Ultrafast heating(UFH)at the rates of 10-300℃/s was employed as a new strategy to anneal a coldrolled 7 wt%Mn steel,followed by the immediate cooling.Severely deformed strain-induced martensite and lightly-deformed t...Ultrafast heating(UFH)at the rates of 10-300℃/s was employed as a new strategy to anneal a coldrolled 7 wt%Mn steel,followed by the immediate cooling.Severely deformed strain-induced martensite and lightly-deformed thermal martensite,both had been already enriched with C and Mn before,transformed to fine and coarse austenite grains during the UFH,leading to the bimodal size distribution.Compared with the long intercritical annealing(IA)process,the UFH processes produced larger fraction of RA grains(up to 37%)with a high density of dislocation,leading to the significant increase in yield strength by 270 MPa and the product of strength and elongation up to 55 GPa%due to the enormous work hardening capacity.Such a significant strengthening is first attributed to high density dislocations preserved after UFH and then to the microstructural refinement and the precipitation strengthening;whilst the sustainable work hardening is attributed to the successive TRIP effect during deformation,resulting from the large fraction of RA instantly formed with the bimodal size distribution during UFH.Moreover,the results on the microstructural characterization,thermodynamics calculation on the reverse transformation temperature and the kinetic simulations on the reverse transformation all suggest that the austenitization during UFH is displacive and involves the diffusion and partition of C.Therefore,we propose that it is a bainite-like transformation.展开更多
Dry sliding wear tests of a Cr-Mo-V cast hot-forging die steel was carried out within a load range of 50--300 N at 400℃ by a pin-on-disc high temperature wear machine. The effect of heat treatment process on wear res...Dry sliding wear tests of a Cr-Mo-V cast hot-forging die steel was carried out within a load range of 50--300 N at 400℃ by a pin-on-disc high temperature wear machine. The effect of heat treatment process on wear resistance was systematically studied in order to select heat treatment processes of the steel with high wear resistance. The morphology, structure and composition were analyzed using scanning electron microscopy （SEM）, X-ray diffraction （XRD） and energy dispersive spectroscopy （EDS） ; wear mechanism was also discussed. Tribo-oxide layer was found to form on worn surfaces to reduce wear under low loads, but appear inside the matrix to increase wear under high loads. The tribo-oxides were mainly consisted of Fe3O4 and Fe2O3, FeO only appeared under a high load. Oxidative mild wear, transition of mild-severe wear in oxidative wear and extrusive wear took turns to operate with increasing the load. The wear resistance strongly depended on the selection of heat treatment processes or microstructures. It was found that bainite presented a better wear resistance than martensite plus bainite duplex structure, martensite structure was of the poorest wear resistance. The wear resistance increased with increasing austenizing temperature in the range of 920 to 1 120 ℃, then decreased at up to 1 220 ℃. As for tempering temperature and microstructure, the wear resistance increased in following order： 700℃ （tempered sorbite）, 200 ℃ （tempered martensite）, 440 to 650 ℃ （tempered troostite）. An appropriate combination of hardness, toughness, microstructural thermal stability was re- quired for a good wear resistance in high-temperature wear. The optimized heat treatment process was suggested for the cast hot-forging steel to be austenized at 1020 to 1 120 ℃, quenched in oil, then tempered at 440 to 650℃ for 2 h.展开更多
The microstructural changes of Fe83Si4B13 amorphous mother alloy during the heating process were investigated by Laser Scanning Confocal Microscopy （LSCM） ,and the phase transformation was determined by the Thermo-C...The microstructural changes of Fe83Si4B13 amorphous mother alloy during the heating process were investigated by Laser Scanning Confocal Microscopy （LSCM） ,and the phase transformation was determined by the Thermo-Calc calculations. The differences in the melting points measured by Differential Scanning Calorimetry （DSC） and LSCM, and those obtained by Thermo-Calc calculations were also discussed. It is found that the melting points measured by DSC and LSCM are relatively similar, whereas the onset and end of the melting temperatures calculated by Thermo-Calc software are higher than those measured by DSC and observed by LSCM.展开更多
A 3-D mathematical model considering turbulence phenomena has been established based on a computational fluid dynamics technique, so called 3-D SOLA-VOF (Solution Algorithm-Volume of Fluid), to simulate the fluid flow...A 3-D mathematical model considering turbulence phenomena has been established based on a computational fluid dynamics technique, so called 3-D SOLA-VOF (Solution Algorithm-Volume of Fluid), to simulate the fluid flow of mold filling process of die casting. In addition, the mathematical model for simulating the heat transfer in die casting process has also been established. The computation program has been developed by the authors with the finite difference method (FDM) recently. As verification, the mold filling process of a S-shaped die casting has been simulated and the simulation results coincide with that of the benchmark test. Finally, as a practical application, the gating design of a motorcycle component was modified by the mold filling simulation and the dies design of another motorcycle component was optimized by the heat transfer simulation. All the optimized designs were verified by the production practice.展开更多
During the production of Ti-bearing Al-killed ultra-low-carbon(ULC) steel, two different heating processes were used when the converter tapping temperature or the molten steel temperature in the Ruhrstahl–Heraeus(RH)...During the production of Ti-bearing Al-killed ultra-low-carbon(ULC) steel, two different heating processes were used when the converter tapping temperature or the molten steel temperature in the Ruhrstahl–Heraeus(RH) process was low: heating by Al addition during the RH decarburization process and final deoxidation at the end of the RH decarburization process(process-Ⅰ), and increasing the oxygen content at the end of RH decarburization, heating and final deoxidation by one-time Al addition(process-Ⅱ). Temperature increases of 10°C by different processes were studied; the results showed that the two heating processes could achieve the same heating effect. The T.[O] content in the slab and the refining process was better controlled by process-Ⅰ than by process-Ⅱ. Statistical analysis of inclusions showed that the numbers of inclusions in the slab obtained by process-Ⅰ were substantially less than those in the slab obtained by process-Ⅱ. For process-Ⅰ, the Al_2O_3 inclusions produced by Al added to induce heating were substantially removed at the end of decarburization. The amounts of inclusions were substantially greater for process-Ⅱ than for process-Ⅰ at different refining stages because of the higher dissolved oxygen concentration in process-Ⅱ. Industrial test results showed that process-Ⅰ was more beneficial for improving the cleanliness of molten steel.展开更多
