNR更好的客观评价指标。 展开更多
关键词 压缩感知 毛玻璃 高速摄影 分块对角矩阵 全变分
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高密度电阻率法在章丘—邹平地区地表基质层调查中的应用
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作者 董健 都祎 +3 位作者 代杰瑞 喻超 陈磊 王金辉 《山东国土资源》 2025年第5期30-37,共8页
依托山东省章丘—邹平地区地表基质层调查项目,探索高密度电阻率法在地表基质层调查中的应用效果。对同一剖面不同观测装置的观测效果进行了研究,通过与地质、钻探等资料的对比分析,阐述了温纳装置、偶极-偶极装置在高密度电法研究地层... 依托山东省章丘—邹平地区地表基质层调查项目,探索高密度电阻率法在地表基质层调查中的应用效果。对同一剖面不同观测装置的观测效果进行了研究,通过与地质、钻探等资料的对比分析,阐述了温纳装置、偶极-偶极装置在高密度电法研究地层分层方面的可行性,为相同地质条件地表基质层调查规范的拟定提供了技术支撑。完成高密度电法测线5条,分别用2 m极距和5 m极距探明了10 m以浅和50 m以浅地层电阻率异常规律,反演解释了地层层位分布,对地表基质层的划分提供了依据。 展开更多
关键词 高密度电阻率 地表基质层 章丘—邹平
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基于响应面分析的养殖水产品中高风险喹诺酮类抗生素残留及其基质效应研究 被引量:1
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作者 徐汇镔 朱洁 +2 位作者 周朝生 胡园 陆荣茂 《浙江农业学报》 北大核心 2025年第3期689-700,共12页
为建立大黄鱼、鲫鱼、中华鳖等大宗养殖水产品中高风险喹诺酮类抗生素的通用、高效、准确的残留分析方法,利用超声振荡联用法对目标物进行提取,经液液萃取完成净化并采用UPLC-MS/MS测定。通过提取试剂中的酸含量、振荡时间、超声时间、... 为建立大黄鱼、鲫鱼、中华鳖等大宗养殖水产品中高风险喹诺酮类抗生素的通用、高效、准确的残留分析方法,利用超声振荡联用法对目标物进行提取,经液液萃取完成净化并采用UPLC-MS/MS测定。通过提取试剂中的酸含量、振荡时间、超声时间、氮吹压力、温度等变量结合Box-Behnken响应面分析确定最优前处理条件。同时评价大黄鱼、鲫鱼、中华鳖、南美白对虾、青蟹及其性腺、缢蛏中目标物的基质效应,并通过同位素内标、基质匹配曲线探讨了基质效应的补偿途径。结果表明:6种目标物的平均回收率为82.20%~118.00%;在0.2~20 ng·mL^(-1)线性范围内,线性相关系数均大于0.997,氧氟沙星、洛美沙星、诺氟沙星、培氟沙星、环丙沙星检出限为0.1μg·kg^(-1),恩诺沙星检出限为0.5μg·kg^(-1),定量限均为1.0μg·kg^(-1)。该方法满足水产品中喹诺酮类残留的检测要求。南美白对虾、青蟹性腺、大黄鱼基质对6种目标物均有不同程度的抑制作用,基质匹配曲线和内标法均可使基质效应得到有效补偿。 展开更多
关键词 响应面分析 超高效液相色谱串联质谱 养殖水产品 高风险 喹诺酮 基质效应评价
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耐极端烧蚀环境C/C复合材料研究进展 被引量:2
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作者 曾耀莹 王润宁 +3 位作者 侯佳琪 张雨雷 张佳平 李贺军 《航空学报》 北大核心 2025年第6期358-378,共21页
C/C复合材料是空天飞行器热端部件关键的热结构材料,但高温易氧化烧蚀特性限制了其在极端环境下的应用。因此,如何提高C/C复合材料的抗烧蚀性能尤为重要。系统综述了近年来国内外抗烧蚀C/C复合材料的研究进展,围绕基体改性、涂层防护和... C/C复合材料是空天飞行器热端部件关键的热结构材料,但高温易氧化烧蚀特性限制了其在极端环境下的应用。因此,如何提高C/C复合材料的抗烧蚀性能尤为重要。系统综述了近年来国内外抗烧蚀C/C复合材料的研究进展,围绕基体改性、涂层防护和基体改性-涂层一体化3个方面展开阐述。在基体改性方面,基于组元特性差异将材料分为单相陶瓷、复相陶瓷、多组元及高熵陶瓷改性C/C复合材料,揭示了陶瓷氧化产物的阻氧抗烧蚀机制。涂层技术重点剖析了单层涂层、多层梯度复合涂层、微/纳结构增韧涂层及嵌入结构界面涂层的设计原理与烧蚀行为,阐明了界面匹配优化对于缓解涂层热失配和抗烧蚀性能的作用机理。最后,面向极端烧蚀环境应用需求展望了C/C复合材料在氧化烧蚀机理分析、复合材料的结构和组分优化、构件的功能设计及高效低成本制备工艺等方面的发展方向。 展开更多
