This study investigates the effect of high current density electropulsing on the material in a rapid stress relaxation process.An AISI 1020 steel was shot-peened to induce surface compressive residual stresses in a co...This study investigates the effect of high current density electropulsing on the material in a rapid stress relaxation process.An AISI 1020 steel was shot-peened to induce surface compressive residual stresses in a controlled manner and subsequently electropulsed to investigate the changes in microstructure and defect configuration.AISI 1020 steel was chosen as it has a simple microstructure(plain ferritic)and composition with low alloying conditions.It is an appropriate material to study the effect of trans-mitting electric pulses on the microstructural defect evolution.A combination of electron-backscattered diffraction and transmission electron microscopy proved to be an effective tool in characterizing the post-electropulsing effects critically.By application of electropulsing,a reduction in the surface residual stress layer was noticed.Also,reductions in misorientation and dislocation density together with the disentan-glement of dislocations within the cold-worked layer were observed after electropulsing.Additionally,the annihilation of shot-peening-induced deformation bands beyond the residual layer depth was observed.These effects have been rationalised by taking into account the various possibilities of athermal effects of electropulsing.展开更多
The fatigue life of components can be significantly enhanced by the formation of the surface hardness layer through surface strengthening technology.To avoid the geometric distortion of thin-walled com-ponents caused ...The fatigue life of components can be significantly enhanced by the formation of the surface hardness layer through surface strengthening technology.To avoid the geometric distortion of thin-walled com-ponents caused by strengthening,the strengthening energy is limited and the ideal strengthening effect cannot be obtained.This work aims to propose a novel approach to address this issue effectively.The surface layer with high-density dislocations was obtained by a low-energy surface strengthening method(shot peening)at first.Then the surface strengthening mechanism changes from dislocation strengthen-ing to grain boundary strengthening after electropulsing treatment(EPT).The evolution of residual stress and microstructure was analyzed using multi-scale characterization techniques.The results demonstrate that EPT followed by surface strengthening makes a remarkable 304%increase in fatigue life of TC11 titanium alloy.The enhancement of fatigue life can be attributed to the grain refinement accompanied by the formation of nanotwins and sub-grains in the surface-strengthened layer,as well as the reduction in dislocation density within the substrate after EPT.This study demonstrates the significant potential of EPT in further enhancing the fatigue life of surface pre-strengthened thin-walled components.展开更多
Mg-Nd-Zn-Zr(JDBM)alloy was studied as a candidate for biodegradable implant material because of its moderate mechanical properties,good biocompatibility,and favorable uniform degradation behavior.To verify whether JDB...Mg-Nd-Zn-Zr(JDBM)alloy was studied as a candidate for biodegradable implant material because of its moderate mechanical properties,good biocompatibility,and favorable uniform degradation behavior.To verify whether JDBM alloy exhibits electroplasticity effect and then study the mechanism of electropulsing treatment on JDBM alloy,in this study,homogenized and pre-tensile deformed samples were treated by electropulsing.After the electropulsing treatment,the average grain size was refined due to recrystallization,micron-scale Mg12Nd secondary phases precipitated slightly,while the morphology of nanoscale Zr particles changed from rodlike to ellipsoidal shape.The elongation to failure(EL)increased obviously for the homogenized and pre-tensile deformed JDBM alloy samples after electropulsing treatment,accompanying with no obvious sacrifice of the yield strength(YS)for the former and an evident decrease of YS for the latter,mainly due to the reduction of the dislocation density.The YS decrement and EL increment(77.57%)for the latter are more apparent attributed to the higher density of dislocations introduced by pre-tensile deformation.Therefore,the electropulsing treatment can obviously improve the mechanical properties of JDBM alloy,especially for the plasticity.The present work opens a new window for the fabrication of JDBM alloy profiles with high mechanical properties,especially for the plasticity,such as the cold drawing wires and tubes for biomedical applications.It also could provide theoretical references for other magnesium alloy processing.展开更多
Electron backscattered diffraction （EBSD） and transmission electron microscopy （TEM） were used to investigate effect of electropulsing on microstructure and texture evolution of Ti-6Al-4V during cold drawing. Rese...Electron backscattered diffraction （EBSD） and transmission electron microscopy （TEM） were used to investigate effect of electropulsing on microstructure and texture evolution of Ti-6Al-4V during cold drawing. Research results demonstrate that the electropulsing treatment （EPT） can enhance the deformability of the grains with unfavorable orientations, which makes the compatibility of deformation among grains much better. A comparison in texture evolution between conventional cold drawing and EPT cold drawing indicates that the EPT promotes prismatic 〈a〉 slip moving, restricts pyramidal 〈c＋a〉 slip occurring and accommodates the deformation with c-component by grain boundary sliding. The fraction decrease of low-angle grain boundaries for samples deformed with EPT reveals that the application of electropulsing restricts the formation of the incidental dislocation boundaries and the geometrically necessary boundaries.展开更多