An as-cast Al-Zn-Mg-Sc alloy was friction stir processed varying tool related parameters, yielding microstructures with different grain sizes （0.68, 1.8 and 5.5 μm）. Significant increases in room temperature ductil...An as-cast Al-Zn-Mg-Sc alloy was friction stir processed varying tool related parameters, yielding microstructures with different grain sizes （0.68, 1.8 and 5.5 μm）. Significant increases in room temperature ductility were obtained in these materials with reasonable enhancement in strength. It is demonstrated that the type of microstructure produced by friction stir processing （FSP） has a significant influence on the choice of post-FSP heat treatment design for achieving improved tensile properties. It is also found that the ultrafine grained FSP material could not achieve the desired high strength during the post-FSP heat treatment without grain coarsening, whereas the micro-grained FSP materials could reach such strength levels （〉560 MPa） under conventional age hardening heat treatment conditions.展开更多
This paper investigates the thermal-coupled effect across the wall and the optimal heat transfer region of the wall for enhancing the energy saving effect of dividing wall column (DWC), and also studies the effects of...This paper investigates the thermal-coupled effect across the wall and the optimal heat transfer region of the wall for enhancing the energy saving effect of dividing wall column (DWC), and also studies the effects of feed thermal condition (q) and middle component composition of feed (cB) on the heat transfer process, the optimal heat transfer region, and the maximum heat transfer quantity across the wall. The simulation results show that the maximum heat transfer quantity across the wall and the potential for energy saving increase with the increase of q, while with the limitation of temperature difference across the wall, the beneficial heat transfer effect between certain range of stages, which are involved in the optimal heat transfer region, cannot be realized completely for a specific value of q. Besides, compared with q, a changing cB does not change the degree of realizing the beneficial heat transfer effect, but can bring about the variation of liquid split ratio (RL) and vapor split ratio (Rv). Thus, for achieving a maximum energy-saving effect of DWC, different q and cB need to find its own corresponding suitable heat transfer process across the wall.展开更多
The objective of this study is to predict grain size and heat transfer coefficient at the metal-die interface during high pressure die casting process and solidification of the magnesium alloy AM60. Multiple runs of t...The objective of this study is to predict grain size and heat transfer coefficient at the metal-die interface during high pressure die casting process and solidification of the magnesium alloy AM60. Multiple runs of the commercial casting simulation package, ProCASTTM, were used to model the mold filling and solidification events employing a range of interfacial heat transfer coefficient values. The simulation results were used to estimate the centerline cooling curve at various locations through the casting. The centerline cooling curves, together with the die temperature and the thermodynamic properties of the alloy, were then used as inputs to compute the solution to the Stefan problem of a moving phase boundary, thereby providing the through-thickness cooling curves at each chosen location of the casting, Finally, the local cooling rate was used to calculate the resulting grain size via previously established relationships. The effects of die temperature, filling time and heat transfer coefficient on the grain structure in skin region and core region were quantitatively characterized. It was observed that the grain size of skin region strongly depends on above three factors whereas the grain size of core region shows dependence on the interracial heat transfer coefficient and thickness of the samples. The grain size distribution from surface to center was estimated from the relationship between grain size and the predicted cooling rate. The prediction of grain size matches well with experimental results. A comparison of the predicted and experimentally determined grain size profiles enables the determination of the apparent interracial heat transfer coefficient for different locations.展开更多
The properties of matched streams, the simultaneous operation time, and the distance between integrated processes, are the main factors which determine whether the direct integration is feasible or not. According to w...The properties of matched streams, the simultaneous operation time, and the distance between integrated processes, are the main factors which determine whether the direct integration is feasible or not. According to whether such synthetic integration is economically better than the separate integration of each process, a mathematical formulation is established. The retrofit of reforming and arene processes in a certain petrochemical factory, which are independent each other, is chosen as a case study. By only considering the simultaneous operation time, two retrofit designs are proposed: one is that each of the two processes is separately integrated by itself, and the other is that the two processes are integrated comprehensively. Under different simultaneous operation hours, the energy-saving effects and the economic profits of the two designs are calculated, and furthermore, the critical simultaneous operation time for direct heat integration of the two processes is obtained. When the actual simultaneous operation time of the two processes is longer than the critical value, the direct heat integration of the two processes is better economically, and otherwise the separate heat integration for each process should be considered.展开更多
