There is a constant search for biomaterials from natural products like plants for food and industrial applications.The work embodied in this report aimed at investigating the effects of microwave-assisted and soxhlet ...There is a constant search for biomaterials from natural products like plants for food and industrial applications.The work embodied in this report aimed at investigating the effects of microwave-assisted and soxhlet extraction(MAE and SE) techniques on the functional physicochemical quality characteristics of Moringa oleifera seed oil and proteins extracts. M. oleifera seeds were ground to fine powders and oil was extracted by microwave-assisted and soxhlet extraction techniques using petroleum ether. Quality attributes including yield percent, moisture content,iodine, saponification, specific gravity, viscosity, p H, thiobarbituric acid, acid and peroxide values were measured. Mineral and vitamin contents, chemical/functional groups, fatty acid(FA) composition, and reducing power of the oil were evaluated. Metabolomics of protein extracted from the defatted powders were analyzed by nuclear magnetic resonance(NMR). M. oleifera oil from MAE and SE methods had good yield(34.25 ± 0.0%,28.75 ± 0.0%), low moisture content(0.008 ± 0.0%, 0.011 ± 0.0%), non-drying and unsaturated, moderately saponified, less dense(0.91 ± 0.01, 0.92 ± 0.02 g m L^(-1)), had Newtonian flow, were weakly acidic, showed good content of FAs, recorded strong potential for long shelf-life, showed stability against oxidative rancidity and enzymatic hydrolysis, had very rich deposits of micro-and macro-nutrients as well as water-soluble and lipidsoluble vitamins, and functional groups in the oil were reflective of its content of long-and medium-chain triglycerides(LCT and MCT). Monounsaturated and saturated fatty acids(MUFA and SFA) were detected and the oil has excellent ferric ion reducing power. NMR metabolomic assay revealed the presence of nine essential amino acids(EAAs) in the protein extract. MAE technique is a feasible and acceptable alternative for high throughput extraction of M. oleifera oil with high yield and excellent quality attributes. The study revealed that MAE did not impart any remarkable advantage(s) on the physicochemical properties of M. oleifera seed oil and protein compared to SE technique.展开更多
Most image saliency detection models are dependent on prior knowledge and demand high computational cost. However, spectral residual（SR） and phase spectrum of the Fourier transform（PFT） models are simple and fast ...Most image saliency detection models are dependent on prior knowledge and demand high computational cost. However, spectral residual（SR） and phase spectrum of the Fourier transform（PFT） models are simple and fast saliency detection approaches based on two-dimensional Fourier transform without the prior knowledge. For seismic data, the geological structure of the underground rock formation changes more obviously in the time direction. Therefore, one-dimensional Fourier transform is more suitable for seismic saliency detection. Fractional Fourier transform（FrFT） is an improved algorithm for Fourier transform, therefore we propose the seismic SR and PFT models in one-dimensional FrF T domain to obtain more detailed saliency maps. These two models use the amplitude and phase information in FrFT domain to construct the corresponding saliency maps in spatial domain. By means of these two models, several saliency maps at different fractional orders can be obtained for seismic attribute analysis. These saliency maps can characterize the detailed features and highlight the object areas, which is more conducive to determine the location of reservoirs. The performance of the proposed method is assessed on both simulated and real seismic data. The results indicate that our method is effective and convenient for seismic attribute extraction with good noise immunity.展开更多
Differences are found in the attributes of microseismic events caused by coal seam rupture,underground structure activation,and groundwater movement in coal mine production.Based on these differences,accurate classific...Differences are found in the attributes of microseismic events caused by coal seam rupture,underground structure activation,and groundwater movement in coal mine production.Based on these differences,accurate classification and analysis of microseismic events are important for the water inrush warning of the coal mine working facefloor.Cluster analysis,which classifies samples according to data similarity,has remarkable advantages in nonlinear classification.A water inrush early warning method for coal minefloors is proposed in this paper.First,the short time average over long time average(STA/LTA)method is used to identify effective events from continuous microseismic records to realize the identification of microseismic events in coal mines.Then,ten attributes of microseismic events are extracted,and cluster analysis is conducted in the attribute domain to realize unsupervised classification of microseismic events.Clustering results of synthetic andfield data demonstrate the effectiveness of the proposed method.The analysis offield data clustering results shows that thefirst kind of events with time change rules is of considerable importance to the early warning of water inrush from the coal mine working facefloor.展开更多
基金funded by International Foundation for Science(IFS)and Organisation for the Prohibition of Chemical Weapons(OPCW)research grant awarded to Dr.Chukwuebuka Emmanuel Umeyor in 2019(Grant number:I-2-F-6448-1).