In order to optimize the ductility of orthorhombic Ti2AlNb-based alloys sheet,Ti22Al27Nb sheet was treated by high density electropulsing（J max =6.80 7.09 kA/mm2,tp =110 μs） under ambient condition.Microstructures ...In order to optimize the ductility of orthorhombic Ti2AlNb-based alloys sheet,Ti22Al27Nb sheet was treated by high density electropulsing（J max =6.80 7.09 kA/mm2,tp =110 μs） under ambient condition.Microstructures were observed by SEM,and the tensile properties were also studied using uniaxial tension tests.The experimental results show that electropulsing can refine the microstructures of Ti22Al27Nb sheets.The specimen with the fine and homogeneous microstructures has good plasticity,and its elongation reaches 19.4%.The mechanism about the effect of electropulsing treatment on the microstructure of Ti22Al27Nb sheets was discussed.It was thought that the increase in nucleation rate during phase transformation and a very short treating time were regarded as the main reasons of producing smaller grains and increase in the plasticity by electropulsing.展开更多
To investigate the effect of the electropulsing on dislocation mobility,specimens cut from the cold-rolled titanium sheet were treated by high density electropulsing with the maximum current density of 7.22,7.64,7.96 ...To investigate the effect of the electropulsing on dislocation mobility,specimens cut from the cold-rolled titanium sheet were treated by high density electropulsing with the maximum current density of 7.22,7.64,7.96 kA/mm 2 ,pulse period 110μs.The internal friction and elastic modulus were measured by a dynamic mechanical analyzer（DMA）.When strain amplitude lowers a certain critical one,the damping of the electropulsed titanium sheet is lower than that of the cold-rolled one.When the strain amplitude exceeds the critical one,the damping of the electropulsed titanium sheet is extraordinarily higher than that of the cold-rolled or conventional annealed one.Furthermore,it is found that the damping peak of the electropulsed titanium sheet shifts to lower temperature compared with the conventional annealed one.It is demonstrated that the electropulsing treatment can decrease dislocation tangles and enhance dislocation mobility.展开更多
Specimens cut from the cold-rolled commercially pure （CP） Ti sheet were treated by high density electropulsing （the maximum current density 7.22 kA/mm2, pulse period 110 las）. The deformation behaviors of the CP T...Specimens cut from the cold-rolled commercially pure （CP） Ti sheet were treated by high density electropulsing （the maximum current density 7.22 kA/mm2, pulse period 110 las）. The deformation behaviors of the CP Ti specimens at different states were determined by the uniaxial tensile test. The microstructure morphologies were observed by the optical microscopy. The results show that the electropulsing induced formation of f＇me equal-axial grains and lamellar microstructures, which leads to the strength of the electropulsed CP Ti higher than that of the conventional annealed CP Ti. After electropulsing, the tensile strength and yield strength are increased by 100 MPa. And the electropulsed CP Ti has a good plasticity. The experimental results demonstrate that the electropulsing provides an effective approach to enhance the strength of cold-rolled CP Ti sheet and retain the required high ductility.展开更多
Electropulsing rolling （ER） and warm rolling （WR） processes were performed to roll AZ31 magnesium alloy sheets. Mechanical properties, microstructure and texture evolution of these specimens were investigated afte...Electropulsing rolling （ER） and warm rolling （WR） processes were performed to roll AZ31 magnesium alloy sheets. Mechanical properties, microstructure and texture evolution of these specimens were investigated after rolling. The results indicate that electropulsing accelerates the recrystallization of AZ31 alloy sheets during hot rolling. After electropulsing rolling at a relatively low temperature, the microstructure of the sample shows fine equiaxed recrystallized grains with a lower density of dislocations and precipitates. In contrast, the microstructure of the sample after warm rolling shows elongated grain, numerous deformed twins, and a high density of dislocation and precipitates. Electropulsing rolling helps weaken the basal fiber texture. Although both the alloy sheets （ER and WR） have typical basal fiber texture, the maximum pole intensity of basal in ER sample is weaker. ER sheet has higher yield strength and elongation compared to WR sheet. As a promising technique, electropulsing rolling can be used to improve the microstructure and mechanical properties of materials.展开更多
Electropulsing treatment（EPT） was performed on a nickel base corrosion resistant alloy during aging.The effect of EPT on the microstructure and corrosion resistance of the alloy and the mechanisms were investigated....Electropulsing treatment（EPT） was performed on a nickel base corrosion resistant alloy during aging.The effect of EPT on the microstructure and corrosion resistance of the alloy and the mechanisms were investigated.The results show that the intergranular corrosion resistance can be improved substantially without the degradation of mechanical properties of the alloy by EPT.The EPT has an effect of enhancing the interface diffusion rate of the alloying element,which is higher than the body diffusion rate.And thus discontinuous precipitation of M23C6 type carbides appears at the grain boundary in the alloy by EPT,which decreases the depletion extent of the alloying elements at the grain boundary substantially.As a result,the intergranular corrosion resistance of the alloy can be improved by the EPT without any degradation of mechanical properties.展开更多