Sealing quality strongly affects heat pipe performance, but few studies focus on the process of heat pipe sealing. Cold welding sealing technology based on a stamping process is applied for heat pipe sealing. The bond...Sealing quality strongly affects heat pipe performance, but few studies focus on the process of heat pipe sealing. Cold welding sealing technology based on a stamping process is applied for heat pipe sealing. The bonding mechanism of the cold welding sealing process （CWSP） is investigated and compared with the experimental results obtained from the bonding interface analysis. An orthogonal experiment is conducted to observe the effects of various parameters, including the sealing gap, sealing length, sealing diameter, and sealing velocity on bonding strength. A method with the utilization of saturated vapor pressure inside a copper tube is proposed to evaluate bonding strength. A corresponding finite element model is developed to investigate the effects of sealing gap and sealing velocity on plastic deformation during the cold welding process. Effects of various parameters on the bonding strength are determined and it is found that the sealing gap is the most critical factor and that the sealing velocity contributes the least effect. The best parameter combination （AIB3CID3, with a 0.5 mm sealing gap, 6 mm sealing length, 3.8 mm sealing diameter, and 50 mm/s sealing velocity） is derived within the experimental parameters. Plastic deformation results derived from the finite element model are consistent with those from the experiment. The instruction for the CWSP of heat pipes and the design of sealing dies of heat pipes are provided.展开更多
We analyzed cloud microphysical processes' latent heat characteristics and their influence on an autumn heavy rain event over Hainan Island,China,using the mesoscale numerical model WRF and WRF-3DVAR system.We fou...We analyzed cloud microphysical processes' latent heat characteristics and their influence on an autumn heavy rain event over Hainan Island,China,using the mesoscale numerical model WRF and WRF-3DVAR system.We found that positive latent heat occurred far above the zero layer,while negative latent heat occurred mainly under the zero layer.There was substantially more positive latent heat than negative latent heat,and the condensation heating had the most important contribution to the latent heat increase.The processes of deposition,congelation,melting and evaporation were all characterized by weakening after their intensification;however,the variations in condensation and sublimation processes were relatively small.The main cloud microphysical processes for positive latent heat were condensation of water vapor into cloud water,the condensation of rain,and the deposition increase of cloud ice,snow and graupel.The main cloud microphysical processes for negative latent heat were the evaporation of rain,the melting and enhanced melting of graupel.The latent heat releases due to different cloud microphysical processes have a significant impact on the intensity of precipitation.Without the condensation and evaporation of rain,the total latent heating would decrease and the moisture variables and precipitation would reduce significantly.Without deposition and sublimation,the heating in high levels would decrease and the precipitation would reduce.Without congelation and melting,the latent heating would enhance in the low levels,and the precipitation would reduce.展开更多
Ground-state cooling of mesoscopic mechanical objects is still a major challenge in the unresolved-sideband regime.We present a frequency modulation(FM)scheme to achieve cooling of the mechanical resonator to its grou...Ground-state cooling of mesoscopic mechanical objects is still a major challenge in the unresolved-sideband regime.We present a frequency modulation(FM)scheme to achieve cooling of the mechanical resonator to its ground-state in a double-cavity optomechanical system containing a mechanical resonator.The mean phonon number is determined by numerically solving a set of differential equations derived from the quantum master equations.Due to efficient suppression of Stokes heating processes in the presence of FM,the ground-state cooling,indicated by numerical calculations,is significantly achievable,regardless of whether in the resolved-sideband regime or the unresolved-sideband regime.Furthermore,by choosing parameters reasonably,the improvement of the quantum cooling limit is found to be capable of being positively correlated with the modulation frequency.This method provides new insight into quantum manipulation and creates more possibilities for applications of quantum devices.展开更多
The reducing efficiencies of the commonly used heat treatment methods and fermentation processes on aflatoxin M1 (AFM1) in Nigeria were investigated. Seventy samples of fresh cow milk from both conventional and tradit...The reducing efficiencies of the commonly used heat treatment methods and fermentation processes on aflatoxin M1 (AFM1) in Nigeria were investigated. Seventy samples of fresh cow milk from both conventional and traditional dairy cattle herds were collected and analyzed for the determination of AFM1 using Cobra-cell incorporated high performance liquid chromatography. Of these analyzed samples, 56 (80.0%) tested positive for AFM1 out of which 3 milk samples with high AFM1 concentrations were selectively pooled and subjected to varied conditions of heat treatments and fermentation processes using both indigenized and exotic strains of lactic acid bacteria (Lactobacillus bulgaricus + Streptococcus thermophilus and L. rhamnosus and L. plantarum) as starter cultures respectively. Both processes used either singly or combined, demonstrated high degrees of reducing effects on AFM1 levels. Sterilization of the milk at 121?C and 80?C under the same condition of time (15 - 20) min showed significant reduction of up to 58.8% (p 0.05) in the level of AFM1 when compared with the initial mean AFM1 concentration of the untreated fresh milk. The situation was however different around the boiling temperature of 100?C at which point the level of AFM1 reduction was found to be inconsistent. The indigenized combined strains showed some slight margins of AFM1 reduction in the proportions of (20.5, 30.8 and 43.9)% over and above that of the exotic strains (17.4, 30.0 and 41.1)% in 12 h, 48 h and 72 h of fermentation respectively. Generally, fermentation alone showed lower reduction of AFM1 in milk from 24.5% to 43.9% compared with the reducing activities of (35.4 to 58.8)% when heat-treated milk samples were subsequently subjected to varied fermentation conditions.展开更多