关键词 C/C复合材料 抗烧蚀性能 超高温陶瓷 涂层 基体改性
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电感耦合等离子体原子发射光谱法测定高纯五氧化二钒中11种元素的含量 被引量:2
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作者 贾美丽 王少娜 +3 位作者 刘金玉 杜浩 张懿 祁健 《理化检验(化学分册)》 北大核心 2025年第7期818-823,共6页
取0.0500~0.1000 g高纯五氧化二钒样品置于铂金坩埚中,加入1.0000~1.2000 g助熔剂(质量比1∶2的硼酸-碳酸钾混合物),搅拌均匀,于950℃熔融15 min,冷却后将坩埚置于含40 mL 20%(体积分数)盐酸溶液的烧杯中,浸出完毕后转移至100 mL容量瓶... 取0.0500~0.1000 g高纯五氧化二钒样品置于铂金坩埚中,加入1.0000~1.2000 g助熔剂(质量比1∶2的硼酸-碳酸钾混合物),搅拌均匀,于950℃熔融15 min,冷却后将坩埚置于含40 mL 20%(体积分数)盐酸溶液的烧杯中,浸出完毕后转移至100 mL容量瓶,用水定容,采用电感耦合等离子体原子发射光谱法测定钠、铝、钙、铁、镁、锰、铬、砷、钛、硅、磷等11种元素的含量,其中钠、硅、钙采用基质匹配法定量,其余8种元素采用外标法定量。结果显示,各元素的质量浓度在2.0 mg·L^(−1)以内与对应的响应强度呈线性关系,检出限(3s)为0.0013~0.027 mg·L^(−1)。实际样品测定值的相对标准偏差(n=10)均小于0.50%,按照标准加入法进行回收试验,回收率为95.5%~100%。采用标准样品进行准确度验证,测定值与认定值基本一致。 展开更多
关键词 电感耦合等离子体原子发射光谱法 高纯五氧化二钒 基质匹配 元素
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成分对共晶高铬铸铁组织及抗磨性能的影响
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作者 张静慧 《铸造工程》 2025年第S1期48-54,共7页
从高铬铸铁化学成分、含量对碳化物及基体组织的影响进行了阐述,并就显微组织对合金的宏观抗磨性进行了全面解析。着重从碳铬两种元素对合金共晶成分,对碳化物体量、类别、形貌以及分布状态进行说明,进一步就共晶组织对铸造成形、退火... 从高铬铸铁化学成分、含量对碳化物及基体组织的影响进行了阐述,并就显微组织对合金的宏观抗磨性进行了全面解析。着重从碳铬两种元素对合金共晶成分,对碳化物体量、类别、形貌以及分布状态进行说明,进一步就共晶组织对铸造成形、退火、淬火处理及机加工等工艺性进行剖析,就铬碳比对合金韧性及硬度进行论述,最后就辅助元素镍钼铜对提高材料淬透性的影响,常存元素硅锰磷硫对合金抗磨性的作用进行了分析。 展开更多
关键词 化学成分 高铬铸铁 碳化物 基体 组织 抗磨性
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碳纤维树脂基复合材料高性能化进展暨北化录取通知书的应用 被引量:1
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作者 梁思韫 曲宇辰 +4 位作者 杨沛文 宋粲 李刚 杨小平 李庆 《北京化工大学学报(自然科学版)》 北大核心 2025年第3期1-13,共13页
碳纤维是关乎国家安全必须自主保障的关键战略材料,必然变成复合材料才能实现其高性能和高附加值。从碳纤维、树脂基体及二者之间的界面3个要素出发,简述了碳纤维树脂基复合材料国内外研究进展,介绍了北京化工大学先进复合材料研究中心(... 碳纤维是关乎国家安全必须自主保障的关键战略材料,必然变成复合材料才能实现其高性能和高附加值。从碳纤维、树脂基体及二者之间的界面3个要素出发,简述了碳纤维树脂基复合材料国内外研究进展,介绍了北京化工大学先进复合材料研究中心(ACC)在碳纤维树脂基复合材料方面的高性能化研究工作,其中包括新型界面相构筑及界面相容新机制、高性能树脂基体的关键制备技术。并重点介绍了北京化工大学“碳纤维”录取通知书的制备工艺和流程,包括环氧树脂合成制备、碳纤维预浸料制备、预浸料铺层设计、复合材料板材成型以及表面印刷等。最后展望了碳纤维树脂基复合材料的未来发展方向。 展开更多
关键词 碳纤维复合材料 高性能化 界面相 高性能树脂 增强增韧 复合材料成型
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