Studies show that the proper solid solution treatment(SST)is a key step in the precipitation strengthening of AA7150 Al alloy.Despite the superior characteristics of the fully dissolved phase,it has major drawbacks,in...Studies show that the proper solid solution treatment(SST)is a key step in the precipitation strengthening of AA7150 Al alloy.Despite the superior characteristics of the fully dissolved phase,it has major drawbacks,including high consumption of energy and low efficiency.Recently,electropulsing treatment(EPT)has been proposed to study dissolved precipitations and modify microstructures of AA7150 Al alloy faster than conventional SST.Experiments have been conducted in the present article,and the obtained results show that EPT can promote the rapid dissolution of theη’phase at relatively low temperatures in only 20 s.Meanwhile,the strength and ductility of electropulsed samples decrease drastically.Compared with conventional SST,EPT accelerates recrystallization and obtains relatively fine grains after 20 and 50 s electric pulses.Moreover,as the EPT time increases,the corresponding non-uniform local heating and the electron force promote dislocation generation and annihilation.展开更多
The influence of electropulsing on the creep behaviour,strength,and microstructure of an Al−Cu−Li alloy during creep ageing was investigated.Electropulsing assisted creep ageing(ECA)and conventional creep ageing(CCA)w...The influence of electropulsing on the creep behaviour,strength,and microstructure of an Al−Cu−Li alloy during creep ageing was investigated.Electropulsing assisted creep ageing(ECA)and conventional creep ageing(CCA)were carried out under various stress levels and time conditions.Applying electropulsing results in a noteworthy change of creep behaviour,including a variation in creep curves,an increased creep rate in early stage,and an improved creep strain.The ECA specimen experiences a shorter time to the peak strength,and an increase in elongation by~17.4% without loss of the peak-aged strength compared with CCA specimen.The ultrafine nano-size subgrains are observed to form under electropulsing,which can result in an increased creep strain by increasing grain-boundary sliding.The enhancement of both dislocation interactions and solute diffusion under electropulsing is considered as a primary cause of disappearance of a platform stage during early creep ageing.Some of T1 precipitates around the grain boundary are observed in the peak ECA sample,resulting in an occurrence of transgranular fracture,which is further responsible for an increased elongation of the ECA specimen.展开更多
The specimens cut from the cold-rolled pure titanium sheet at 0°,45°and 90°to the rolling direction were treated by high density electropulsing(maximum current density J=(7.22-7.96)×10^(3)A/mm^(2),...The specimens cut from the cold-rolled pure titanium sheet at 0°,45°and 90°to the rolling direction were treated by high density electropulsing(maximum current density J=(7.22-7.96)×10^(3)A/mm^(2),pulse period t_(p)=110μs).The mechanical properties and microstructures of the cold-rolled,electropulsed and conventional annealed commercially pure titanium sheet were examined by using uniaxial tension test machine and optical microscope(OM),respectively.The results show that the deformation behavior of the electropulsed pure titanium sheet is significantly different from that of conventional annealed pure titanium sheet.The difference of the mechanical properties between the 0°,45°and 90°direction specimens is almost diminished.It is mainly due to the increase in dislocation mobility and formation of lamellar microstructure after the electropulsing.展开更多
Electropulsing-induced recrystallization and its effect on mechanical properties of oriented silicon steel strips （Fe-3.0%Si） were studied by optical microscopy, scanning electron microscopy and electron back-scatte...Electropulsing-induced recrystallization and its effect on mechanical properties of oriented silicon steel strips （Fe-3.0%Si） were studied by optical microscopy, scanning electron microscopy and electron back-scatter diffraction. The results indicated that electropulsing accelerated recrystallization, and decreased the temperature of recrystallization. Electropulsing favors refinement of the grain structure of the alloy. Effects of electropulsing on strength and elongation of the alloy were discussed from the point view of dislocation dynamics, microstructural changes, and electropulsing kinetics.展开更多
Conventional kinetics theory for diffusion-controlled phase transformation shows that the reverse transition should lag behind the temperature rise through rapid heating,i.e.,overheating is required.In this work,we fo...Conventional kinetics theory for diffusion-controlled phase transformation shows that the reverse transition should lag behind the temperature rise through rapid heating,i.e.,overheating is required.In this work,we found that theβ-transus temperature decreased by∼50℃ during studying theα→βtransformation in Ti-6Al-4V alloy via electropulsing treatment(EPT).The calculation suggests that the acceleration of transformation kinetics cannot be fully explained by Joule heat and athermal effects of the electromigration effect and electron wind theory.The microstructural evolution during EPT was systematically investigated utilizing scanning electron microscope(SEM),electron backscattered diffraction(EBSD),X-ray diffraction(XRD),transmission Kikuchi diffraction(TKD),and transmission electron micro-scope(TEM).Microscopic analysis shows that the nano-sizedωand O'phases formed in theβphase,which causes large numbers of lattice distortion regions.The defects are conducive to accelerating the bulk diffusion of alloying elements inβ.Moreover,the nanodomains limited the growth of martensite,therefore nanocrystalline martensite formed after quenching.These findings develop the understanding of the destructive effect of current on metallic crystal,which will help to guide microstructural regulation in titanium and other alloys.展开更多