According to heat transfer principle and the process of solving engineering problems by finite element method, examples were given to demonstrate how finite element analysis can be used to describe transient heat tran...According to heat transfer principle and the process of solving engineering problems by finite element method, examples were given to demonstrate how finite element analysis can be used to describe transient heat transfer through fabrics. Details were given to describe how conduction and convection affect temperature distribution and heat loss during heat transfer processes by taking advantage of the quick calculation of FEA software MSC.Marc. Experimental results show good agreement with the theoretical results.展开更多
An extraordinary rainstorm that occurred in Beijing on 21 July 2012 was simulated using the Weather Research and Forecasting model. The results showed that:(1) The two precipitation phases were based on a combination ...An extraordinary rainstorm that occurred in Beijing on 21 July 2012 was simulated using the Weather Research and Forecasting model. The results showed that:(1) The two precipitation phases were based on a combination of cold cloud processes and warm cloud processes. The accumulated conversion amount and conversion rate of microphysical processes in the warm-area phase were all much larger than those in the cold front phase.(2) 72.6% of rainwater was from the warm-area phase. Rainwater mainly came from the melting of graupel and the melting of snow, while the accretion of cloud water by rain ranked second.(3) The net heating rate with height appeared as an overall warming with two strong heating centers in the lower and middle layers of the troposphere and a minimum heating center around the melting layer. The net heating effect in the warm-area phase was stronger than that in the cold front phase.(4) Warm cloud processes contributed most to latent heat release, and the thermal effect of cold cloud processes on the storm in the cold front phase was enhanced compared to that in the warm-area phase.(5) The melting of graupel and snow contributed most to latent heat absorption, and the effect of the evaporation of rainwater was significantly reduced in the cold front phase.展开更多
The results of numerical simulation of the mosaic embedding iron ore sintering （MEBIOS） process according to the model presented in the first part of the study are introduced. The main objective of the second part i...The results of numerical simulation of the mosaic embedding iron ore sintering （MEBIOS） process according to the model presented in the first part of the study are introduced. The main objective of the second part is the elucidation of key factors influencing the process efficiency, particularly the sintering completeness, velocity of the heat wave propagation and maximum temperature achievable in the pellet during the wave propagation. Numerical results reveal that the mass fraction of coal, diameter of coal particles and air inlet velocity are of prime importance in determining efficiency of the MEBIOS sintering process.展开更多
In-situ HVEM observation on phase transition of the YBa_2Cu_3O_(7-x) superconducting compound in pro- cess of heating was carried out,and high temperature X-ray diffraction analysis in air and X-ray diffraction phase ...In-situ HVEM observation on phase transition of the YBa_2Cu_3O_(7-x) superconducting compound in pro- cess of heating was carried out,and high temperature X-ray diffraction analysis in air and X-ray diffraction phase analysis for the sample treated in vacuum condition were made.The results showed that the temperature of phase transition is related to oxygen content in the sample and in general,is 100℃ to 120℃ lower in vacu- um condition than in air.At 320℃ to 350℃ twin bands begin to disappear,and some Cu_2O are formed on the surface of the sample and transit from orthorhombic YBa_2Cu_3O_(7-x) to arthorhombic Y_2BaCuO_5 compound. This transition was completed at about 500℃.Above 900℃,this compound consists of the Y_2BaCuO_5, BaCuO_2,Y_2O_3 and some other minor compounds.No phase transition was observed during cooling the sample.展开更多
The continuous constructive challenge to improve the functionality and efficiency of components always results in higher demands on production engineering, against the background of the generally increasing cost press...The continuous constructive challenge to improve the functionality and efficiency of components always results in higher demands on production engineering, against the background of the generally increasing cost pressure. In many cases, you will just succeed in producing competitive and innovative products by combining and coupling of different procedures to an independent (hybrid) technology. The use of hybrid procedures for metal joining and heat treatment of metallic materials finds more and more industrial fields of application. Modern vacuum lines with integrated pressurized gas quenching are considered high-performance and flexible means of production for brazing and heat treatment tasks as well in the turbine industry as in the mould making and tool manufacturing industry. In doing so, the heat treatment is coupled with the brazing cycle in a combined process so that the brazing temperatures and soak times are adapted to the necessary temperatures and times for solution heat treatment and austeniting. This user-oriented article describes on the one hand examples of brazing of turbine components, but above all the practical experience from the plastics processing industry, where the requirement for a high-efficient cooling of injection moulding dies gains more and more importance. The combined procedure "Vacuum Brazing and Hardening" offers plenty of possibilities to produce mould inserts with an efficient tempering system in an economic way.展开更多
