For effectively removing the water-based drilling fluid filter cake and improving interfacial cementing strength and cementing quality,a new type of cementation flushing fluid(WD-C)was developed based on the strong fl...For effectively removing the water-based drilling fluid filter cake and improving interfacial cementing strength and cementing quality,a new type of cementation flushing fluid(WD-C)was developed based on the strong flushing principle of water soluble fiber and the oxygenolysis principle of filter cake.It is composed of 0.5%WF-H fiber,2.2%WF-O oxidant,0.35%FeSO_(4),1.8%KCl,3.0%swollen powder perlite and water with its density of 1.03 g/cm^(3).This cementation flushing fluid was systematically tested and evaluated in terms of its washing efficiency on the filter cake of water-based drilling fluid and its capacity to improve the bonding strength of cementation interface.In addition,an analysis was performed of its effect on the physical-chemical characteristics and the micro-structures of interfacial cements by means of infrared spectrum(IR),scanning electron microscope(SEM)and energy dispersive X-ray detector(EDS).It is shown that the new cementation flushing fluid presents excellent washing effect on water-based drilling fluid filter cake(with washing time within 10 min).The cement particles at the cemented interface can be hydrated normally,and hydrated calcium silicate gel,Ca(OH)_(2)and rod-shaped ettringite(AFt)crystal are generated and interwoven with each other.In this way,dense network structures are formed,so the bonding strength of the second cementing interface rises significantly,and then cementing quality is improved.Based on the research results,one more technology is set up for removing the water-based drilling fluid filter cake efficiently and improving the bonding strength of the second cementing interface.展开更多
Because there are plenty of clay particles in the flush fluid of Pingguo Aluminum Mine, the consolidationtechnology in geotechnical engineering was adopted to carry out the disassociation of water and soil disassociat...Because there are plenty of clay particles in the flush fluid of Pingguo Aluminum Mine, the consolidationtechnology in geotechnical engineering was adopted to carry out the disassociation of water and soil disassociation. Inthis method, vacuum method, electro-osmosis and chemical flocculation were used comprehensively to separate soilfrom flush fluid. The experiments of the method of "vacuum + electro-osmosis" for drainage was made. After pretreat-ing the flush fluid, suction pressure was offered by the sand well in the bottom and electro-osmosis was used to drainoff water. The results of the experiment show that the good effect can be obtained in drainage when the electric gradi-ent is greater than 8.3 V/cm and the quantity of sand well is more than 6. In industrial production, it is necessary to in-crease the quantity of sand well, to arrange the electrodes rationally and to set up an intermittent electric circuit. On thebasis of the experiments , the industrial feasible flow was put forward. It may be a helpful attempt to apply consolida-tion technology to the fields of the environmental protection and so on.展开更多
基金Supported by National Natural Science Foundation of China(Grand No.51174226)National Science and Technology Major Project(Grand No.2009ZX05060)。
文摘For effectively removing the water-based drilling fluid filter cake and improving interfacial cementing strength and cementing quality,a new type of cementation flushing fluid(WD-C)was developed based on the strong flushing principle of water soluble fiber and the oxygenolysis principle of filter cake.It is composed of 0.5%WF-H fiber,2.2%WF-O oxidant,0.35%FeSO_(4),1.8%KCl,3.0%swollen powder perlite and water with its density of 1.03 g/cm^(3).This cementation flushing fluid was systematically tested and evaluated in terms of its washing efficiency on the filter cake of water-based drilling fluid and its capacity to improve the bonding strength of cementation interface.In addition,an analysis was performed of its effect on the physical-chemical characteristics and the micro-structures of interfacial cements by means of infrared spectrum(IR),scanning electron microscope(SEM)and energy dispersive X-ray detector(EDS).It is shown that the new cementation flushing fluid presents excellent washing effect on water-based drilling fluid filter cake(with washing time within 10 min).The cement particles at the cemented interface can be hydrated normally,and hydrated calcium silicate gel,Ca(OH)_(2)and rod-shaped ettringite(AFt)crystal are generated and interwoven with each other.In this way,dense network structures are formed,so the bonding strength of the second cementing interface rises significantly,and then cementing quality is improved.Based on the research results,one more technology is set up for removing the water-based drilling fluid filter cake efficiently and improving the bonding strength of the second cementing interface.
文摘Because there are plenty of clay particles in the flush fluid of Pingguo Aluminum Mine, the consolidationtechnology in geotechnical engineering was adopted to carry out the disassociation of water and soil disassociation. Inthis method, vacuum method, electro-osmosis and chemical flocculation were used comprehensively to separate soilfrom flush fluid. The experiments of the method of "vacuum + electro-osmosis" for drainage was made. After pretreat-ing the flush fluid, suction pressure was offered by the sand well in the bottom and electro-osmosis was used to drainoff water. The results of the experiment show that the good effect can be obtained in drainage when the electric gradi-ent is greater than 8.3 V/cm and the quantity of sand well is more than 6. In industrial production, it is necessary to in-crease the quantity of sand well, to arrange the electrodes rationally and to set up an intermittent electric circuit. On thebasis of the experiments , the industrial feasible flow was put forward. It may be a helpful attempt to apply consolida-tion technology to the fields of the environmental protection and so on.