The effect of electropulsing treatment on microstructure and mechanical strength of laser metal deposited Ti−6Al−4V alloy was investigated in order to eliminate the anisotropy in strength of laser metal deposited Ti−6...The effect of electropulsing treatment on microstructure and mechanical strength of laser metal deposited Ti−6Al−4V alloy was investigated in order to eliminate the anisotropy in strength of laser metal deposited Ti−6Al−4V alloy by tensile tests,optical microscopy,scanning electron microscopy,electron back-scattered diffraction analyses and transmission electron microscopy.With increasing applied voltages from 0 to 130 V,the evolution of microstructure within columnarβgrains followed the sequence ofα′martensite→colonyαstructure→basket-weaveαstructure.The electropulsing treated at 130 V weakened the texture of martensite withinβgrains.The as-built Ti−6Al−4V alloy showed an anisotropy in yield strength(6.2%).After processing at 130 V,the anisotropy in yield strength was reduced to 0.6%,which was attributed to the almost equivalent distribution of Schmid factor in the samples deformed along different orientations.展开更多
Electropulsing is introduced into the cutting process for quenched and tempered 45 steel, which is a novel method to improve the material machinability compared with the conventional cutting process. The effects of el...Electropulsing is introduced into the cutting process for quenched and tempered 45 steel, which is a novel method to improve the material machinability compared with the conventional cutting process. The effects of electropulsing on cutting performances, microstructure evolution, and surface qualities of 45 steel rods were studied. The results indicate that electropulsing is beneficial for the cutting process in 3 aspects as follows：（1） reducing the principal cutting force, surface microhardness and surface roughness of the machined sample dramatically;（2） improving the machining efficiency and prolonging the life of cutting tools;（3） decreasing the thickness of rheological layer which was usually caused by work hardening in the cutting process. The morphology and microstructure of the cutting chips showed that the length of the chips increased significantly with the increase of the current density. The advantage of electropulsing is that it can improve the plastic deformation capability as well as increase the lubricating property between the specimen and the cutting tool.展开更多
We explore the application of electropulsing for the control of phase transformation in a low-carbon steel.The effect of electropulsing on the transformation from austenite to ferrite in continuous casting low-carbon ...We explore the application of electropulsing for the control of phase transformation in a low-carbon steel.The effect of electropulsing on the transformation from austenite to ferrite in continuous casting low-carbon steel slab has been studied through experimental and thermodynamic investigations.The results reveal that electropulsing promotes the precipitation of ferrite within austenite grain in the low-carbon steel.When the electropulsing intensity increases,the precipitation of ferrite increases within austenite grains,and ferrite omentum precipitates become thinner along the austenite grain boundary.The results provide a basis for controlling the austenite to ferrite transformation in low-carbon steel.展开更多
The effect of electropulsing on the mechanical behaviors and microstructures of Ti-6Al-4V titanium alloy was investigated by an uniaxial tensile test. Compared to the value measured in cold tensile test, the alloy exh...The effect of electropulsing on the mechanical behaviors and microstructures of Ti-6Al-4V titanium alloy was investigated by an uniaxial tensile test. Compared to the value measured in cold tensile test, the alloy exhibits lower ultimate tensile strength when the tensile deformation is assisted by electropulsing. The tensile elongation is found to vary non-monotonically with increasing root mean square(RMS) current density. Though decreasing at first, the tensile elongation increases with current density once the value exceeds 8.1 A/mm^2. Through applying current with RMS current density of 12.7 A/mm^2, the tensile elongation at strain rate 0.001 s^(-1) can be improved by 94.1%. In addition, it is observed that more remarkable electroplastic effect is induced by the higher peak current density under similar thermal effect. Microstructure analysis reveals that the low plasticity at 8.1 A/mm^2 is attributed to the micro-void easily formation near the tips of acicular β phases. The enhanced ductility at higher current densities, on the other hand, is attributed to the dynamic recrystallization.展开更多
The effect of electropulsing treatment（EPT）on the microstructure of a Ti-based bulk metallic glass（BMG）has been studied.The maximum current density applied during EPT can exert a crucial role on tuning the microst...The effect of electropulsing treatment（EPT）on the microstructure of a Ti-based bulk metallic glass（BMG）has been studied.The maximum current density applied during EPT can exert a crucial role on tuning the microstructure of the BMG.When the maximum current density is no more than 2 720A/mm^2,the samples retains amorphous nature,whereas,beyond that,crystalline phases precipitate from the glassy matrix.During EPT,the maximum temperature within the samples EPTed at the maximum current densities larger than 2 720A/mm^2 is higher than the crystallization temperature of the BMG,leading to the crystallization event.展开更多
The effects of dynamic electropulsing on microstructure changes and phase transformations of a rolled Mg-9Al-1Zn alloy were studied by using optical microscopy, X-ray diffraction, back-scattered scanning microscopy an...The effects of dynamic electropulsing on microstructure changes and phase transformations of a rolled Mg-9Al-1Zn alloy were studied by using optical microscopy, X-ray diffraction, back-scattered scanning microscopy and transmission electron microscopy techniques. The decomposition of β phase was accelerated under dynamic electropulsing, compared with the conventional thermal processes. Dynamic electropulsing was less effective in affecting the phase transformations, but more effective in reducing residual stress than the static electropulsing. Dynamic electropulsing improved machinability of single point diamond turning, the mechanism of which is discussed from the point of view of dislocation dynamics.展开更多
基金supported by the National Research Foundation of Singapore,Rolls-Royce Singapore Pte.Ltd.,and Nanyang Technological University through grants#002123-00009 and #002124-00009.