The plan of heat-treatment process for 2014Al alloy is designed using orthogonal method, the heat-treatment experiments are made and the mechanical properties are tested according to the designed plan. The effect of s...The plan of heat-treatment process for 2014Al alloy is designed using orthogonal method, the heat-treatment experiments are made and the mechanical properties are tested according to the designed plan. The effect of solid solution temperature, ageing temperature, ageing time on microscopic mechanism of the mechanical properties of the 2014Al alloy is studied using microscope, transmission electron microscope. The best heat treatment process of the 2014Al alloy is developed. The experimental results indicate that the strength σ<sub>b</sub>, yield stress σ<sub>0.2</sub>, percentage elongation δ of the alloy reach separately 490～500 MPa, 450～490 MPa, 10～12％ adopting the new heat treatment process. Compared with GB, the strength increases 20～30％, the percentage elongation increases 30～40％. The mechanism of the new heat-treatment process is also discussed.展开更多
Three-dimensional thermal a nalysis simulation of a horizontal zone refining system is conducted for germanimn semiconductor materials. The considered geometry includes a g＇ral）hite boat filled with germanium placed...Three-dimensional thermal a nalysis simulation of a horizontal zone refining system is conducted for germanimn semiconductor materials. The considered geometry includes a g＇ral）hite boat filled with germanium placed in a cylindrical quartz tube. A flow of Ar and H2 gas mixture is purged througll the tube. A narrow section of the, boat is assmned to be exposed to a constant heat rate produced b v an rf coil located outside the quartz tube. The results of this analysis provide essential information about various parameters such as the shape of tile molten zone, required power and temperature gradient in the system.展开更多
基金financial support from National Natural Science Foundation of China[Nos.51831002 and 51861135302]the Fundamental Research Funds for the Central Universities(No.FRF-TP-18-002C2)。
文摘Ultrafast heating(UFH)at the rates of 10-300℃/s was employed as a new strategy to anneal a coldrolled 7 wt%Mn steel,followed by the immediate cooling.Severely deformed strain-induced martensite and lightly-deformed thermal martensite,both had been already enriched with C and Mn before,transformed to fine and coarse austenite grains during the UFH,leading to the bimodal size distribution.Compared with the long intercritical annealing(IA)process,the UFH processes produced larger fraction of RA grains(up to 37%)with a high density of dislocation,leading to the significant increase in yield strength by 270 MPa and the product of strength and elongation up to 55 GPa%due to the enormous work hardening capacity.Such a significant strengthening is first attributed to high density dislocations preserved after UFH and then to the microstructural refinement and the precipitation strengthening;whilst the sustainable work hardening is attributed to the successive TRIP effect during deformation,resulting from the large fraction of RA instantly formed with the bimodal size distribution during UFH.Moreover,the results on the microstructural characterization,thermodynamics calculation on the reverse transformation temperature and the kinetic simulations on the reverse transformation all suggest that the austenitization during UFH is displacive and involves the diffusion and partition of C.Therefore,we propose that it is a bainite-like transformation.
基金Item Sponsored by National Nature Science Foundation of China(51071078)
文摘Dry sliding wear tests of a Cr-Mo-V cast hot-forging die steel was carried out within a load range of 50--300 N at 400℃ by a pin-on-disc high temperature wear machine. The effect of heat treatment process on wear resistance was systematically studied in order to select heat treatment processes of the steel with high wear resistance. The morphology, structure and composition were analyzed using scanning electron microscopy （SEM）, X-ray diffraction （XRD） and energy dispersive spectroscopy （EDS） ; wear mechanism was also discussed. Tribo-oxide layer was found to form on worn surfaces to reduce wear under low loads, but appear inside the matrix to increase wear under high loads. The tribo-oxides were mainly consisted of Fe3O4 and Fe2O3, FeO only appeared under a high load. Oxidative mild wear, transition of mild-severe wear in oxidative wear and extrusive wear took turns to operate with increasing the load. The wear resistance strongly depended on the selection of heat treatment processes or microstructures. It was found that bainite presented a better wear resistance than martensite plus bainite duplex structure, martensite structure was of the poorest wear resistance. The wear resistance increased with increasing austenizing temperature in the range of 920 to 1 120 ℃, then decreased at up to 1 220 ℃. As for tempering temperature and microstructure, the wear resistance increased in following order： 700℃ （tempered sorbite）, 200 ℃ （tempered martensite）, 440 to 650 ℃ （tempered troostite）. An appropriate combination of hardness, toughness, microstructural thermal stability was re- quired for a good wear resistance in high-temperature wear. The optimized heat treatment process was suggested for the cast hot-forging steel to be austenized at 1020 to 1 120 ℃, quenched in oil, then tempered at 440 to 650℃ for 2 h.
文摘The microstructural changes of Fe83Si4B13 amorphous mother alloy during the heating process were investigated by Laser Scanning Confocal Microscopy （LSCM） ,and the phase transformation was determined by the Thermo-Calc calculations. The differences in the melting points measured by Differential Scanning Calorimetry （DSC） and LSCM, and those obtained by Thermo-Calc calculations were also discussed. It is found that the melting points measured by DSC and LSCM are relatively similar, whereas the onset and end of the melting temperatures calculated by Thermo-Calc software are higher than those measured by DSC and observed by LSCM.
文摘A 3-D mathematical model considering turbulence phenomena has been established based on a computational fluid dynamics technique, so called 3-D SOLA-VOF (Solution Algorithm-Volume of Fluid), to simulate the fluid flow of mold filling process of die casting. In addition, the mathematical model for simulating the heat transfer in die casting process has also been established. The computation program has been developed by the authors with the finite difference method (FDM) recently. As verification, the mold filling process of a S-shaped die casting has been simulated and the simulation results coincide with that of the benchmark test. Finally, as a practical application, the gating design of a motorcycle component was modified by the mold filling simulation and the dies design of another motorcycle component was optimized by the heat transfer simulation. All the optimized designs were verified by the production practice.