文摘There is a constant search for biomaterials from natural products like plants for food and industrial applications.The work embodied in this report aimed at investigating the effects of microwave-assisted and soxhlet extraction(MAE and SE) techniques on the functional physicochemical quality characteristics of Moringa oleifera seed oil and proteins extracts. M. oleifera seeds were ground to fine powders and oil was extracted by microwave-assisted and soxhlet extraction techniques using petroleum ether. Quality attributes including yield percent, moisture content,iodine, saponification, specific gravity, viscosity, p H, thiobarbituric acid, acid and peroxide values were measured. Mineral and vitamin contents, chemical/functional groups, fatty acid(FA) composition, and reducing power of the oil were evaluated. Metabolomics of protein extracted from the defatted powders were analyzed by nuclear magnetic resonance(NMR). M. oleifera oil from MAE and SE methods had good yield(34.25 ± 0.0%,28.75 ± 0.0%), low moisture content(0.008 ± 0.0%, 0.011 ± 0.0%), non-drying and unsaturated, moderately saponified, less dense(0.91 ± 0.01, 0.92 ± 0.02 g m L^(-1)), had Newtonian flow, were weakly acidic, showed good content of FAs, recorded strong potential for long shelf-life, showed stability against oxidative rancidity and enzymatic hydrolysis, had very rich deposits of micro-and macro-nutrients as well as water-soluble and lipidsoluble vitamins, and functional groups in the oil were reflective of its content of long-and medium-chain triglycerides(LCT and MCT). Monounsaturated and saturated fatty acids(MUFA and SFA) were detected and the oil has excellent ferric ion reducing power. NMR metabolomic assay revealed the presence of nine essential amino acids(EAAs) in the protein extract. MAE technique is a feasible and acceptable alternative for high throughput extraction of M. oleifera oil with high yield and excellent quality attributes. The study revealed that MAE did not impart any remarkable advantage(s) on the physicochemical properties of M. oleifera seed oil and protein compared to SE technique.
基金supported by the National Natural Science Foundation of China (Nos.61571096,61775030,41274127,41301460,and 40874066)
文摘Most image saliency detection models are dependent on prior knowledge and demand high computational cost. However, spectral residual（SR） and phase spectrum of the Fourier transform（PFT） models are simple and fast saliency detection approaches based on two-dimensional Fourier transform without the prior knowledge. For seismic data, the geological structure of the underground rock formation changes more obviously in the time direction. Therefore, one-dimensional Fourier transform is more suitable for seismic saliency detection. Fractional Fourier transform（FrFT） is an improved algorithm for Fourier transform, therefore we propose the seismic SR and PFT models in one-dimensional FrF T domain to obtain more detailed saliency maps. These two models use the amplitude and phase information in FrFT domain to construct the corresponding saliency maps in spatial domain. By means of these two models, several saliency maps at different fractional orders can be obtained for seismic attribute analysis. These saliency maps can characterize the detailed features and highlight the object areas, which is more conducive to determine the location of reservoirs. The performance of the proposed method is assessed on both simulated and real seismic data. The results indicate that our method is effective and convenient for seismic attribute extraction with good noise immunity.
基金supported in part by the National Natural Science Foundation of China under Grant 41904098in part by the Beijing Nova Program under Grant 2022056in part by the National Natural Science Foundation of China (52174218)。
文摘Differences are found in the attributes of microseismic events caused by coal seam rupture,underground structure activation,and groundwater movement in coal mine production.Based on these differences,accurate classification and analysis of microseismic events are important for the water inrush warning of the coal mine working facefloor.Cluster analysis,which classifies samples according to data similarity,has remarkable advantages in nonlinear classification.A water inrush early warning method for coal minefloors is proposed in this paper.First,the short time average over long time average(STA/LTA)method is used to identify effective events from continuous microseismic records to realize the identification of microseismic events in coal mines.Then,ten attributes of microseismic events are extracted,and cluster analysis is conducted in the attribute domain to realize unsupervised classification of microseismic events.Clustering results of synthetic andfield data demonstrate the effectiveness of the proposed method.The analysis offield data clustering results shows that thefirst kind of events with time change rules is of considerable importance to the early warning of water inrush from the coal mine working facefloor.
文摘目的研究金荞麦(Fagopyri Dibotryis Rhizoma,FDR)从饮片到标准汤剂的关键质量属性传递规律。方法收集15批FDR饮片,制备标准汤剂,测定出膏率,建立饮片和标准汤剂的高效液相色谱(HPLC)指纹图谱,采用超快速液相色谱-四级杆飞行时间质谱(ultra fast liquid chromatography quadrupole time-of-flight mass spectrometry,UFLC-Q-TOF-MS/MS)技术对标定的共有峰进行成分鉴定,HPLC法测定其中10个指标性成分的含量,以出膏率、指纹图谱共有峰传递数、指标性成分转移率为关键质量属性,分析从饮片到标准汤剂的传递规律。结果FDR饮片指纹图谱标定共有峰56个,其中38个传递到了标准汤剂,共有峰个数传递率67.86%,56个共有峰共鉴定了93个成分,包括鞣质类成分33个,酚类成分22个,黄酮类成分、苯丙素苷类成分各14个,氨基酸类成分4个,有机酸类成分3个,萜类成分、生物碱类成分及其他类成分各1个,其中6个鞣质类成分(原花青素A2、原花青素B1、原花青素B2、原花青素B3、原花青素C1和原花青素C2)、3个酚类成分(原儿茶酸、没食子酸和原儿茶醛)、4个黄酮类成分(儿茶素、表儿茶素、表儿茶素没食子酸酯和芦丁)采用对照品比对确认,原儿茶酸、没食子酸、原儿茶醛、原花青素A2、原花青素B1、原花青素B3、原花青素C1、儿茶素、表儿茶素、表儿茶素没食子酸酯平均转移率分别为115.50%、81.36%、126.36%、36.86%、69.60%、47.15%、43.10%、86.78%、69.00%、16.18%,标准汤剂的出膏率范围为6.36%~10.61%。结论本研究为FDR配方颗粒制备工艺和质量标准研究奠定了基础。