文摘This study investigates the effect of high current density electropulsing on the material in a rapid stress relaxation process.An AISI 1020 steel was shot-peened to induce surface compressive residual stresses in a controlled manner and subsequently electropulsed to investigate the changes in microstructure and defect configuration.AISI 1020 steel was chosen as it has a simple microstructure(plain ferritic)and composition with low alloying conditions.It is an appropriate material to study the effect of trans-mitting electric pulses on the microstructural defect evolution.A combination of electron-backscattered diffraction and transmission electron microscopy proved to be an effective tool in characterizing the post-electropulsing effects critically.By application of electropulsing,a reduction in the surface residual stress layer was noticed.Also,reductions in misorientation and dislocation density together with the disentan-glement of dislocations within the cold-worked layer were observed after electropulsing.Additionally,the annihilation of shot-peening-induced deformation bands beyond the residual layer depth was observed.These effects have been rationalised by taking into account the various possibilities of athermal effects of electropulsing.
基金supported by the National Nature Science Foun-dation of China(Grant No.50875061).
文摘The fatigue life of components can be significantly enhanced by the formation of the surface hardness layer through surface strengthening technology.To avoid the geometric distortion of thin-walled com-ponents caused by strengthening,the strengthening energy is limited and the ideal strengthening effect cannot be obtained.This work aims to propose a novel approach to address this issue effectively.The surface layer with high-density dislocations was obtained by a low-energy surface strengthening method(shot peening)at first.Then the surface strengthening mechanism changes from dislocation strengthen-ing to grain boundary strengthening after electropulsing treatment(EPT).The evolution of residual stress and microstructure was analyzed using multi-scale characterization techniques.The results demonstrate that EPT followed by surface strengthening makes a remarkable 304%increase in fatigue life of TC11 titanium alloy.The enhancement of fatigue life can be attributed to the grain refinement accompanied by the formation of nanotwins and sub-grains in the surface-strengthened layer,as well as the reduction in dislocation density within the substrate after EPT.This study demonstrates the significant potential of EPT in further enhancing the fatigue life of surface pre-strengthened thin-walled components.
基金National Natural Science Foundation of China(No.U1804251)National Key R&D Program of China(2021YFC2400701)。
文摘Mg-Nd-Zn-Zr(JDBM)alloy was studied as a candidate for biodegradable implant material because of its moderate mechanical properties,good biocompatibility,and favorable uniform degradation behavior.To verify whether JDBM alloy exhibits electroplasticity effect and then study the mechanism of electropulsing treatment on JDBM alloy,in this study,homogenized and pre-tensile deformed samples were treated by electropulsing.After the electropulsing treatment,the average grain size was refined due to recrystallization,micron-scale Mg12Nd secondary phases precipitated slightly,while the morphology of nanoscale Zr particles changed from rodlike to ellipsoidal shape.The elongation to failure(EL)increased obviously for the homogenized and pre-tensile deformed JDBM alloy samples after electropulsing treatment,accompanying with no obvious sacrifice of the yield strength(YS)for the former and an evident decrease of YS for the latter,mainly due to the reduction of the dislocation density.The YS decrement and EL increment(77.57%)for the latter are more apparent attributed to the higher density of dislocations introduced by pre-tensile deformation.Therefore,the electropulsing treatment can obviously improve the mechanical properties of JDBM alloy,especially for the plasticity.The present work opens a new window for the fabrication of JDBM alloy profiles with high mechanical properties,especially for the plasticity,such as the cold drawing wires and tubes for biomedical applications.It also could provide theoretical references for other magnesium alloy processing.
基金Project (NCET-10-0278) supported by the Program for New Century Excellent Talents in University,China
文摘Electron backscattered diffraction （EBSD） and transmission electron microscopy （TEM） were used to investigate effect of electropulsing on microstructure and texture evolution of Ti-6Al-4V during cold drawing. Research results demonstrate that the electropulsing treatment （EPT） can enhance the deformability of the grains with unfavorable orientations, which makes the compatibility of deformation among grains much better. A comparison in texture evolution between conventional cold drawing and EPT cold drawing indicates that the EPT promotes prismatic 〈a〉 slip moving, restricts pyramidal 〈c＋a〉 slip occurring and accommodates the deformation with c-component by grain boundary sliding. The fraction decrease of low-angle grain boundaries for samples deformed with EPT reveals that the application of electropulsing restricts the formation of the incidental dislocation boundaries and the geometrically necessary boundaries.