基金financially supported by the National Natural Science Foundation of China (No.51404022)
文摘During the production of Ti-bearing Al-killed ultra-low-carbon(ULC) steel, two different heating processes were used when the converter tapping temperature or the molten steel temperature in the Ruhrstahl–Heraeus(RH) process was low: heating by Al addition during the RH decarburization process and final deoxidation at the end of the RH decarburization process(process-Ⅰ), and increasing the oxygen content at the end of RH decarburization, heating and final deoxidation by one-time Al addition(process-Ⅱ). Temperature increases of 10°C by different processes were studied; the results showed that the two heating processes could achieve the same heating effect. The T.[O] content in the slab and the refining process was better controlled by process-Ⅰ than by process-Ⅱ. Statistical analysis of inclusions showed that the numbers of inclusions in the slab obtained by process-Ⅰ were substantially less than those in the slab obtained by process-Ⅱ. For process-Ⅰ, the Al_2O_3 inclusions produced by Al added to induce heating were substantially removed at the end of decarburization. The amounts of inclusions were substantially greater for process-Ⅱ than for process-Ⅰ at different refining stages because of the higher dissolved oxygen concentration in process-Ⅱ. Industrial test results showed that process-Ⅰ was more beneficial for improving the cleanliness of molten steel.
文摘An as-cast Al-Zn-Mg-Sc alloy was friction stir processed varying tool related parameters, yielding microstructures with different grain sizes （0.68, 1.8 and 5.5 μm）. Significant increases in room temperature ductility were obtained in these materials with reasonable enhancement in strength. It is demonstrated that the type of microstructure produced by friction stir processing （FSP） has a significant influence on the choice of post-FSP heat treatment design for achieving improved tensile properties. It is also found that the ultrafine grained FSP material could not achieve the desired high strength during the post-FSP heat treatment without grain coarsening, whereas the micro-grained FSP materials could reach such strength levels （〉560 MPa） under conventional age hardening heat treatment conditions.
基金supported by the Natural Science Research Youth Foundation of Hebei Higher Education of China [QN2016084]the National Natural Science Foundation of China[21878066]
文摘This paper investigates the thermal-coupled effect across the wall and the optimal heat transfer region of the wall for enhancing the energy saving effect of dividing wall column (DWC), and also studies the effects of feed thermal condition (q) and middle component composition of feed (cB) on the heat transfer process, the optimal heat transfer region, and the maximum heat transfer quantity across the wall. The simulation results show that the maximum heat transfer quantity across the wall and the potential for energy saving increase with the increase of q, while with the limitation of temperature difference across the wall, the beneficial heat transfer effect between certain range of stages, which are involved in the optimal heat transfer region, cannot be realized completely for a specific value of q. Besides, compared with q, a changing cB does not change the degree of realizing the beneficial heat transfer effect, but can bring about the variation of liquid split ratio (RL) and vapor split ratio (Rv). Thus, for achieving a maximum energy-saving effect of DWC, different q and cB need to find its own corresponding suitable heat transfer process across the wall.
基金jointly supported by Canadian Network for Research and Innovation in Machining TechnologyNatural Sciences and Engineering Research Council of Canada-Automotive Partnership Canada programNRCan’s Office of Energy R&D through the Program on Energy R&D
文摘The objective of this study is to predict grain size and heat transfer coefficient at the metal-die interface during high pressure die casting process and solidification of the magnesium alloy AM60. Multiple runs of the commercial casting simulation package, ProCASTTM, were used to model the mold filling and solidification events employing a range of interfacial heat transfer coefficient values. The simulation results were used to estimate the centerline cooling curve at various locations through the casting. The centerline cooling curves, together with the die temperature and the thermodynamic properties of the alloy, were then used as inputs to compute the solution to the Stefan problem of a moving phase boundary, thereby providing the through-thickness cooling curves at each chosen location of the casting, Finally, the local cooling rate was used to calculate the resulting grain size via previously established relationships. The effects of die temperature, filling time and heat transfer coefficient on the grain structure in skin region and core region were quantitatively characterized. It was observed that the grain size of skin region strongly depends on above three factors whereas the grain size of core region shows dependence on the interracial heat transfer coefficient and thickness of the samples. The grain size distribution from surface to center was estimated from the relationship between grain size and the predicted cooling rate. The prediction of grain size matches well with experimental results. A comparison of the predicted and experimentally determined grain size profiles enables the determination of the apparent interracial heat transfer coefficient for different locations.
基金Supported by the National Natural Science Foundation of China(No. 20176045)Major State Basic Research Development Program of China(No. G20000263)
文摘The properties of matched streams, the simultaneous operation time, and the distance between integrated processes, are the main factors which determine whether the direct integration is feasible or not. According to whether such synthetic integration is economically better than the separate integration of each process, a mathematical formulation is established. The retrofit of reforming and arene processes in a certain petrochemical factory, which are independent each other, is chosen as a case study. By only considering the simultaneous operation time, two retrofit designs are proposed: one is that each of the two processes is separately integrated by itself, and the other is that the two processes are integrated comprehensively. Under different simultaneous operation hours, the energy-saving effects and the economic profits of the two designs are calculated, and furthermore, the critical simultaneous operation time for direct heat integration of the two processes is obtained. When the actual simultaneous operation time of the two processes is longer than the critical value, the direct heat integration of the two processes is better economically, and otherwise the separate heat integration for each process should be considered.