基金Project(50875061) supported by the National Natural Science Foundation of ChinaProject(20092302110016) supported by the Specialized Research Fund for the Doctoral Program of Higher Education of China
文摘In order to optimize the ductility of orthorhombic Ti2AlNb-based alloys sheet,Ti22Al27Nb sheet was treated by high density electropulsing（J max =6.80 7.09 kA/mm2,tp =110 μs） under ambient condition.Microstructures were observed by SEM,and the tensile properties were also studied using uniaxial tension tests.The experimental results show that electropulsing can refine the microstructures of Ti22Al27Nb sheets.The specimen with the fine and homogeneous microstructures has good plasticity,and its elongation reaches 19.4%.The mechanism about the effect of electropulsing treatment on the microstructure of Ti22Al27Nb sheets was discussed.It was thought that the increase in nucleation rate during phase transformation and a very short treating time were regarded as the main reasons of producing smaller grains and increase in the plasticity by electropulsing.
基金Project(50875061)supported by the National Natural Science Foundation of ChinaProject(20092302110016)supported by the Specialized Research Fund for the Doctoral Program of Higher Education of China
文摘To investigate the effect of the electropulsing on dislocation mobility,specimens cut from the cold-rolled titanium sheet were treated by high density electropulsing with the maximum current density of 7.22,7.64,7.96 kA/mm 2 ,pulse period 110μs.The internal friction and elastic modulus were measured by a dynamic mechanical analyzer（DMA）.When strain amplitude lowers a certain critical one,the damping of the electropulsed titanium sheet is lower than that of the cold-rolled one.When the strain amplitude exceeds the critical one,the damping of the electropulsed titanium sheet is extraordinarily higher than that of the cold-rolled or conventional annealed one.Furthermore,it is found that the damping peak of the electropulsed titanium sheet shifts to lower temperature compared with the conventional annealed one.It is demonstrated that the electropulsing treatment can decrease dislocation tangles and enhance dislocation mobility.
基金Project (50875061) supported by the National Natural Science Foundation of China
文摘Specimens cut from the cold-rolled commercially pure （CP） Ti sheet were treated by high density electropulsing （the maximum current density 7.22 kA/mm2, pulse period 110 las）. The deformation behaviors of the CP Ti specimens at different states were determined by the uniaxial tensile test. The microstructure morphologies were observed by the optical microscopy. The results show that the electropulsing induced formation of f＇me equal-axial grains and lamellar microstructures, which leads to the strength of the electropulsed CP Ti higher than that of the conventional annealed CP Ti. After electropulsing, the tensile strength and yield strength are increased by 100 MPa. And the electropulsed CP Ti has a good plasticity. The experimental results demonstrate that the electropulsing provides an effective approach to enhance the strength of cold-rolled CP Ti sheet and retain the required high ductility.
基金Project(13520503100)supported by the Science and Technology Commission Foundation of Shanghai Municipality,China
文摘Electropulsing rolling （ER） and warm rolling （WR） processes were performed to roll AZ31 magnesium alloy sheets. Mechanical properties, microstructure and texture evolution of these specimens were investigated after rolling. The results indicate that electropulsing accelerates the recrystallization of AZ31 alloy sheets during hot rolling. After electropulsing rolling at a relatively low temperature, the microstructure of the sample shows fine equiaxed recrystallized grains with a lower density of dislocations and precipitates. In contrast, the microstructure of the sample after warm rolling shows elongated grain, numerous deformed twins, and a high density of dislocation and precipitates. Electropulsing rolling helps weaken the basal fiber texture. Although both the alloy sheets （ER and WR） have typical basal fiber texture, the maximum pole intensity of basal in ER sample is weaker. ER sheet has higher yield strength and elongation compared to WR sheet. As a promising technique, electropulsing rolling can be used to improve the microstructure and mechanical properties of materials.
基金Project(2010CB631203)supported by National Basic Research Program of ChinaProject(51001021)supported by the National Natural Science Foundation of ChinaProjects(20100042120008,20100042110006)supported by the PhD Programs Foundation of Ministry of Education of China
文摘Electropulsing treatment（EPT） was performed on a nickel base corrosion resistant alloy during aging.The effect of EPT on the microstructure and corrosion resistance of the alloy and the mechanisms were investigated.The results show that the intergranular corrosion resistance can be improved substantially without the degradation of mechanical properties of the alloy by EPT.The EPT has an effect of enhancing the interface diffusion rate of the alloying element,which is higher than the body diffusion rate.And thus discontinuous precipitation of M23C6 type carbides appears at the grain boundary in the alloy by EPT,which decreases the depletion extent of the alloying elements at the grain boundary substantially.As a result,the intergranular corrosion resistance of the alloy can be improved by the EPT without any degradation of mechanical properties.
基金financially supported by the Fundamental Research Funds for the National Key R&D Program of China(No.2017YFB0306300)the Hunan Provincial Innovation Foundation for Postgraduate(No.CX20200185)+1 种基金the Fundamental Research Funds for the Central Universities of Central South University(No.2020zzts098)the National Natural Science Foundation of China(Nos.19055551,51675538 and 51601060)。
文摘Studies show that the proper solid solution treatment(SST)is a key step in the precipitation strengthening of AA7150 Al alloy.Despite the superior characteristics of the fully dissolved phase,it has major drawbacks,including high consumption of energy and low efficiency.Recently,electropulsing treatment(EPT)has been proposed to study dissolved precipitations and modify microstructures of AA7150 Al alloy faster than conventional SST.Experiments have been conducted in the present article,and the obtained results show that EPT can promote the rapid dissolution of theη’phase at relatively low temperatures in only 20 s.Meanwhile,the strength and ductility of electropulsed samples decrease drastically.Compared with conventional SST,EPT accelerates recrystallization and obtains relatively fine grains after 20 and 50 s electric pulses.Moreover,as the EPT time increases,the corresponding non-uniform local heating and the electron force promote dislocation generation and annihilation.
基金the financial supports by the National Key R&D Program of China(No.2017YFB0306300)the National Natural Science Foundation of China(Nos.51601060,51675538).
文摘The influence of electropulsing on the creep behaviour,strength,and microstructure of an Al−Cu−Li alloy during creep ageing was investigated.Electropulsing assisted creep ageing(ECA)and conventional creep ageing(CCA)were carried out under various stress levels and time conditions.Applying electropulsing results in a noteworthy change of creep behaviour,including a variation in creep curves,an increased creep rate in early stage,and an improved creep strain.The ECA specimen experiences a shorter time to the peak strength,and an increase in elongation by~17.4% without loss of the peak-aged strength compared with CCA specimen.The ultrafine nano-size subgrains are observed to form under electropulsing,which can result in an increased creep strain by increasing grain-boundary sliding.The enhancement of both dislocation interactions and solute diffusion under electropulsing is considered as a primary cause of disappearance of a platform stage during early creep ageing.Some of T1 precipitates around the grain boundary are observed in the peak ECA sample,resulting in an occurrence of transgranular fracture,which is further responsible for an increased elongation of the ECA specimen.
文摘The specimens cut from the cold-rolled pure titanium sheet at 0°,45°and 90°to the rolling direction were treated by high density electropulsing(maximum current density J=(7.22-7.96)×10^(3)A/mm^(2),pulse period t_(p)=110μs).The mechanical properties and microstructures of the cold-rolled,electropulsed and conventional annealed commercially pure titanium sheet were examined by using uniaxial tension test machine and optical microscope(OM),respectively.The results show that the deformation behavior of the electropulsed pure titanium sheet is significantly different from that of conventional annealed pure titanium sheet.The difference of the mechanical properties between the 0°,45°and 90°direction specimens is almost diminished.It is mainly due to the increase in dislocation mobility and formation of lamellar microstructure after the electropulsing.
文摘Electropulsing-induced recrystallization and its effect on mechanical properties of oriented silicon steel strips （Fe-3.0%Si） were studied by optical microscopy, scanning electron microscopy and electron back-scatter diffraction. The results indicated that electropulsing accelerated recrystallization, and decreased the temperature of recrystallization. Electropulsing favors refinement of the grain structure of the alloy. Effects of electropulsing on strength and elongation of the alloy were discussed from the point view of dislocation dynamics, microstructural changes, and electropulsing kinetics.
基金Financial support from the National Key Research and Development Program of China(Nos.2020YFB008300,2020YFB008303,and 2020YFB008304)Provincial Natural Science Foundation of Shandong(No.ZR202102220408)+1 种基金National Natural Science Foundation of China(No.51701080)Talent Development Excellent Young Talents Fund Project China(No.20190103053JH).
文摘Conventional kinetics theory for diffusion-controlled phase transformation shows that the reverse transition should lag behind the temperature rise through rapid heating,i.e.,overheating is required.In this work,we found that theβ-transus temperature decreased by∼50℃ during studying theα→βtransformation in Ti-6Al-4V alloy via electropulsing treatment(EPT).The calculation suggests that the acceleration of transformation kinetics cannot be fully explained by Joule heat and athermal effects of the electromigration effect and electron wind theory.The microstructural evolution during EPT was systematically investigated utilizing scanning electron microscope(SEM),electron backscattered diffraction(EBSD),X-ray diffraction(XRD),transmission Kikuchi diffraction(TKD),and transmission electron micro-scope(TEM).Microscopic analysis shows that the nano-sizedωand O'phases formed in theβphase,which causes large numbers of lattice distortion regions.The defects are conducive to accelerating the bulk diffusion of alloying elements inβ.Moreover,the nanodomains limited the growth of martensite,therefore nanocrystalline martensite formed after quenching.These findings develop the understanding of the destructive effect of current on metallic crystal,which will help to guide microstructural regulation in titanium and other alloys.