基金Supported by National Natural Science Foundation of China(Grant Nos.51175186,51675185)Guangdong Provincial Natural Science Foundation of China(Grant No.S2013020012757)EU project PIIF-GA-2012-332304(Grant No.ESR332304)
文摘Sealing quality strongly affects heat pipe performance, but few studies focus on the process of heat pipe sealing. Cold welding sealing technology based on a stamping process is applied for heat pipe sealing. The bonding mechanism of the cold welding sealing process （CWSP） is investigated and compared with the experimental results obtained from the bonding interface analysis. An orthogonal experiment is conducted to observe the effects of various parameters, including the sealing gap, sealing length, sealing diameter, and sealing velocity on bonding strength. A method with the utilization of saturated vapor pressure inside a copper tube is proposed to evaluate bonding strength. A corresponding finite element model is developed to investigate the effects of sealing gap and sealing velocity on plastic deformation during the cold welding process. Effects of various parameters on the bonding strength are determined and it is found that the sealing gap is the most critical factor and that the sealing velocity contributes the least effect. The best parameter combination （AIB3CID3, with a 0.5 mm sealing gap, 6 mm sealing length, 3.8 mm sealing diameter, and 50 mm/s sealing velocity） is derived within the experimental parameters. Plastic deformation results derived from the finite element model are consistent with those from the experiment. The instruction for the CWSP of heat pipes and the design of sealing dies of heat pipes are provided.
基金National Natural Science Foundation of China(41275060)National Natural Science Foundation of China(41275145)+1 种基金National Key Basic Research Program of China(2014CB953903)Fundamental Research Funds for the Central Universities(131gjc03)
文摘We analyzed cloud microphysical processes' latent heat characteristics and their influence on an autumn heavy rain event over Hainan Island,China,using the mesoscale numerical model WRF and WRF-3DVAR system.We found that positive latent heat occurred far above the zero layer,while negative latent heat occurred mainly under the zero layer.There was substantially more positive latent heat than negative latent heat,and the condensation heating had the most important contribution to the latent heat increase.The processes of deposition,congelation,melting and evaporation were all characterized by weakening after their intensification;however,the variations in condensation and sublimation processes were relatively small.The main cloud microphysical processes for positive latent heat were condensation of water vapor into cloud water,the condensation of rain,and the deposition increase of cloud ice,snow and graupel.The main cloud microphysical processes for negative latent heat were the evaporation of rain,the melting and enhanced melting of graupel.The latent heat releases due to different cloud microphysical processes have a significant impact on the intensity of precipitation.Without the condensation and evaporation of rain,the total latent heating would decrease and the moisture variables and precipitation would reduce significantly.Without deposition and sublimation,the heating in high levels would decrease and the precipitation would reduce.Without congelation and melting,the latent heating would enhance in the low levels,and the precipitation would reduce.
基金supported by the National Natural Science Foundation of China(Grant No.62061028)the Foundation for Distinguished Young Scientists of Jiangxi Province(Grant No.20162BCB23009)+2 种基金the Open Research Fund Program of the State Key Laboratory of Low-Dimensional Quantum Physics(Grant No.KF202010)the Interdisciplinary Innovation Fund of Nanchang University(Grant No.9166-27060003-YB12)the Open Research Fund Program of Key Laboratory of Opto-Electronic Information Acquisition and Manipulation of Ministry of Education(Grant No.OEIAM202004)。
文摘Ground-state cooling of mesoscopic mechanical objects is still a major challenge in the unresolved-sideband regime.We present a frequency modulation(FM)scheme to achieve cooling of the mechanical resonator to its ground-state in a double-cavity optomechanical system containing a mechanical resonator.The mean phonon number is determined by numerically solving a set of differential equations derived from the quantum master equations.Due to efficient suppression of Stokes heating processes in the presence of FM,the ground-state cooling,indicated by numerical calculations,is significantly achievable,regardless of whether in the resolved-sideband regime or the unresolved-sideband regime.Furthermore,by choosing parameters reasonably,the improvement of the quantum cooling limit is found to be capable of being positively correlated with the modulation frequency.This method provides new insight into quantum manipulation and creates more possibilities for applications of quantum devices.
文摘The reducing efficiencies of the commonly used heat treatment methods and fermentation processes on aflatoxin M1 (AFM1) in Nigeria were investigated. Seventy samples of fresh cow milk from both conventional and traditional dairy cattle herds were collected and analyzed for the determination of AFM1 using Cobra-cell incorporated high performance liquid chromatography. Of these analyzed samples, 56 (80.0%) tested positive for AFM1 out of which 3 milk samples with high AFM1 concentrations were selectively pooled and subjected to varied conditions of heat treatments and fermentation processes using both indigenized and exotic strains of lactic acid bacteria (Lactobacillus bulgaricus + Streptococcus thermophilus and L. rhamnosus and L. plantarum) as starter cultures respectively. Both processes used either singly or combined, demonstrated high degrees of reducing effects on AFM1 levels. Sterilization of the milk at 121?C and 80?C under the same condition of time (15 - 20) min showed significant reduction of up to 58.8% (p 0.05) in the level of AFM1 when compared with the initial mean AFM1 concentration of the untreated fresh milk. The situation was however different around the boiling temperature of 100?C at which point the level of AFM1 reduction was found to be inconsistent. The indigenized combined strains showed some slight margins of AFM1 reduction in the proportions of (20.5, 30.8 and 43.9)% over and above that of the exotic strains (17.4, 30.0 and 41.1)% in 12 h, 48 h and 72 h of fermentation respectively. Generally, fermentation alone showed lower reduction of AFM1 in milk from 24.5% to 43.9% compared with the reducing activities of (35.4 to 58.8)% when heat-treated milk samples were subsequently subjected to varied fermentation conditions.
文摘According to heat transfer principle and the process of solving engineering problems by finite element method, examples were given to demonstrate how finite element analysis can be used to describe transient heat transfer through fabrics. Details were given to describe how conduction and convection affect temperature distribution and heat loss during heat transfer processes by taking advantage of the quick calculation of FEA software MSC.Marc. Experimental results show good agreement with the theoretical results.
基金supported by the National Basic Research Program of China (973 Program, Grant Nos. 2013CB430105 and 2014CB441403)the National Natural Science Foundation of China (Grant No. 41205099)+1 种基金Guizhou Province Scientific Research Joint Project (Grant No. G[2013]4001)the Special Scientific Research Project of Meteorological Public Welfare Profession of China (Grant No. GYHY201006031)
文摘An extraordinary rainstorm that occurred in Beijing on 21 July 2012 was simulated using the Weather Research and Forecasting model. The results showed that:(1) The two precipitation phases were based on a combination of cold cloud processes and warm cloud processes. The accumulated conversion amount and conversion rate of microphysical processes in the warm-area phase were all much larger than those in the cold front phase.(2) 72.6% of rainwater was from the warm-area phase. Rainwater mainly came from the melting of graupel and the melting of snow, while the accretion of cloud water by rain ranked second.(3) The net heating rate with height appeared as an overall warming with two strong heating centers in the lower and middle layers of the troposphere and a minimum heating center around the melting layer. The net heating effect in the warm-area phase was stronger than that in the cold front phase.(4) Warm cloud processes contributed most to latent heat release, and the thermal effect of cold cloud processes on the storm in the cold front phase was enhanced compared to that in the warm-area phase.(5) The melting of graupel and snow contributed most to latent heat absorption, and the effect of the evaporation of rainwater was significantly reduced in the cold front phase.
文摘The results of numerical simulation of the mosaic embedding iron ore sintering （MEBIOS） process according to the model presented in the first part of the study are introduced. The main objective of the second part is the elucidation of key factors influencing the process efficiency, particularly the sintering completeness, velocity of the heat wave propagation and maximum temperature achievable in the pellet during the wave propagation. Numerical results reveal that the mass fraction of coal, diameter of coal particles and air inlet velocity are of prime importance in determining efficiency of the MEBIOS sintering process.
文摘In-situ HVEM observation on phase transition of the YBa_2Cu_3O_(7-x) superconducting compound in pro- cess of heating was carried out,and high temperature X-ray diffraction analysis in air and X-ray diffraction phase analysis for the sample treated in vacuum condition were made.The results showed that the temperature of phase transition is related to oxygen content in the sample and in general,is 100℃ to 120℃ lower in vacu- um condition than in air.At 320℃ to 350℃ twin bands begin to disappear,and some Cu_2O are formed on the surface of the sample and transit from orthorhombic YBa_2Cu_3O_(7-x) to arthorhombic Y_2BaCuO_5 compound. This transition was completed at about 500℃.Above 900℃,this compound consists of the Y_2BaCuO_5, BaCuO_2,Y_2O_3 and some other minor compounds.No phase transition was observed during cooling the sample.
文摘The continuous constructive challenge to improve the functionality and efficiency of components always results in higher demands on production engineering, against the background of the generally increasing cost pressure. In many cases, you will just succeed in producing competitive and innovative products by combining and coupling of different procedures to an independent (hybrid) technology. The use of hybrid procedures for metal joining and heat treatment of metallic materials finds more and more industrial fields of application. Modern vacuum lines with integrated pressurized gas quenching are considered high-performance and flexible means of production for brazing and heat treatment tasks as well in the turbine industry as in the mould making and tool manufacturing industry. In doing so, the heat treatment is coupled with the brazing cycle in a combined process so that the brazing temperatures and soak times are adapted to the necessary temperatures and times for solution heat treatment and austeniting. This user-oriented article describes on the one hand examples of brazing of turbine components, but above all the practical experience from the plastics processing industry, where the requirement for a high-efficient cooling of injection moulding dies gains more and more importance. The combined procedure "Vacuum Brazing and Hardening" offers plenty of possibilities to produce mould inserts with an efficient tempering system in an economic way.
文摘The plan of heat-treatment process for 2014Al alloy is designed using orthogonal method, the heat-treatment experiments are made and the mechanical properties are tested according to the designed plan. The effect of solid solution temperature, ageing temperature, ageing time on microscopic mechanism of the mechanical properties of the 2014Al alloy is studied using microscope, transmission electron microscope. The best heat treatment process of the 2014Al alloy is developed. The experimental results indicate that the strength σ<sub>b</sub>, yield stress σ<sub>0.2</sub>, percentage elongation δ of the alloy reach separately 490～500 MPa, 450～490 MPa, 10～12％ adopting the new heat treatment process. Compared with GB, the strength increases 20～30％, the percentage elongation increases 30～40％. The mechanism of the new heat-treatment process is also discussed.
文摘Three-dimensional thermal a nalysis simulation of a horizontal zone refining system is conducted for germanimn semiconductor materials. The considered geometry includes a g＇ral）hite boat filled with germanium placed in a cylindrical quartz tube. A flow of Ar and H2 gas mixture is purged througll the tube. A narrow section of the, boat is assmned to be exposed to a constant heat rate produced b v an rf coil located outside the quartz tube. The results of this analysis provide essential information about various parameters such as the shape of tile molten zone, required power and temperature gradient in the system.