基金financial supports from the National Key R&D Program of China (No.2017YFE0123500)。
文摘The effect of electropulsing treatment on microstructure and mechanical strength of laser metal deposited Ti−6Al−4V alloy was investigated in order to eliminate the anisotropy in strength of laser metal deposited Ti−6Al−4V alloy by tensile tests,optical microscopy,scanning electron microscopy,electron back-scattered diffraction analyses and transmission electron microscopy.With increasing applied voltages from 0 to 130 V,the evolution of microstructure within columnarβgrains followed the sequence ofα′martensite→colonyαstructure→basket-weaveαstructure.The electropulsing treated at 130 V weakened the texture of martensite withinβgrains.The as-built Ti−6Al−4V alloy showed an anisotropy in yield strength(6.2%).After processing at 130 V,the anisotropy in yield strength was reduced to 0.6%,which was attributed to the almost equivalent distribution of Schmid factor in the samples deformed along different orientations.
基金Funded by National Natural Science Foundation of China(No.50571048)Research&Development Funding Project of Shenzhen(No.JCYJ20120619152539900)
文摘Electropulsing is introduced into the cutting process for quenched and tempered 45 steel, which is a novel method to improve the material machinability compared with the conventional cutting process. The effects of electropulsing on cutting performances, microstructure evolution, and surface qualities of 45 steel rods were studied. The results indicate that electropulsing is beneficial for the cutting process in 3 aspects as follows：（1） reducing the principal cutting force, surface microhardness and surface roughness of the machined sample dramatically;（2） improving the machining efficiency and prolonging the life of cutting tools;（3） decreasing the thickness of rheological layer which was usually caused by work hardening in the cutting process. The morphology and microstructure of the cutting chips showed that the length of the chips increased significantly with the increase of the current density. The advantage of electropulsing is that it can improve the plastic deformation capability as well as increase the lubricating property between the specimen and the cutting tool.
基金This work was supported financially by the National Natural Science Foundation of China(Nos.51974003 and 51304003)the National Key Research and Development Program of China(No.2017YFB0305100).
文摘We explore the application of electropulsing for the control of phase transformation in a low-carbon steel.The effect of electropulsing on the transformation from austenite to ferrite in continuous casting low-carbon steel slab has been studied through experimental and thermodynamic investigations.The results reveal that electropulsing promotes the precipitation of ferrite within austenite grain in the low-carbon steel.When the electropulsing intensity increases,the precipitation of ferrite increases within austenite grains,and ferrite omentum precipitates become thinner along the austenite grain boundary.The results provide a basis for controlling the austenite to ferrite transformation in low-carbon steel.
基金supported by the Natural Science Foundation of Shandong Province(No.ZR2016EEM25)
文摘The effect of electropulsing on the mechanical behaviors and microstructures of Ti-6Al-4V titanium alloy was investigated by an uniaxial tensile test. Compared to the value measured in cold tensile test, the alloy exhibits lower ultimate tensile strength when the tensile deformation is assisted by electropulsing. The tensile elongation is found to vary non-monotonically with increasing root mean square(RMS) current density. Though decreasing at first, the tensile elongation increases with current density once the value exceeds 8.1 A/mm^2. Through applying current with RMS current density of 12.7 A/mm^2, the tensile elongation at strain rate 0.001 s^(-1) can be improved by 94.1%. In addition, it is observed that more remarkable electroplastic effect is induced by the higher peak current density under similar thermal effect. Microstructure analysis reveals that the low plasticity at 8.1 A/mm^2 is attributed to the micro-void easily formation near the tips of acicular β phases. The enhanced ductility at higher current densities, on the other hand, is attributed to the dynamic recrystallization.
基金Item Sponsored by National Natural Science Foundation of China(51371065)Postdoctoral Science-Research Developmental Foundation of Heilongjiang Province of China(LBH-Q12073)
文摘The effect of electropulsing treatment（EPT）on the microstructure of a Ti-based bulk metallic glass（BMG）has been studied.The maximum current density applied during EPT can exert a crucial role on tuning the microstructure of the BMG.When the maximum current density is no more than 2 720A/mm^2,the samples retains amorphous nature,whereas,beyond that,crystalline phases precipitate from the glassy matrix.During EPT,the maximum temperature within the samples EPTed at the maximum current densities larger than 2 720A/mm^2 is higher than the crystallization temperature of the BMG,leading to the crystallization event.
文摘The effects of dynamic electropulsing on microstructure changes and phase transformations of a rolled Mg-9Al-1Zn alloy were studied by using optical microscopy, X-ray diffraction, back-scattered scanning microscopy and transmission electron microscopy techniques. The decomposition of β phase was accelerated under dynamic electropulsing, compared with the conventional thermal processes. Dynamic electropulsing was less effective in affecting the phase transformations, but more effective in reducing residual stress than the static electropulsing. Dynamic electropulsing improved machinability of single point diamond turning, the mechanism of which is discussed from the point of view of dislocation dynamics.
